Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

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      102 033
      Determination of sterols and fatty acids in prostata health dietary supplements by silica gel high performance thin layer chromatography with visible mode densitometry
      T. HALKINA, J. SHERMA* (*Department of Chemistry, Lafayette College, Easton, PA 18042, USA; shermaj@lafayette.edu)

      J. Liq. Chromatogr. Relat. Technol. 30, 2329-2335 (2007). HPTLC of sterols and fatty acids on silica gel (prewashed with methanol) with petroleum ether (36-60 °C) - diethyl ether - acetic acid 80:20:1 in a twin-trough chamber with chamber saturation. Detection by spraying with a 5 % ethanolic phosphomolybdic acid solution followed by heating at 110 °C for 10 min. Quantitative determination by absorbance measurement in the visible range.

      Classification: 11a, 13c
      102 054
      Stability-indicating HPTLC method for analysis of moclobemide, and use of the method to study degradation kinetics
      S.S. PATEL*, R.S. KESHALKAR, M.B. PATEL (*Department of Pharmaceutical Chemistry, Shri S. K. Patel College of Pharmaceutical Education and Research Centre, Ganpat University, Mehsana, Gujarat, 411038, India)

      Chromatographia 68 (9-10), 855-859 (2008). HPTLC of moclobemide on silica gel with benzene – methanol – 40 % ammonia 70:30:1. Quantification by absorbance measurement at 238 nm. The degradation products reached under acidic, basic, and oxidising conditions were well resolved from the pure drug. Linearity was in the range of 50–600 ng/band, with a determination coefficient r2 of 0.9967 ± 0.51. LOD and LOQ, determined experimentally, were 10 and 30 ng/band, respectively. The method was used to investigate the kinetics of alkaline degradation, the Arrhenius plot was constructed and the activation energy calculated.

      Classification: 17c
      102 085
      Analysis of natural colorings in foods by thin layer chromatography
      H. OKA*, N. OZEKI, T. HAYASHI, Y. ITAKURA (*School of Pharmacy, Kinjogakuin University, Omori, Morigama-ku, Nagoya 463-8521, Japan; oka@kinjo-u.ac.jp)

      J. Liq. Chromatogr. Relat. Technol. 30, 2021-2036 (2007). TLC of carotenoid colorings of 95 commercial foods (33 for tomato color [lycopene], 38 for orange color [e.g. fatty acid ester of beta-cryptoxanthin], and 24 for marigold colorings [fatty acid ester of lutein]) on RP-18 with acetonitrile - acetone - n-hexane 11:7:2 and acetone - water 9:1. TLC of beta-carotene and paprika colorings of 77 commercial foods (e.g. capsanthin and its esters) on RP-18 with n-hexane - acetone - acetonitrile 2:7:1. TLC of quinone colorings (lac and cochineal colors) on RP-18 with methanol - 0.5 mol/L oxalic acid 11:9. TLC of anthocyanin colorings of 45 commercial foods (red cabbage color [derivatives of cyanidin acylglycoside]) on RP-18 with acetonitrile - 0.2 mol/L trifluoroacetic acid 1:2. Identification by recording of visible absorption spectra.

      Classification: 30b
      102 103
      Simultaneous determination of 3-acetyl-11-keto-beta-boswellic acid and 6-gingerol by HPTLC
      A. GOEL*, F. AHMAD, R. SINGH, R. GOEL, G. SINGH (*Indian Pharmacopeia Commission, Central Indian Pharmacopoeia Laboratory, Raj Nagar, Ghaziabad, U.P., India)

      60th Indian Pharmaceutical Congress PA-202 (2008). HPTLC of 6-gingerol and 3-acetyl-11-keto-beta-boswellic acid on silica gel with n-hexane - ethyl actate 7:3 in a chamber saturated at ambient temperature. Quantitative determination by absorbance measurement at 254 nm. The hRf values were 48 and 58 for 3-acetyl-11-keto-beta-boswellic acid and 6-gingerol respectively. The recovery was 98.7-100.8 % for both compounds. The chromatographic conditions were suitable for routine analysis.

