Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      108 050
      HPTLC estimation of nateglinide in bulk drug and tablet dosage form
      D. KALE*, R. KAKDE (*Dept. of Pharmaceutical Sciences, R.T.M. Nagpur University, Amravati Rd., Nagpur, India)

      Asian Journal of Chemistry 23(10), 4351-4354 (2011). HPTLC of nateglinide in tablet dosage form on silica gel with n-hexane - methanol - isopropanol 75:15:10. The hRf value was 56. Quantitative evaluation by absorbance measurement at 210 nm. The method was linear in the range of 300-1000 ng/band. The average recovery was 98.5 %.

      Classification: 17a
      108 093
      Validated stability-indicating HPTLC and HPLC methods for determination of pipazethate and its degradant
      G. HADAD*, R. SALAM, S. EMARA (*Faculty of Pharmacy, Pharmaceutical Analytical Chemistry Department, University of Suez Canal, Ismailia, 41522, Egypt, ghhadad@yahoo.com)

      J. Liq. Chromatogr. Relat. Technol. 34, 1850-1869 (2011). HPTLC of pipazethate (1) and its degradant 10H-pyrido[3,2-b][1,4] benzothiadiazine-10-carboxylic acid (2) on silica gel with chloroform - diethylamine - methanol 94:1:5. Quantitative determination by absorbance measurement at 225 nm. The hRf values of (1) and (2) were 35 and 28, respectively. Linearity was between 2-9 µg/zone for (1) and 1-6 µg/zone for (2). Limits of detection and quantification were found to be 53 and 180 ng/zone for (1), and 40 and 130 ng/zone for (2), respectively. Recoveries (by standard addition) were 100.1 % for (1) and 99.5 % for (2). Comparable results were obained with a validated HPLC method.

      Classification: 32a
      108 113
      Validated HPTLC method for quantification of myrecitin in the stem bark of Myrica esculenta Buch
      K.G. PATEL*, V.G. PATEL, K.V. PATEL, T.R. GANDHI (*Anand Pharmacy College, Shri Ram Krishna Seva Mandal Campus, Near Town Hall, Anand, Gujarat, India; kalpana_jpatel@yahoo.com)

      Ham. Ex D. Don, Myricaceae. J. Planar Chromatogr. 23, 326-331 (2010). HPTLC of myrecitin and stem bark extracts on silica gel with toluene - ethyl acetate - formic acid - methanol 15:15:3:2. Quantitative determination by absorbance measurement at 268 nm. Linearity was between 0.4-2.0 µg/band. The limits of detection and quantitation were 93 ng and 284 ng/zone. The intra-day and inter-day precision of the method was in the range of 0.14-0.55 %. The recovery of myrecitin at three concentrations was in the range of 98.9-100.1 % and the average recovery was 99.3 %.

      Classification: 32e
      108 137
      Ecogeographical phytochemistry of Adhatoda vasica Nees in relation to quantitative variations of alkaloids
      A. VARMA, H. PADH, N. SHRIVASTAVA* (*B. V. Patel Pharmaceutical Education & Research Development (PERD) Centre, Sarkhej - Gandhinagar Highway, Thaltej, Ahmedabad - 380054, Gujarat, India; neetashrivastava_perd@yahoo.co.in)

      J. Planar Chromatogr. 24, 406-411 (2011). HPTLC of plant extracts and vasicine on silica gel with ethyl acetate - methanol - ammonia (17.3 % ammonia) 40:10:1 in a twin-trough chamber saturated for 15 min. Quantitative determination by densitometry at 298 nm. The hRf value of vasicine was 47. The limit of detection and the limit of quantification was 40 and 100 ng/zone, respectively. The average intra-day and inter-day precision was 0.7 and 2.2 %, respectively. Linearity was between 100-1300 ng/zone with a correlation coefficient of 0.999 and a %RSD of 2.3 %. Average recovery was 98.9 %.

