Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      98 105
      Quantitative determination of sildenafil citrate in herbal medicinal formulations by high-performance thin-layer chromatography
      T. S. REDDY, A. S. REDDY, P. S. DEVI* (*Analytical Chemistry Division, Indian Institute of Chemical Technology, Tarnaka, Hyderabad-500007, India)

      J. Planar Chromatogr. 19, 427-431 (2006). HPTLC of sildenafil citrate on silica gel, pre-washed with methanol, with toluene - acetone - methanol 3:1:1 in a saturated twin-trough chamber. Quantitative determination by absorbance measurement at 312 nm. The method was validated in accordance with ICH guidelines on the validation of analytical methods.

      Classification: 32a
      99 019
      Determination of the effects of estivation and starvation on neutral lipids and phospholipids in Biomphalaria glabrata (NMRI strain) and Helisoma trivolvis (Colorado strain) snails by quantitative High Performance Thin-Layer Chromatography-densitometry
      M. M. WHITE, B. FRIED*, J. SHERMA (*Department of Biology, Lafayette College, Easton, PA 18042, USA; friedb@lafayette.edu)

      J. Liq. Chromatogr. & Relat. Technol. 29, 2167-2180 (2006). HPTLC of neutral lipids on prewashed silica gel with petroleum ether - diethyl ether - glacial acetic acid 80:20:1; and of methyl and steryl esters with hexane - petroleum ether (35-60°C) - diethyl ether - glacial acetic acid 50:25:5:1 in a twin trough chamber saturated for 20 min. Detection by spraying with a 50 % solution of phosphomolybdic acid in ethanol, followed by heating at 115°C for 10 min. Polar lipids were separated with chloroform - methanol - water 65:25:4. Detection by spraying with 10 % cupric sulfate solution, followed by heating at 140 °C for 10 min. Quantitative determination by absorbance measurement at 610 nm for neutral lipids and at 370 nm for polar lipids.

      Classification: 11c
      99 101
      Validated High Performance Thin Layer Chromatography Method for Simultaneous Estimation of Ofloxacin and Ornidazole in Tablet Dosage Form
      M. GANDHIMATI*, T. K. RAVI, Nilima SHUKLA (*Department of Pharmaceutical Analysis,Sri Ramkrishna College of Pharmacy, 395, Sarojini Naidu Road, Coimbatore 641044, India)

      Ind. J. Pharm. Sci. 68 (6), 838-840 (2006). HPTLC of ofloxacin and ornidazole in tablet dosage form on silica gel with n-butanol - ethanol - ammonia 5:5:4. Quantitative determination by absorbance measurement at 295 nm. The method was found to be linear in the concentrate range of 1-5 ng/spot with recovery of 99.5-102.5 % for both compounds. The method was validated for linearity, accuracy, precision, repeatability, and specificity.

      Classification: 32a
      99 146
      Separation and evaluation of free radical-scavenging activity of phenol components of Emblica officinalis extract by using an HPTLC-DPPH method
      O. POZHARITSKAYA, S. IVANOVA, A. SHIKOV*, V. MAKAROV (*Interregional Center “Adaptogen”, Piskarevsky prosp., St.-Petersburg, Russia, alexs79@mail.ru)

      J. Sep. Sci. 30, 1250-1254 (2007). HPTLC of Emblica officinalis extract on silica gel with ethyl acetate – formic acid – glacial acetic acid – water 10:1:1:2. Primary detection under UV 280 nm. Antiradical activity of individual components was estimated on intensity of disappearance of violet/purple background of plate after dipping in DPPH radical solution (0.5 mM in methanol) at room temperature for 90 s and that 30 s at 60 °C. Quantitative determination by absorbance measurement at 517 nm as negative peak. DPPH radical scavenging activity of emblicanins A and B was 7.9 and 11.2 times more active than that of ascorbic acid and 1.3 and 1.8 times more active than gallic acid, respectively.

      Classification: 32e
      100 022
      TLC and HPLC analysis of the flavonoid glycosides in the aerial parts of Peucedanum tauricum Bieb
      Magdalena BARTNIK*, K. GLOWNIAK, A. GROMEK (*Department of Pharmacognosy, Medical Plant Laboratory, Skubiszewski Medical University, Chodzki 1, 20-093 Lublin, Poland; mbartnik@pharmacognosy.org)

      J. Planar Chromatogr. 20, 127-130 (2007). TLC of isorhamnetin-3-glucoside, isorhamnetin-3-rutinoside, kaempferol-3-rhamnosidoglucoside, isoquercitrin, rutoside, hyperoside on silica gel in horizontal chamber with ethyl acetate - methyl ethyl ketone - formic acid - water 5:3:1:1 or ethyl acetate - formic acid - water 9:1:1. Quantitation by scanning at 366 nm; detection by spraying with a 1 % methanolic solution of Natural Product Reagent A followed by a 4 % methanolic solution of polyethylene glycol 400.

      Classification: 8a
      100 040
      Assessing the authenticity of absinthe using sensory evaluation and HPTLC analysis of the bitter principle absinthin
      D. LACHENMEIER (Chemisches und Veterinaeruntersuchungsamt, Karlsruhe, Germany, lachenmeier@web.de)

      Food Res. Int. 40, 167-175 (2007). HPTLC of absinthin in absinthe beverage (from the wormwood plant Artemisia absinthium L.) on silica gel with acetone - acetic acid (98 %) – toluene – dichloromethane 1:1:3:5. Detection by dipping into a solution of acetic anhydride – sulphuric acid – ethanol 1:1:10, followed by heating for 5 min at 104 °C. Quantitative determination by absorbance measurement at 554 nm. The hRf value of absinthin was 64 and selectivity regarding matrix was given. Linearity was between 0.1 and 10 g/L. The precision was better than 13.5 % (intraday) and 15.8 % (interday). The limit of detection and quantification for absinthin was 0.05 and 0.11 g/L, respectively.

      Classification: 15a
      100 070
      Expression pattern study of important flavonoids and sapogenins in plants and in callus culture of the medicinal plant Calendula officinalis
      S. BANERJEE (Department of BIOtECHNOLOGY, KOLKATA, WEST BENGAL, INDIA)

      59th Indian Pharmaceutical congress C-323, 302,(2007). TLC of flavonoids and sapogenins from different plant parts (leaves and petals) of Calendula officinialis on silica gel with ethyl acetate - formic acid - glacial acetic acid - water 100:11:11:20, and chloroform - glacial acetic acid - methanol - water 15:8:3:2.

      Classification: 32e
      100 090
      Method development, validation and determination of study of sumatriptane succinate in bulk poder and tablet forms by RP-HPLC and HPTLC methods
      S.P. GANDHI*, C.R. SHAH, N.J. SHAH, D.R. PATEL, B.N. SUHAGIA (*Shri B.M. Shah College of Pharm. Edu. and Res. Gujrat, India)

      59th Indian Pharmaceutical congress F-9, 392, (2007). HPTLC of sumatriptan succinate in bulk and tablet formulations on silica gel with methanol - water - glacial acetic acid 40:80:1. Densitometric evaluation at 230 nm.

      Classification: 32a
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