Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      102 150
      HPTLC METHOD FOR DETERMINATION OF EZETIMIBE IN TABLETS
      S. Sonawane*, A. Shirkhedkar, S. Surana (*Dept. of Pharmaceutical Chemistry, R.C. Patel College of Pharmacy Karwad Naka, Shirpur 425405, India, atul_shirkhedkar@yahoo.com)

      Asian J. Chem. 19(6), 4925 - 4927 (2007). TLC of ezetimibe on silica gel with toluene - acetone 3:2. Quantitative determination by absorbance measurement at 233 nm. The hRf value was 52 for ezetimibe. Linearity was in the range of 300 to 2100 ng/spot. Recovery (by standard addition method) was 99-101 %.

      Classification: 32a
      103 006
      Chemometric analysis of retention data from salting-out thin-layer chromatography in relation to structural parameters and biological activity of chosen sulphonamides
      Jolanta FLIEGER*, R. SWIEBODA, M. TATARCZAK (*Department of Inorganic and Analytical Chemistry, Medical University of Lublin, 20-081 Lublin, Staszica 6, Poland)

      J. Chromatogr. B 846 (1-2), 334-340 (2007). Salting-out TLC of sulphonamides on silica gel with aqueous solutions of salts (sulphates, chlorides, nitrates, phosphates, acetates, and thiocyanates) showed that the applied salts have different effects on the retention of sulphonamides according to Hofmeister's classification (e.g. kosmotropes, chaotropes and neutral). Parameters of the linear regression analysis were compared with QSAR data of dependences between the RM values and salt concentration. Chromatographic data obtained by salting-out TLC showed not only the physico-chemical properties of the examined compounds but also information about their activity. The method was suitable for prediction and classification of sulphonamide drugs by localization of other structurally similar compounds with antagonistic activity towards sulphonamides.

      Classification: 2c
      103 045
      High-performance thin-layer chromatographic analysis of the polar lipid content of human urine and urine from BALB/c mice experimentally infected with Echinostoma caproni
      D.R. MASSA, J.D. VASTA, B. FRIED, J. SHERMA* (*Department of Chemistry, Lafayette College. Easton, PA, USA; shermaj@lafayette.edu)

      J. Planar Chromatogr. 21, 337-341 (2008). HPTLC of phospholipids (cholesterol, phosphatidylethanolamine, phosphatidylcholine, and lysophosphatidylcholine) on silica gel plates with a concentration zone (prewashed with dichloromethane - methanol 1:1) with chloroform - methanol - water 65:25:4 in a saturated twin trough chamber. Detection by spraying with aqueous copper sulfate reagent followed by heating. Quantitative determination by absorbance measurement at 370 nm. Ninhydrin spray reagent was used to confirm the presence of phosphatidylethanolamine. The limit of quantification was 250 ng/spot.

      Classification: 11c
      103 083
      (Study of the quality standard for compound Shenyi granules) (Chinese)
      R. AN (An Rui)*, S. ZHOU (Zhou Sili), L. YOU (You Lisha), X. WANG (Wang Xinhong) (*Shanghai Univ. TCM, Shanghai 201203, China)

      J. Chinese Trad. Patent Med. 30 (12), 1781-1785 (2008). TLC of Shenyi granule extracts on silica gel with 1) dichloromethane - ethyl acetate - petroleum ether (60-90 ºC) - methanol 20:14:6:1; 2) ethyl acetate - formic acid - glacial acetic acid - water 30:3:4:3; 3) toluene - ethyl acetate - formic acid 8:6:1; 4) chloroform - methanol - water 26:10:3. Detection 1) by spraying with 10 % sulfuric acid in ethanol and heating; 2) by spraying with iron(III) chloride solution; 3) by spraying with vanillin reagent. Identification by comparison with the standards glycyrrhizic acid and glycyrrhetinic acid.

      Classification: 32e
      103 105
      (Study of the quality standard for Yinao pills) (Chinese)
      W. JIANG (Jiang Weike)*, T. ZHOU (Zhou Tao), P. GUO (Guo Peinan), Z. CHEN (Chen Zaifa) (*Guiyang Coll. TCM, Guiyang, Guizhou 550002, China)

      J. Chinese Trad. Patent Med. 30 (11), 1642-1646 (2008). TLC of Yinao pill extracts on silica gel with 1) toluene - ethyl acetate 9:1; 2) benzene - ethyl acetate 3:2; 3) toluene - ethyl acetate - formic acid 28:8:1. Detection 1) by spraying with 10 % phosphomolybdic acid in ethanol and heating at 105 ºC; 2) by spraying with 10 % sulfuric acid in ethanol and heating at 105 ºC.

      Classification: 32e
      103 129
      Standardization, validation and safety evaluation of Emblica officinalis Linn
      S. PANDIT*, S. PONNUSANKAR, M. VENKATESH, A. GANTAIT, A. BANDYOPADHYAY, P. MUKHERJEE (*School of Natural Product Studies, Dept. of Pharmaceutical Tech., Jadavpur University, Kolkata, India)

      Abstract No. 9148, IHCB (2009). HPTLC of gallic acid in Emblica officinalis (an important constituent of Triphala, a popular ayurvedic formulation) on silica gel with toluene - ethyl acetate - formic acid 10:10:3. The hRf value of gallic acid was 45. Quantitative determination by absorbance measurement at 254 nm. The method was linear in the range of 150-530 ng/spot. The extract was found to contain 7.5 mg/g of gallic acid.

      Classification: 32e
      103 154
      Quantitative densitometric HPTLC analysis of purpurin in the parts of Rubia cordifolia and in pharmaceutical dosage forms
      A.K. THAKUR*, P.D. HAMRAPURKAR (*Department of Pharmaceutical Analysis, Prin. K. M. Kundanani College of Pharmacy, Jote Joy Building, Rambhau Salgaonkar Road, Cuff Parade, Mumbai 400005, Maharashtra, India; achalthakur@gmail.com)

      J. Planar Chromatogr. 22, 109-113 (2009). HPTLC of purpurin on silica gel with toluene - ethyl acetate - formic acid 98:2:1 in a twin trough chamber saturated for 20 min at 25 +/- 2 °C. Quantitative determination by absorbance measurement at 255 nm. The limit of detection and quantification was 50 and 100 ng/band, respectively.

      Classification: 32e
      104 021
      An HPTLC-AMD method for understanding the metabolic behavior of microorganisms in the presence of mixed carbon sources
      T. BERNARDI, Elena TAMBURINI* (*Department of Chemistry, University of Ferrara, Via L. Borsari 46, 44100 Ferrara, Italy; tme@unife.it)

      The case of Bifidobacterium adolescentis MB 239. J. Planar Chromatogr. 22, 321-325 (2009). HPTLC of glucose, fructose, galactose, lactose, raffinose, 1-kestose, nystose, and fructosyl-nystose on diol phase by automated multiple development with acetonitrile - acetone - water and acetonitrile - water. Preliminary isocratic developments were performed at 22-25 °C at 65-75 % relative humidity in a twin trough chamber. Detection by vaporization with 37 % hydochloric acid vapor for 30 min followed by dipping in 4-aminobenzoic acid. Quantitative determination by fluorescence measurement at 313 nm.

      Classification: 10a
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