      Classification: 32c
      102 120
      Simultaneous densitometric determination of 6-gingerol and 6-shogaol in some commercial gingers (Zingiber officinale Roscoe)
      F. MELIANITA, S. CHOLIFAH, E. SUMARLIK, W. F. KARTINASARI, G. INDRAYANTO* (*Faculty of Pharmacy, Assessment Service Unit, Airlangga University, Surabaya, Jl. Dharmawangsa dalam, Surabaya 60286, Indonesia; gunawanindrayanto@yahoo.com)

      J. Liq. Chromatogr. Relat. Technol. 30, 2941-2951 (2007). TLC of 6-gingerol and 6-shogaol in commercial Ginger on silica gel with n-hexane - diethyl ether 2:3. Detection by spraying with anisaldehyde - sulfuric acid reagent. Evaluation under white light and quantitative determination by absorbance measurement at 577 nm.

      Classification: 32e
      102 139
      Validated high performance thin layer chromatography method for simultaneous estimation of rofecoxib and tizanidine hydrochloride in pure and tablet dosage forms
      C. ROOSEWELT*, N. HARIKRISHNAN, P. MUTHUPRASANNA, P. SHANMUGAPANDIYAN, V. GUNASEKARAN (*Dept. of Pharmaceutical Analysis, Vel’s College of Pharmacy, Pallavaram, Chennai 600117, India, kalavaivgs30@rediffmail.com)

      Asian J. Chem. 19(6), 4286 - 4290 (2008). HPTLC of rofecoxib and tizanidine hydrochloride on silica gel with acetone - methanol 1:1. The method was linear in the range of 2200-3300 ng/spot and 180-260 ng/spot for rofecoxib and tizanidine respectively. The recovery was between 99.7 and 102.6 % for both compounds. The method was useful for the simultaneous estimation of the drug content in pure and tablet dosage form.

      Classification: 32a
      102 156
      Simultaneous estimation of levofloxacin hemihydrate and ornidazole in tablet dosage form by HPTLC
      K. SURENDRA*, S. Mageswari, R. Maheswari, N. Harikrishnan, C. Roosewelt & V. Gunasekaran (*Dept. of Pharmaceutical Analysis, Vel’s College of Pharmacy, Chennai 6000117, India, kalavaivgs30@rediffmail.com)

      Asian J. Chem. 19(7), 5647-5651 (2007). HPTLC of levofloxacin hemihydrate and ornidazole on silica gel with n-butanol - water - acetic acid 3:1:1. Quantitative determination by absorbance measurement at 366 nm. The method was linear in the range of 1050-1400 µg/mL and 2600-2900 µg/mL for levofloxacin and ornidazole respectively. The recovery was between 97.3 and 98.0 % for both drugs. The method was suitable for simultaneous estimation of both drugs in combined tablet dosage form.

      Classification: 32a
      103 041
      Determination of Fructose, Glucose and Sucrose in Beverages by High-Performance Thin-Layer Chromatography
      J. SHERMA*, D. ZULICK (*Department of Chemistry, Lafayette College, Easton, PA 18042-1782, USA)

      Acta Chromatographica 6, 7-14 (1996). HPTLC of fructose, glucose and sucrose on a channeled silica gel plate with concentration zone with acetonitrile - water 17:3 for three times (freshly prepared each time, taking 15 min per run) with chamber saturation for 10-15 min. Before, just the silica gel layer was impregnated by spraying with 0.10 M sodium bisulfate solution, and subsequently with citrate buffer (1:10 dilution of citrate buffer with water, pH 4.8), each followed by drying. Detection by spraying with 1-naphthol-sulfuric acid reagent, followed by heating at 100-110 °C for 5-10 min. Quantitative determination by absorbance measurement at 515 nm. The hRf values of fructose, glucose and sucrose were 47, 43, and 28, respectively, and selectivity regarding matrix was given. No zones other than the sugars were detected in sample chromatograms because of the selectivity of the detection reagent and the retention of the beverage components in the preadsorbent. Correlation coefficients (r) for linear regression of the calibration curves typically ranged from 0.90-0.99, with an average of 0.97. The precision in matrix was 2.5 % (n = 5). The mean reproducibility of the twofold sample analyses was 4 %, ranged between 0.45 % and 7.5 %. The accuracy of the method was 94.6 %, 97.0 % and 90.8 % for sucrose, glucose and fructose, respectively. Sugar concentrations in the samples ranged from 18.4-34.3 mg/mL.

      Classification: 10a
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