Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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Anal. Chim. Acta 633 (2) 188-196 (2009). HPTLC of lycorine and galanthamine from Narcissus jonquilla ‘Pipit’ on silica gel with chloroform - methanol - 25 % ammonia 18:1:1. Quantitative evaluation by absorbance measurement at 207 nm. The correlation coefficients were r=0.9882 and 0.9908, respectively, for the mean values of galanthamine and lycorine. Investigation of different extraction solvents showed that extraction with methanol and 1 % tartaric acid in methanol at default conditions (120 °C, p = 60 bar, time: 10 min, one static cycle) provide the highest yields of total alkaloids, whereas for toluene the lowest amounts were measured. Lycorine to galanthamine mean ratios were dependant on the type of solvent used, and in toluene galanthamine and related alkaloids were preferably extracted.
Asian Journal of Chemistry 23 (5), 2098-2100 (2011). HPTLC of glycyrrhizic acid in herbal formulation on silica gel with chloroform - glacial acetic acid - methanol - water 15:8:3:2. The hRf value of glycyrrhizic acid was 28. Quantitative evaluation by absorbance measurement at 254 nm. The method was found to be linear in the range of 100-500 ng/band with average recovery between 99-102 %.
Asian Journal of Chemistry 23(5), 1917-1921 (2011). TLC of concentrated methanolic extracts of a polyherbal ayurvedic syrup formulation (containing vasaka as main ingredient) on silica gel with methanol - toluene - dioxane - 25 % ammonia 2:2:5:1. The hRf value of vasicine was 74. Quantitative evaluation by absorbance measurement at 254 nm using vasicine as marker for standardization of the formulation. The method was found to be linear in the range of 4-12 ng/band. Isolation of vasicine from Adhatoda varica is also described.
Asian Journal of Chemistry 23 (5), 2046-2048 (2011). TLC of alpha- and beta-asarone in Acorus calamus on caffeine modified silica gel (with 10 % caffeine in dichloromethane and dried at 100 °C for 10 min) with toluene - ethyl acetate 93:7. The hRf value of alpha-asarone was 67 and of beta-asarone 77. Quantitative evaluation by absorbance measurement at 313 nm. The linearity was in the range of 50-1000 ng/band for beta-asarone. The alcoholic extracts of samples from different geographical regions were found to contain 0.2-0.8 % of alpha-asarone and 8.7-11.2 % of beta-asarone.
of Chromatogr. A 1231, 59-65 (2012) Reversed-phase HPTLC of lutein, lycopene and beta-carotene standards on RP-18 (pre-washed by development with dichloromethane – methanol 1:1) with methanol – acetone 1:1 with 0.1 % of 2-tert-butylhydroquinone. The hRf value was 4 of lutein esters, 24 of beta-carotene, 32 of lycopene, and 68 of lutein. Quantitative determination of lutein by densitometry at 450 nm. The repeatabilities were %RSD = 3.4, 1.3 and 1.6 at levels of 5 ng, 15 ng and 25 ng, respectively (n = 6). The calibration curve was best fit with a polynomial function in the range of 5-30 ng. The LOD was 1.5 ng, the LOQ 5 ng. With these chromatographic conditions also dietary carotenoids lutein esters, lycopene, free lutein and ß-carotene from food supplements were identified. It was shown that the standards remain stable on the plate for 1 h after chromatogram development.
Kinetic evaluation of the degradation process and identification of photoproducts by mass spectrometry. J. Liq. Chromatogr. Relat. Technol. 36, 2431-2445 (2013). HPTLC of difloxacin and its degradation products on silica gel with methylene chloride - methanol - 2-propanol - ammonia 25 % 4:4:5:2. Quantitative determination by absorbance measurement at 294 nm. The hRf values of difloxacin and its degradation products were 43, 25, 32, 39, respectively. Linearity was 1.2-2.4 µg/zone. LOD and LOQ were 0.01 and 0.03 µg/zone, respectively. Intermediate precision was below 2.0 %. Recovery (by standard addition) was in the range of 101.1-110.9 %.
J. Liq. Chromatogr. Relat. Technol. 36, 2387-2394 (2014). The image processing programs ImageJ and Sorbfil TLC Videodensitometer were compared to study direct antioxidant properties of compounds separated from extracts obtained from Medicago sativa. Comparable results were obtained based on built-in functions present in both programs for processing TLC videoscans.
J. Planar Chromatogr. 27, 245-250 (2014). HPTLC of fructooligosaccharides DP3-DP9 in Morinda officinalis on silica gel with n-butanol - isopropanol - water - acetic acid 7:5:2:1. Detection by spraying with 1-naphthol–sulfuric acid reagent, followed by heating at 110 ºC for 3 min. Quantitative determination by absorbance measurement at 585 nm. The hRF values for DP3 to DP9 were between 20 and 70. Linearity was in the range of 150-1050 ng/zone for DP3, 137-962 ng/zone for DP4 and DP5, 131-919 ng/zone for DP6 and DP9, 144-862 ng/zone for DP7 and 156-1094 ng/zone for DP8. The intermediate/interday/intra-day precisions were below 5 % (n=6). Average recoveries for DP3 to DP9 were between 91.4 and 99.0 %.