Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      111 108
      Separation and determination of lamivudine, tenofovir disoproxil fumarate and efavirenz in tablet dosage form by thin-layer chromatographic-densitometric method
      S. MORE, S. TANDULWADKAR, A. NIKAM, A. RATHORE, L. SATHIYANARAYANAN, K. MAHADIK* (*Department of Pharmaceutical Chemistry, Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Erandwane, Pune 411038, Maharashtra, India, krmahadik@rediffmail.com)

      J. Planar Chromatogr. 26, 78-85 (2013). HPTLC of lamivudine (1), tenofovir disoproxil fumarate (2) and efavirenz (3) on silica gel with chloroform - methanol - toluene 30:4:1. Quantitative determination by absorbance measurement at 260 nm. The hRf values of (1), (2) and (3) were 20, 61 and 73, respectively. Linearity was in the range of 400-800 ng/zone for (1) and (2) and 800-1600 ng/zone for (3). Intermediate precision was below 2 %. LOD and LOQ were 180 and 300 ng/zone for (1), 150 and 210 ng/zone for (2) and 300 and 400 ng/zone for (3), respectively.

      Classification: 32a
      112 010
      Comparison of two TLC-DPPH-Image processing procedures for studying free radical scavenging activity of compounds from selected varieties of Medicago sativa
      I. KOWALSKA, L. CIESLA, T. ONISZCZUK, M. HAJNOS, W. OLESZEK, A. STOCHMAL (*Department of Inorganic Chemistry, Medical University of Lublin, 20-093 Lublin, Poland, lukecarpenter@poczta.onet.pl)

      J. Liq. Chromatogr. Relat. Technol. 36, 2387-2394 (2014). The image processing programs ImageJ and Sorbfil TLC Videodensitometer were compared to study direct antioxidant properties of compounds separated from extracts obtained from Medicago sativa. Comparable results were obtained based on built-in functions present in both programs for processing TLC videoscans.

      Classification: 3f
      112 030
      High-performance thin-layer chromatographic analysis of the neutral lipid content of urine and feces in mice experimentally infected with Schistosoma mansoni
      Meghan CICCHI, J. BOLSTRIDGE, Nevena POPOVIC, B. FRIED*, J. SHERMA (*Biology Department at Lafayette College, Easton, PA 18042, USA, friedb@lafayette.edu)

      Trends in Chromatography 8, 1-6 (2013). HPTLC of neutral lipids and a neutral lipid standard (consisting of 20 % each of cholesterol, oleic acid, triolein, methyl oleate, and cholesteryl oleate) on silica gel (HLF plates with 19 scored channels of 9 mm width) prewashed with dichloromethane - methanol 1:1 and heated for 30 min at 120 °C, with petroleum ether - diethyl ether - glacial acetic acid 80:20:1 with chamber saturation. Detection by spraying with 5 % ethanolic phosphomolybdic acid reagent and heating at 120 °C for 5 min. Neutral lipids appeared as blue zones on a yellow background. The fractions of free sterols, free fatty acids, triacylglycerols, methyl esters, and steryl esters were identified by comparison with the standard mixture. Quantification by absorption measurement at 610 nm via linear calibration (peak area).

      Classification: 11c
      112 050
      Isolation and HPTLC analysis of iridoids in Premna integrifolia, an important ingredient of Ayurvedic drug dashmool
      D. YADAV, M. GUPTA* (*Analytical Chemistry Department, Central Institute of Medicinal and Aromatic Plants, Lucknow-226015, India, guptammg@rediffmail.com)

      J. Planar Chromatogr. 26, 260-266 (2013). HPTLC of of iridoids 10-O-trans-p-coumaroylcatalpol (1), 4-hydroxy-E-globularinin (2) and premnosidic acid (3) in the stem bark of Premna integrifolia on silica gel with ethyl acetate - methanol - water - acetic acid 40:6:3:1. Detection by dipping into vanillin - sulphuric acid reagent (1 % vanillin in ethanol - sulfuric acid 19:1), followed by heating at 110 ºC for 3 min. Quantification by absorbance measurement at 510 nm. The hRf values for (1) to (3) were 52, 41 and 33, respectively. Linearity was in the range of 1-10 µg/zone for (1) to (3). LOD and LOQ were 198 and 663 ng/zone for (1), 312 and 1040 ng/zone for (2) and 200 and 666 ng/zone for (3), respectively. Average recoveries for (1) to (3) were found to be 97.3 %, 98.3 % and 97.6 %, respectively. Intermediate/interday/intra-day precision was below 2 % (n=9).

