Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      125 003
      A simple, rapid and sensitive high-performance thin-layer chromatographic method for the simultaneous estimation of berberine and 5-fluorouracil in rabbit plasma
      P. TAMANE*, R. PAI, V. POKHARKAR (*Department of Drug Regulatory Affairs, Bharati Vidyapeeth (Deemed to be) University, Poona College of Pharmacy, Erandwane, Pune, Maharashtra 411038, India, varsha.pokharkar@bharatividyapeeth.edu)

      J. Planar Chromatogr. 33, 169-177 (2020). HPTLC of berberine (1) and 5-fluorouracil (2) in rabbit plasma on silica gel with toluene - methanol - ethyl acetate - formic acid 6:2:6:1. Quantitative determination by absorbance measurement at 266 nm. The hRF values for (1) and (2) were 28 and 57, respectively. Linearity was between 20 and 300 ng/zone for both (1) and (2). Intermediate precisions were below 7 % (n=3). The LOQ was 29 ng/zone for (1) and 26 ng/zone for (2), respectively. Average recovery was 86.5 % for (1) and 87.2 % for (2).

      Classification: 32c
      125 055
      Thin-layer chromatographic enantioseparation of atenolol and propranolol using (S)-naproxen as chiral selector: direct and indirect approaches
      V. VASHISTHA, R. BHUSHAN* (*Department of Chemistry, GLA University, Mathura, Uttar Pradesh 281406, India, rbushfcy54@gmail.com)

      J. Planar Chromatogr. 33, 101-107 (2020). HPTLC of (RS)-atenolol and (RS)-propranolol on silica gel  impregnated with 50 mM (S)-naproxen as chiral selector with acetonitrile - dichloromethane - water 6:2:1 pH = 5 for (RS)-atenolol and 7:3:1 pH = 5 for (RS)-propanolol. Detection by exposure to iodine vapor. The LOD was 1.2 and 1.6 µg/mL for (1) and (2), respectively. The chiral selector allowed the separation of atenolol and propranolol with a resolution of 2.4.

      Classification: 38
      125 054
      Stability-indicating HPTLC method development for determination of arterolane maleate and piperaquine phosphate in combined dosage form
      S. GAILKWAD, A. BANSODE, N. PATADE, S. TATHE (*Department of Pharmaceutical Chemistry, Sinhgad Institute of Pharmacy, Narhe, Pune, Maharashtra 411041, India, shubhangi_pharma@rediffmail.com)

      J. Planar Chromatogr. 33, 131-139 (2020). HPTLC of arterolane maleate (1) and piperaquine phosphate (2) on silica gel with isopropyl alcohol - n-butanol - methanol - triethylamine 15:30:5:1. Quantitative determination by absorbance measurement at 232 nm. The hRF values for (1) and (2) were 64 and 18, respectively. Linearity was 150-900 ng/zone for (1) and 750-4500 ng/zone for (2). Intermediate precisions were below 2 % (n=6). The LOD and LOQ were 6 and 18 mg/zone for (1) and 23 and 70 ng/zone for (2), respectively. Mean recovery rate was 98.9 and 103.9 % for (2).

      Classification: 32a
      125 053
      High-performance thin-layer chromatographic determination of trigonelline content in various extracts and different varieties of some commercial coffees available in the Saudi Arabian market
      A. FOUDAH*, P. ALAM, M. ABDEL-KADER, F. SHAKEEL, S. ALQASOUMI, A. SALKINI, H. YUSUFOGLU (*Department of Pharmacognosy, College of Pharmacy, Prince Sattam bin Abdulaziz University, Al-Kharj, Saudi Arabia, a.foudah@psau.edu.sa)

      J. Planar Chromatogr. 33, 43-50 (2020). HPTLC of trigonelline in coffee samples with ethyl acetate - methanol - water - formic acid 54:23:15:8. Quantitative determination by absorbance measurement at 267 nm. The hRF value for trigonelline was 24. Linearity was between 100 and 700 ng/zone. Intermediate precisions were below 2 % (n=3). The LOD and LOQ were 33 and 110 ng/zone. Recovery rate was between 97.6 and 99.4 %.

