Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
- Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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J. Planar Chromatogr. 22, 43-47 (2009). HPTLC of alpha-solanine and alpha-chaconine on silica gel with dichloromethane - methanol - 2.5 % ammonia 175: 75:11 in a horizontal chamber saturated for 15 min. After drying and heating at 90 °C for 25 min detection by dipping twice in modified Carr-Price reagent (antimony(III) chloride in acetic acid - dichloromethane), followed by heating at 110 °C for 3 min. Quantitative determination by absorbance measurement at 560 nm. Linearity was between 30 and 700 ng. The limit of detection was 5-20 ng/zone depending on the sample matrix, the limit of quantification was 30 ng/zone. The ratio of alpha-chaconine and alpha-solanine was between 4:1 to 2:1 for all analyzed samples.
J. Planar Chromatogr. 22, 83-88 (2009). TLC of isoniazid, pyrazinamide, ethambutol, and aminosalicylic acid on RP-18 in a horizontal chamber at 20 °C with acetonitrile - water 3:7. The mobile phase was modified by adding copper(II) chloride to the mixture at a constant concentration of 0.05 M. Detection under UV light at 254 nm. Quantitative determination by absorbance measurement in the range 200 - 700 nm with a TLC scanner equipped with a diode-array detector.
J. Planar Chromatogr. 21, 277-282 (2008). TLC of clotrimazole and metronidazole on silica gel in a twin trough chamber saturated for 10 min with toluene - ethyl acetate - methanol - acetic acid 55:2:6:1. Quantitative determination by absorbance measurement at 220 nm.
Indian J. Pharma. Sci. 70(6), 831-834 (2008). HPTLC of sumatriptan on silica gel (pre-washed) with methanol - water - glacial acetic acid 40:80:1 with chamber saturation for 10 min. Quantitative determination by absorbance measurement at 230 nm. The hRf value was 64. The method was linear in the range of 200-800 ng/spot.
Anal. Chem. 80, 6821-6823 (2008). HPTLC of Cr3+ and Cr 6+ on silica gel in a saturated chamber with distilled deionized water and Triton-X-100 in concentrations between 0.001 and 0.1%, which is around the critical micelle concentration. Separation was achieved in seconds over 1 cm. Laser ablation was used to volatilize the chromium species directly from the chromatographic material prior to ICP-MS detection. The reliability of calibration was satisfying with precisions between 3 - 30 % and detection limits in the low ng-range. Silicium, which is present in the silica gel plate, was discussed as suitable internal standard.
60th Indian Pharmaceutical Congress PA-217 (2008). HPTLC of oleanolic acid in total methanolic extract of fruits of Randia dumetorum lam. on silica gel with toluene - ethyl acetate - acetic acid 70:30:1 in a twin trough chamber saturated for 10 min. Detection by treatment with 10 % sulphuric acid in methanol, followed by heating at 110 °C and immediate densitometric evaluation. Quantitative determination by absorbance measurement at 540 nm. The method was linear in the range of 50-500 ng/spot. Recovery was in the range of 99.4-100.8 %.
Food Addit. Contam. 24, 351-359 (2007). Inter-laboratory validation of the analytical method (published in the SIMBAG-FEED report 4.6) based on TLC coupled to bio-autography for the detection of tylosin, spiramycin and virginiamycin in feeding-stuffs for poultry, pig, cattle and calf. The detection limit of spiramycin was 2 mg/kg and the method has a target concentration of 1 mg/kg for tylosin and virginiamycin. The method showed high specificity and offers the possibility for screening before LC/MS analysis.
60th Indian Pharmaceutical Congress PA-226 (2008). HPTLC of olmesartan medoxomil (an angiotensin-II antagonist) on silica gel with toluene - acetonitrile - methanol - ethyl acetate - acetic acid (mobile phase ratio not specified by the authors). The hRf value was 56. Quantitative determination by absorbance measurement at 262 nm. The linearity was between 300-800 ng/spot. The method was suitable for separation of olmesartan medoxomil from degradation products obtained by forced stress conditions (acid, alkali, peroxide, light, heat).