      Classification: 15a
      112 070
      Development and validation of a TLC method for the analysis of synthetic food-stuff dyes
      J. VLAJKOVIC, F. ANDRIC, P. RISTIVOJEVIC, A. RADOICI, Z. TESIC, D. OPSENICA* (*Faculty of Chemistry, University of Belgrade, P. O. Box 51, 11158, Belgrade, Serbia, dusankam@chem.bg.ac.rsk)

      J. Liq. Chromatogr. Relat. Technol. 36, 2476-2488 (2013). HPTLC of synthetic colorants tartrazine (1), quinoline yellow (2), sunset yellow FCF (3), azorubine (4), amaranth (5), ponceau 4R (6), allura Red AC (7), patent blue V (8), indigo carmine (9), and brilliant blue FCF (10) on RP-18 with 0.5 M ammonium sulfate in 30 % of ethanol - water solution. Quantitative determination by absorbance measurement at 450, 500 and 625 nm. The hRf values were in the range of 17 and 64. Linearity was in the range of 20-180 ng/zone for (1) to (8) and 35-300 ng/zone for (9) and (10). LOD and LOQ were 2 and 3 ng/zone, respectively. Recovery (by standard addition) was in the range of 81-108 %. Intermediate intra- and inter-day precision was below 5 % (n=3).

      Classification: 30a
      112 108
      Validated specific densitometric method for simultaneous estimation of telmisartan and atorvastatin in presence of degradation products formed under ICH-recommended stress conditions
      R. THANGAVELU*, S. MAKAPOTHULA, N. GOWDA (*Analytical Research Laboratory, Department of Pharmaceutical Analysis, PES College of Pharmacy, Hanumanthanagar, Rajiv Gandhi University of Health Sciences, Bengaluru-560050, Karnataka, India, nraj_msubaroda@yahoo.co.in)

      J. Planar Chromatogr. 26, 445-451 (2013). HPTLC of telmisartan (1) and atorvastatin (2) on silica gel with methanol - chloroform 1:7. Quantitative determination by absorbance measurement at 280 nm. The hRf values for (1) and (2) were 64 and 27, respectively. Linearity was between 1.2-7.2 µg/zone for (1) and 0.4-2.4 µg/zone for (2). LOD and LOQ were 3 and 8 ng/zone. Recoveries (by standard addition) were 98-101 % for (1) and 99-101 % for (2). Intermediate intra- and inter-day precision was below 2 %. Comparable results were obtained with HPLC and UV methods.

      Classification: 32a
      113 020
      Evaluation of successive fractions for optimum quantification of bergenin and gallic acid in three industrially important Bergenia species by high-performance thin-layer chromatography
      N. SRIVASTAVA, S. VERMA, S. PRAGYADEEP, S. SRIVASTAVA, A. RAWAT* (*Pharmacognosy and Ethnopharmacology Division, CSIR, National Botanical
      Research Institute, Lucknow 226001, India, pharmacognosy1@rediffmail.com)

      J. Planar Chromatogr. 27, 69-71 (2014). HPTLC of bergenin (1) and gallic acid (2) in the rhizome of three Bergenia species, B. ciliata, B. stracheyi, and B. ligulata on silica gel with toluene - ethyl acetate - formic acid 7:11:2. Quantitative determination by absorbance measurement at 314 nm. The hRF values for (1) and (2) were 25 ad 59, respectively.

      Classification: 7, 32e
      113 039
      Screening and determination of sibutramine in adulterated herbal slimming supplements by
      HPTLC-UV densitometry
      Caroline MATHON, Anita ANKLI, E. REICH, S. BIERI, P. CHRISTEN* (*School of Pharmaceutical Sciences, University of Geneva, University of Lausanne, Quai Ernest-Ansermet 30, 1211 Geneva 4, Switzerland, Philippe.Christen@unige.ch)

      Food Addit. Contam. 31, 15-20 (2014). HPTLC of sibutramine in food supplements and soluble beverages on silica gel with toluene - methanol 9:1. Quantitative determination by absorbance measurement at 225 nm. The hRF value for sibutramine was 53. Linearity was in the range of 78-3020 ng/zone. The method was sensitive to detect 0.3 mg of sibutramine per capsule of food supplement and showed comparable results with those obtained with HPTLC-UV and HPLC-MS.

      Classification: 17c
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