Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      101 078
      Influence of impregnation of silica gel and Kieselguhr with copper(II) sulphate (VI) on profile change of the spectrodensitograms and the Rf values of nicotinic acid and its derivatives
      Alina PYKA*, W. KLIMCZOK (*Department of Analytical Chemistry, Faculty of Pharmacy, Medical University of Silesia, Jagielonska 4, 41-200 Sosnowiec, Poland; apyka@slam.katowice.pl)

      J. Liq. Chromatogr. Relat. Technol. 31, 526-542 (2008). TLC of nicotinic acid, nicotinamide, ethyl, isopropyl, butyl, hexyl, benzyl nicotinate, N-methylnicotinamide, N,N-diethylnicotinamide, 3-pyridinecarbaldehyde, 3-pyridinecarbonitrile, 3-pyridylmethanol, and methyl 3-pyridyl ketone on silica gel and kieselguhr impregnated with 2.5 % and 5 % aqueous solutions of copper(II)sulfate, with acetone - n-hexane in different volume compositions. Detection by spraying with Rhodamine B solution. Quantitation by densitometry. The number of absorption bands of the compounds investigated depends on impregnation of the sorbent and the visualization agent.

      Classification: 32a
      102 011
      QUANTITATIVE ANALYSIS OF PROPRANOLOL HYDROCHLORIDE BY HIGH PERFORMANCE THIN LAYER CHROMATOGRaPHY
      G. Bhavar*, V. Chatpalliwar (*Dept. of Pharmaceutical Chemistry, R. C. Patel College of Pharmacy, Karvad Naka, Shirpur 425405, India)

      Ind. J. Pharm. Sci. 70 (3), 395 - 398 (2008). TLC of propranolol hydrochloride on silica gel with isopropanol - ethyl acetate - ammonia 2:17:1. Quantitative determination by absorbance measurement at 290 nm. The linearity of the method was between 200 and 2000 ng/spot. The method was successively applied for tablets, wherein, no interference from tablet excipients was observed.

      Classification: 6
      102 034
      Determination of dutasteride from its bulk drug and pharmaceutical preparations by HPTLC
      S. KAMAT*, V. VELE, V. CHOUDHARI, S. PRABHUNE (*Ramnarian Ruia College, Dept. of Chem.,Matunga, Mumbai 400019, India, swarup_80@rediffmail.com)

      Asian J. Chem. 20(7), 5514-5518 (2008). HPTLC of dutasteride on silica gel with toluene - ethyl acetate - acetic acid 14:6:1. Absorbance measurement at 210 nm. The method was linear in the range of 50-500 µg/µL. Recovery was 99.3-99.5 %. The method was suitable for routine quality control.

      Classification: 13a
      102 055
      Application of densitometry for the evaluation of the separation effect of nicotinic acid derivatives
      Alina PYKA*, W. KLIMCZOK (*Department of Analytical Chemistry, Faculty of Pharmacy, Silesian Academy of Medicine, 4 Jagiellonska Street, 41-200 Sosnowiec, Poland; apyka@slam.katowice.pl)

      Part I. Nicotinic acid and its amides. J. Liq. Chromatogr. Relat. Technol. 30, 2317-2327 (2007). TLC and HPTLC of nicotinic acid, nicotinamide, N-methylnicotinamide, and N,N-diethylnicotinamide on RP-18 with methanol - water 3:7, and dioxane - water 1:4 and 1:9. The best separation was achieved on alumina with acetone - n-hexane 1:1. Detection under UV light at 254 nm. Quantitative determination by absorbance measurement at 254 nm.

      Classification: 17c
      102 086
      High performance thin layer chromatographic method for quantitative determination of curcuminoids in Curcuma longa germplasm
      M. PARAMASIVAM*, R. POI, H. BANERJEE, A. BANDYOPADHYAY (*Department of Agricultural Chemicals, Faculty of Agriculture, Bidhan Chandra Krishi Viswavidyalaya, Mohanpur, India, sivam25@gmail.com)

      Food Chemistry 113, 640-644 (2009). HPTLC of curcumin (1), demethoxycurcumin (2), and bisdemethoxycurcumin (3) from the rhizomes of Curcuma longa on silica gel with chloroform – methanol 24:1. Quantitative determination by absorbance measurement at 425 nm. The hRf values of (1), (2), and (3) were 66, 48, and 30, respectively. Selectivity regarding matrix was given. Recovery was 98.7 % for (1), 96.3 % for (2), and 97.2 % for (3). The limit of detection for (1), (2), and (3) was 0.1 µg/spot. The linear regression equation was y=4447.26 + 61.993X for (1), y=1089.881 + 70.003X for (2), and y=2611.84 + 51.565X for (3).

      Classification: 30b
      102 104
      High performance thin layer chromatographic determination of carvedilol
      L. Gupta*, S. BHALERAO, S. TAMBE, V. KASTURE (*M. G. V.’s Pharmacy College, Nashik, Maharashtra, India)

      60th Indian Pharmaceutical Congress PA-204, (2008). HPTLC of carvedilol on silica gel with methanol - ethyl acetate 13:7. The hRF was 49. Quantitative determination by absorbance measurement at 242 nm. Linearity was between 200-1000 ng/spot. The recovery was 98-102 %. The method was suitable for routine quality control of the drug in formulation.

      Classification: 32a
      102 121
      Validated HPTLC method and content uniformity test for analysis of telmisartan and hydrochlorothiazide in tablet dosage forms
      S. Mogre*, B. Mehta (*Dept. of Chemistry, University of Mumbai, Vidyanagari, Santacruz (E) Mumbai 400098, India)

      J. Pharm. Res. 7(2), 126-128 (2008). HPTLC on silica gel with acetone - chloroform - ethyl acetate - methanol 6:6:6:1. Quantitative determination by absorbance measurement at 280 nm. The hRf value for telmisartan was 27 and for hydrochlorothiazide 45. The regression curve shows good linear relationship in the concentration range of 25.5 - 128.0 µg for hydrochlorothiazide and 81.6 - 408.0 µg for telmisartan. The content uniformity test was carried out as per the USP specification of the content uniformity test. The percent drug estimated from the marketed formulations were found to be in the range 99.3 and 100.5 for both drugs. The percent recoveries of drug carried out by the standard addition method was found to be 100.3 and 99.4 for hydrochlorothiazide and telmisartan respectively. The proposed method was found suitable for routine quality control and content uniformity tests.

      Classification: 32a
      102 140
      Use of video densitometry and scanning densitometry to study an impact of silica gel and L-arginine on the retention of ibuprofen and naproxen in TLC systems
      M. SAJEWICZ, M. GONTARSKA, A. DABROWA, Teresa KOWALSKA* (*Institute of Chemistry, Silesian University, 9, Szkolna Street, 40-006 Katowice, Poland; kowalska@us.edu.pl)

      J. Liq. Chromatogr. Relat. Technol. 30, 2369-2383 (2007). TLC of 2-arylpropionic acids, namely ibuprofen and naproxen, on silica gel and silica gel impregnated with a 0.03 mol/L solution of L-arginine in methanol by dipping for 2 s, with ethanol and ethanol containing several drops of acetic acid. Quantitative determination by absorbance measurement at 254 nm. It was demonstrated that the crystalline chirality of the silica gel adsorbent is most probably responsible for the horizontal enantioseparation, whereas the molecular chirality of L-arginine deposited on the silica gel layer is responsible for the vertical enantioseparation.

      Classification: 32a
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