      Classification: 22
      125 052
      A new thin-layer chromatography–direct bioautography assay for the qualitative and quantitative determination of peroxidase inhibitors in plant extracts
      R. DARWISH, E. SHAWKY, H. HAMMODA, F. HARRAZ (*Department of Pharmacognosy, Faculty of Pharmacy, Alkhartoom square, Alexandria University, Alexandria 21521, Egypt, eman.m.shawky@alexu.edu.eg)

      J. Planar Chromatogr. 33, 79-87 (2020). HPTLC of quercetin in the aerial parts of Juniperus communis, J. horizontalis and J. chinensis on silica gel with ethyl acetate - methanol - water - acetic acid 900:80:40:7. Assessment of peroxidase inhibition activity by dipping into peroxidase enzyme solution (10 mg/mL solution of peroxidase in cold phosphate buffer (pH 7), followed by dilution with 50 mL of phosphate buffer, pH 7) for 3 s, followed by heating at 35 ºC for 2 min, dipping into a hydrogen peroxide solution and finally dipping into a benzidine solution (4 g in 700 mL methanol). Linearity was between 0.85 and 9 µg/zone for quercetin. Intermediate precisions were below 3 % (n=3). The LOD and LOQ were 280 and 850 ng/zone. Recovery was between 96.6 and 99.7 %.

       

      Classification: 8a
      125 051
      Simultaneous identification of rutin, chlorogenic acid and gallic acid in Moringa oleifera by densitometric high-performance thin-layer chromatography method
      P. ALAM*, P. ALAM, M. SHARAF-ELDIN, M. ALQAMI (*Department of Biology, Sara Alghonaim Research Chair (SRC), College of Science and Humanities, Prince Sattam bin Abdulaziz University (PSAU), Alkharj 11942, Saudi Arabia, alamprez@gmail.com)

      J. Planar Chromatogr. 33, 27-32 (2020). HPTLC of rutin (1), chlorogenic acid (2) and gallic acid (3) in the seeds of Moringa oleifera on silica gel with ethyl acetate - acetone - water - formic acid 6:3:2:2. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (3) were 51, 72 and 83, respectively. Linearity was between 1000 and 7000 ng/zone for (1), 100 and 700 ng/zone for both (2) and (3). Intermediate precisions were below 1 % (n=6). The LOD and LOQ were 5 and 17 ng/mL for (1), 7 and 22 ng/mL for (2) and 7 and 20 ng/mL for (3), respectively. Recovery rate was between 98.1 and 99.5 % for (1), 98.8 and 99.5 % for (2) and 97.6 and 98.6 % for (3).

      Classification: 8a
      125 050
      The use of thin-layer chromatography in the assessment of the quality of lutein-containing dietary supplements
      P. MIGAS*, N. STEMPKA, M. BARANOWSKA (*Department of Pharmacognosy with Medicinal Plants Garden, Medical University of Gdansk, Gen. J. Haller Str. 107, 80-416 Gdansk, Poland, piotr.migas@gumed.edu.pl)

      J. Planar Chromatogr. 33, 11-18 (2020). HPTLC of lutein in dietary supplements on silica gel with n-heptane – ethyl acetate 9:1. The part of the TLC chromatogram containing the zone visible in day light was cut off, followed by developing in the opposite direction with n-heptane – acetone – ethyl acetate 11:5:4. Quantitative determination by absorbance measurement at 450 nm. Linearity was between 90 and 500 ng/zone for lutein. Intermediate precisions were below 2 % (n=9). The LOD and LOQ were 50 and 90 ng/zone, respectively. Recovery rate was between 87 and 102 %.

      Classification: 30b
      125 047
      Comparative study on the determination of ethyl p-methoxycinnamate in Kaempferia galanga rhizome by HPTLCS and HPLC
      K. ZHANG (Zhang Kui), W. WU (Wu Wenxia), S. TIAN (Tian Shuge)* (*College of TCM, Xinjiang Medical University, Urumqi 830011, Xinjiang, China, tianshuge@hotmail.com)

      J. Planar Chromatogr. 33, 51-57 (2020). HPTLCS (high-performance thin-layer chromatography scanning) of ethyl p-methoxycinnamate in the rhizome of Kaempferia galanga on silica gel with hexane - ethyl acetate 18:1. Quantitative determination by absorbance measurement at 309 nm. The hRF value for ethyl p-methoxycinnamate was 29. Linearity was between 2 and 6 ng/zone. Intermediate precisions were below 2.4 % (n=3). Mean recovery rate was 100.1 %. Results were compared with a validated HPLC method and the HPTLCS method was more environmetnally friendly..

      Classification: 32a
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