Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

Page
      109 046
      Validated densitometric method for the quantification of lamotrigine in dosage form
      M.C. SHARMA*, S. SHARMA (*School of Pharmacy, Devi Ahilya Vishwavidyalaya, Indore (MP) 452001, India)

      International Journal of PharmTech Research 3(2), 1174-1178 (2011). TLC of lamotrigine on silica gel with ethyl acetate - chloroform - water 18:6:5. The hRf value was 40. Quantitative determination at 240 nm. The linearity was in the range of 98-590 ng/band with an average recovery of 100.2 %. LOD and LOQ were 44 and 122 ng/zone.

      Classification: 17a
      109 068
      Application of HPLC-DAD and TLC-DAD after SPE to the quantitative analysis of pesticides in water samples
      T. TUZIMSKI*, J. SOBCZYN (*Faculty of Pharmacy, Department of Physical Chemistry, Chair of Chemistry, Medical University of Lublin, 4 Staszica Street, 20-081 Lublin, Poland, tomasz.tuzimski@umlub.pl)

      J. Liq. Chromatogr. Relat. Technol. 32, 1241-1258 (2009). HPTLC of 11 pesticides in water samples on silica gel with ethyl acetate - n-heptane 2:8, 3:7, 2:3 or 7:30. Quantitative determination by absorbance measurement between 200 to 600 nm with average optical resolution better than 2.0 nm. Linearity was between 0.1 and 17 µg/zone for all pesticides. The LOD was between 40-650 ng/zone. Results were comparable with a HPLC method.

      Classification: 29, 37c
      109 088
      Development and validation of an HPTLC method for the analysis of oleanolic acid from the roots of Helicteres isora Linn
      P.A. HARDE*, D.R. SHAH, B.N. SUHAGIA, M.B. SHAH (*Pithawalla Institute of Pharmaceutical Science and Research, Dumas Road, Surat-395007, Gujarat, India; pinalharde@gmail.com)

      J. Planar Chromatogr. 24, 503-506 (2011). HPTLC of oleanolic acid in extracts of dried roots on silica gel with toluene - ethyl acetate - glacial acetic acid 70:30:1 in a saturated twin-trough chamber. Detection by spraying with anisaldehyde-sulfuric acid reagent and heating in an oven at 110 °C for 5 min. Quantification was performed by immediate densitometric absorbance measurement at 529 nm. The average recovery was 98.9 %. LOD and LOQ were 10 and 30 ng/zone, respectively. The hRf value was 58. Linearity was between 100 and 1000 ng/zone. Precision (%RSD) was 1.4 %.

      Classification: 32e
      109 105
      Simultaneous determination of imipramine hydrochloride and chlordiazepoxide in pharmaceutical preparations by spectrophotometric, RP-HPLC, and HPTLC methods
      S.K. PATEL*, N.J. PATEL (*Shree S. K. Patel College of Pharmaceutical Education and Research, Department of Pharmaceutical Chemistry, Ganpat Vidyanagar, Kherva, Mehsana-382711, Gujarat, India; skpatel_2@rediffmail.com)

      J. AOAC Int. 93, 904-910 (2010). HPTLC of imipramine hydrochloride and chlordiazepoxide on silica gel with carbon tetrachloride - acetone - triethylamine (pH 8.3) 20:10:1 in a twin-trough chamber after saturation for 30 min at 25 °C. Quantitative determination by densitometry in absorbance mode at 240 nm. Linearity was between 50-600 and 20-240 ng/zone with mean accuracies of 99.5 and 100.6 % for imiprazine hydrochloride and chlordiazepoxide, respectively. The hRf value of imipramine was 73 and of chlordiazepoxide 32. The %RSD values of intra-day and inter-day precision were between 0.7-1.4 % and 0.4-1.2 % for imipramine and 0.8-1.7 % and 0.7-1.3 % for chlordiazepoxide.