      Classification: 32e
      109 026
      Development and validation of HPTLC method for the determination of andrographolide in Kalmegh Navayas Loha - an Ayurvedic formulation
      R. PAWAR*, Shivani SHARMA, K. SINGH, R. SHARMA (*Pharmacopoeial Laboratory for Indian Medicine, Ghaziabad-201002, India)

      International Journal of Pharmacy and Pharmaceutical Sciences 3(2), 85-89 (2011). TLC of andrographolide on silica gel with toluene - ethyl acetate - formic acid 10:9:1. Densitometric evaluation at 235 nm before derivatization. Evaluation of the fingerprint profile at 254 nm and after derivatization at 366 nm by spraying with anisaldehyde-sulfuric acid reagent followed by heating at 110 °C.

      Classification: 8b
      109 047
      A HPTLC method for quantitative estimation of L-dopa from Mucuna pruriens in polyherbal aphrodisiac formulation
      Urmila VACHHANI, Manisha TRIVEDI, Amrita BAJAJ, Charmi SHAH* (*Dept. of Analysis ROFEL, Shri G M Bilakhia College of Pharmacy, Namdha campus, Vapi Namdha Rd.,Vapi, (Guj), India)

      Research Journal of Pharmaceutical, Biological and Chemical science 2(12), 389-396 (2011). TLC of a polyherbal formulation containing Mucuna pruriens with L-dopa as biological marker on silica gel with n-butanol - water - glacial acetic acid 4:1:1 with chamber saturation for 30 min. Detection by dipping in a 0.5 % solution of ninhydrin in ethanol, followed by heating at 120 °C for 2 min. Quantitative determination of L-dopa by densitometry in absorbance mode at 520 nm. The hRf value of L-dopa was 37. Linearity was given in the range of 600-1400 ng/zone.

      Classification: 17a
      109 070
      Determination of sulfonated water-soluble azo dyes in food by SPE coupled with HPTLC-DAD
      T. TUZIMSKI (Department of Physical Chemistry, Chair of Chemistry, Faculty of Pharmacy with Medical Analytics Division, Medical University in Lublin, 4A Chodzki Street, 20-093 Lublin, Poland; tomasz.tuzimski@umlub.pl)

      J. Planar Chromatogr. 24, 281-289 (2011). TLC of tartrazine (E 102), quinoline yellow (E 104), azorubin (E 122), ponceau 4R (E 124), allura red AC (E129), patent blue V (E 131), and brilliant blue FCF (E133) on RP-18 or cyano phase with methanol - acetate or citric buffer containing diethylamine or octane-1-sulfonic acid sodium salt. Quantitative determination by densitometry in the range of 200-800 nm with a diode array scanner. The LOD and LOQ were 33, 54, 93, 119, 87, 31, 59 and 99, 164, 281, 362, 263, 95, 179 ng/zone for E 102, E 104, E 122, E 124, E 129, E 131, and E133, respectively. The correlation coefficients were 0.9970, 0.9963, 0.9895, 0.9965, 0.9930, 0.9975, and 0.9920, respectively. The linearity was given in the range of 2.5-40 and 2.5-70 µg/mL.

      Classification: 30a
      109 090
      Thin layer chromatographic method for the determination of flurbiprofen
      V. JAGATHI*, V. RAJESH, D. RAMESH, G. DEVALARAO (*K.V.S.R. Siddhartha College Pharmaceutical Sciences, Siddhartha Nagar, Vijayawada, A.P., India)

      Research Journal of Pharmaceutical, Biological and Chemical Sciences 2(1), 108-110 (2011). TLC of flurbiprofen in raw material and tablet dosage form on silica gel with chloroform - methanol - 25 % ammonia 45:5:3. Quantitative evaluation by absorbance measurement at 247 nm. The method was linear in the range of 50-600 ng/band. The sample was subjected to different stress conditions and all the degradation products were well resolved from the main compound. The method can therefore be used for stability studies.

      Classification: 32a
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