Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      122 059
      Development and validation of a high-performance thin-layer chromatographic method for the simultaneous determination of levamisole and cocaine in seized cocaine sample
      R. SHARMA*, J. KUMAR (*Chemistry and Toxicology Division, Forensic Science
      Laboratory, Rohini, New Delhi, India, rahulsharma02@gmail.com)

      J. Planar Chromatogr. 31, 383-388 (2018). HPTLC of cocaine hydrochloride (1) and levamisole hydrochloride (2) on silica gel with cyclohexane – toluene – diphenylamine 75:15:10. Quantitative determination by absorbance measurement at 230 nm. The hRF values for (1) and (2) were 24 and 48, respectively. Linearity was between 200 and 2400 ng/zone for (1) and 100 and 1200 ng/zone for (2). LOD and LOQ were 14 and 42 ng/zone for (1) and 6 and 19 ng/zone for (2), respectively. The intermediate precision was <2 % (n=6). Average recovery was 99.8 % for (1) and 99.9 % for (2).

      Classification: 22, 23e, 32a
      122 081
      Optimization of ultrasound-assisted emulsification microextraction by experimental design for determination of over-the-counter drugs by thin-layer chromatography–image-processing method
      R. JAIN (Forensic Toxicology Division, Central Forensic Science Laboratory,
      Directorate of Forensic Science Services, Ministry of Home Affairs, 16, Lachit
      Borphukan Path, Tetelia, Gotanagar, Guwahati, 781033, India, rajeev.jain-as@gov.in)

      J. Planar Chromatogr. 31, 265-271 (2018). HPTLC of aspirin (1), paracetamol (2), and caffeine (3) in saliva, after ultrasound-assisted emulsification microextraction, with chloroform on silica gel with ethyl acetate - acetic acid 19:1. Detection under UV light at 254 nm. Quantitative determination using ImageJ software. The hRF values for (1) to (3) were 90, 80 and 50, respectively. Linearity ranged between 4 and 200 μg/zone for (1) to (3). LOD and LOQ were 12 and 38 μg/zone for (1), 8 and 26 μg/zone for (2), and 7 and 23 μg/zone for (3), respectively. The intermediate precision was <10 % (n=3). Recovery was in the range of 89-94 % in saliva for (1) to (3).

      Classification: 32c
      55 070
      Amino acids analysis in series of samples by OPLC
      S. PAPP, E. TOTH, B. POLYAK

      Proc. Intern. Symposium on TLC with special Emphasis on OPLC, Szeged, 67, (1984). OPLC (OPTLC) of amino acids on silica with 1) butanol - acetic acid - water 4:1:1, 2) phenol -1 % SDS - isobutanol - propanol - butanol - acetic acid 70:28:2:2:2:1.7. Detection with ninhydrin + Cu or Cd acetate reagent. Detection with videodensitometer, coefficient of variation 6 %.

      Classification: 18a
      55 099
      Improvement of chemical analysis of antibiotics
      H. OKA, M. SUZUKI

      VII. Comparison of analytical methods for determination of impurities in tetracycline pharmaceutical preparations. J. Chromatogr. 314, 303-311 (1984). HPTLC of various tetracyclines on silica with acetone - 5 % aq. sol. of Na2 EDTA 10:1 and RP-TLC on C18-plates with methanol - acetonitrile - 0.5 M oxalic acid (aq. pH 2.0) 1:1:4 or 1:1:2. Detection by UV 366 nm or with 0.5 % Fast Violet B aq. solution and pyridine. Quantification by scanning at the dual-wavelength mode at 366/600 nm for 4-epitetracycline and chlortetracycline and at 425/650 nm for anhydrotetracycline and 4-epianhydrotetracycline. RP-TLC-densitometry appears to be a precise method for the determination of tetracyclines.

      Classification: 28a
      55 139
      Fluorodensitometrische Bestimmung von zytostatisch wirksamen Michael-Addukten alpha, beta-ungesättigter Aldehyde in biologischem Material
      H. TILLIAN, G. GUEBITZ, W. KORSATKO, R. WINTERSTIGER

      (Fluorodensitometric determination of Michaeladducts of (alpha, beta unsaturated aldehydes in biological material.) Arzneim. Forsch. 35, 552-554 (1984). TLC of dansylhydrazine derivatives of Michael adducts of alpha, beta-unsaturated aldehydes on silica with isopropanol - methyl acetate - methanol - NH3 50:5:30:20, resp. chloroform - petrol ether - acetone 7:1:2. Detection after drying and dipping into 20 % polyethyleneglycol 400 in chloroform by UV. Quantification by fluorescence scanning. Detection limit 10 ng.

      Classification: 32c
      56 121
      Simple, rapid clean up method for analysis of aflatoxins and comparison with various methods
      H. KAMIMURA, M. NISHIJIMA, K. YASUDA, H. USHIYAMA, S. TABATA et al.

      J.A.O.A.C. 68, 458-461 (1985). HPTLC separation of aflatoxins B1, B2, G1, G2, M1 on silica with chloroform - acetone 9:1 and/or ether - methanol - water 94:4.5:1.5 or chloroform - isopropanol - acetone 85:5:10. Detection by UV. Densitometry. Recoveries in good agreement with A.O.A.C. CB method.

      Classification: 28b
      57 057
      Chinese Bulletin of Pharm
      S. ZHAO, Y. ZHANG

      ( Chinese) - (TLC-densitometry of isoflavones in pueraria lobata.) TLC of daidzein, daidzin, puerarin and daidzein 4,7-diglucoside in the root of P. lobata and in tablets on silica with toluene - methanol -10 % formic acid 7:3:00.2, or ethyl acetate - methanol -50 % formic acid 8:2:0.2. Quantification by densitometry. Relative standard deviations: 1.51 % for puerarin, 1.61 % for daidzein.

      Classification: 8a, 14
      57 103
      Chinese J
      Y. SUN, F. LI, L. WANG, H. CAI, C. GAO, A. ZHANG, L. ZHANG

      of Chromatogr. (Se Pu) 2, 169-171 (1985). (Chinese). (Determination of the injection preparation of menispermum dahuricum DC by TLC and HPLC.) TLC of dauricine and dauricinoline on silica with chloroform - ethanol - NH3 80:1:5. Quantification by densitometry. Also HPLC.

      Classification: 22, 32c
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