      Classification: 32a
      109 126
      (Study of the quality standard for Biyuan Pills) (Chinese)
      Z. XIONG (Xiong Ze)*, H. XU (Xu Hongxia), W. SHAO (Shao Wei), B. HU (Hu Bin), M. CHOU (Chou Min) (*Coll. of Chem. & Life Sci., China Three Gorges Univ., Yichang 443002, China; 2 Minkang Pharm. Co., Ltd., Yichang 443002, China)

      J. of China Three Gorges Univ. Natural Sciences 33 (4), 92-95 (2011). TLC of extracts of Biyuan Pills on silica gel 1) for Magnolia liliiflora Desr. with dichloromethane - ethyl acetate 9:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 90 °C until the zones were detected; 2) for Xanthium sibiricum Patr., with chloroform - ethyl acetate - methanol - water - formic acid 3:10:2:2:2, detection by exposure to iodine vapor until the zones were detected; 3) for Lonicera japonica and Chrysanthemum indici flos, with toluene - ethyl acetate - formic acid - glacial acetic acid - water 1:15:1:1:2, detection under UV 365 nm.

      Classification: 32e
      110 033
      HPTLC quantification and antimicrobial activity of ursolic acid from Diospyros melanoxylon
      K. KUMAR, B. DASH, R. SINGH* (*Department of Chemistry, North Orissa University, Sriramchandra Vihar, Baripada, Mayurbhanja-757003, Orissa, India, rajeshks2001@yahoo.com)

      J. Planar Chromatogr. 25, 320-325 (2012). HPTLC of ursolic acid in the leaves of Diospyros melanoxylon on silica gel with chloroform - methanol 19:1. Detection by dipping in 5 % methanolic sulphuric acid reagent and heating at 105 °C for 3 min. Quantitative determination by absorbance measurement at 540 nm. Linearity was in the range of 50-450 ng/zone for ursolic acid. Limits of detection and quantification were found to be 20 and 40 ng/zone. Recovery (by standard addition) was 97.5 %.

      Classification: 11a
      110 060
      Application of high-performance thin-layer chromatography for determination of nicotine in different brands of cigarettes
      J. BADR*, F. BAMANE, N. EL-SHAER (*Department of Pharmacognosy, Faculty of Pharmacy, Suez Canal University, Ismailia 41522, Egypt, jihanbadr2010@hotmail.com)

      J. Liq. Chromatogr. Relat. Technol. 35, 1213-1221 (2012). HPTLC of nicotine in cigarettes on silica gel with n-hexane - methylene chloride - methanol 4:16:3. Quantitative determination by absorbance measurement at 254 nm. Linearity was in the range of 0.1-1 mg/mL. Precision was estimated with an %RSD below 2.0. Limits of detection and quantification were 0.008 mg/mL and 0.02 mg/mL, respectively. The method provides acceptable intra-day and inter-day precision for nicotine. Recovery was between 97.5 and 98.4 %, respectively.

      Classification: 32d
      110 099
      Development and validation of reverse phase high-performance liquid chromatographic and high-performance thin-layer chromatographic methods for simultaneous estimation of melitracen hydrochloride and flupentixol hydrochloride in bulk and combined dosage f
      R. LIMGAVKAR*, P. TRIVEDI, A. PATEL (*Institute of Pharmaceutical Education and Research, Sector-23, Gh-6, Gandhinagar 382023, Gujarat, India, ratnalimgavkar@gmail.com)

      J. Liq. Chromatogr. Relat. Technol. 35, 2753-2764 (2012). HPTLC of melitracen hydrochloride (1) and flupentixol hydrochloride (2) on silica gel with methanol - chloroform - toluene 2:9:9 + 1 drop ammonia. Quantitative determination by absorbance measurement at 291 nm. The hRf value of compounds (1) and (2) were 53 and 34 and selectivity regarding matrix was given. Linearity was in the range of 1600-6400 ng/band and 80-320 ng/band for (1) and (2), respectively. Limit of detection was found to be 27 ng/band and 5 ng/band for (1) and (2), respectively. Limit of quantification was found to be 82 ng/band and 14 ng/band for (1) and (2), respectively. The intermediate/inter-day/intra-day precision was below 0.2 % for (1) and 1.1 % for (2) (n=3). Recovery (by standard addition) was between 99.1 and 101.8 % for both (1) and (2). The method showed comparable results with HPLC.

      Classification: 32a
Page