Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      110 070
      Development and validation of an HPTLC method for simultaneous estimation of thiocolchicoside and aceclofenac in combined dosage form
      S. DEVKAR, Y. BADHE, S. JAGTAP, M. HEGDE* (*Interactive Research School for Health Affairs, Bharati Vidyapeeth Deemed University, Medical College Campus, Pune-411043, India, mahabaleshwarh@yahoo.com)

      J. Planar Chromatogr. 25, 290-294 (2012). HPTLC of withaferine A (1), 1,2 deoxy-withastramonolide (2), withanolide A (3), and withanolide B (4) in Withania somnifera on silica gel with dichloromethane - toluene - methanol - acetone - diethyl ether 15:15:6:2:2. Quantitative determination by absorbance measurement at 235 nm. The hRf values of (1) to (4) were found to be 58, 61, 68 and 79, respectively. Linearity was in the range of 200-1200 ng/band. Average recoveries were 98, 99.5, 98 and 99 % for compounds (1) to (4), respectively.

      Classification: 32e
      110 110
      High-performance thin-layer chromatographic determination of nifedipine in human serum after liquid-liquid extraction
      S. MENNICKENT*, J. CONTRERAS, B. SCHULZ, Marta DE DIEGO (*Departamento de Farmacia, Facultad de Farmacia, Universidad de Concepción, P.O. Box 237, Concepción, Chile, smennick@udec.cl)

      Quim. Nova. 35, 411-415 (2012). HPTLC of nifedipine in human serum on silica gel with chloroform - ethyl acetate - cyclohexane 19:2:2. Quantitative determination by absorbance measurement at 238 nm. The hRf of nifedipine was 31. Linearity was in the range of 0.02-0.25 ng/µL. Limits of detection and quantification were 0.7 and 0.9 ng/band, respectively. Intraday precision was in the range of 0.6-3.6 % (n=3) and inter-day precision was in the range of 1.2-3.6 % (n=9). Recovery was between 93 and 102 %.

      Classification: 32f
      110 130
      Development and validation of a stability-indicating HPTLC method for the determination of mirtazapine as bulk drug and in pharmaceutical formulation
      L. POTALE, A. KHODKE, S. PATOLE, M. DAMLE* (*Department of Pharmaceutical Chemistry, AISSMS College of Pharmacy, Kennedy Road, Near RTO, Pune 411001, Maharashtra, India, mcdamle@rediffmail.com)

      J. Planar Chromatogr. 25, 72-76 (2012). HPTLC of mirtazapine on silica gel with methanol - chloroform 9:1. Quantitative determination by absorbance measurement at 294 nm. The hRf of mirtazapine was 56. Linearity was in the range of 400-2000 ng/band. The intermediate/interday/intra-day precision was below 2 %.

      Classification: 32a
      110 179
      Enantioresolution of some beta-blockers and a beta-2-agonist using ligand exchange TLC
      R. BHUSHAN, J. MARTENS*, C. AGARWAL, S. DIXIT (*Institute of Pure and Applied Chemistry, CvO Universitaet Oldenburg, 26129 Oldenburg i. O./Germany, juergen.martens@uni-oldenburg.de)

      J. Planar Chromatogr. 25, 463-467 (2012). HPTLC of the enantiomers of the beta-blockers (bisoprolol, metoprolol, and propranolol) and a beta-2-agonist (salbutamol) on silica gel impregnated with Cu(II) complexes of L-threonine, L-serine, and L-tartaric acid, with different mobile phases. Limits of detection were within the range 0.19-0.26 µg for enantiomers of the selected compounds. L-Ser proved to be a very good ligand for exchange and successful enantio-resolution using common mobile phases.

      Classification: 38
      111 037
      Rapid test for content uniformity of coenzyme Q10 in soft gel capsules by HPTLC
      Anita ANKLI, D. HANDLOSER, Valeria WIDMER, E. REICH*, E. CENIVIVA (*CAMAG Laboratory, Sonnenmattstr. 11, 4132 Muttenz, Switzerland, lab@camag.com)

      CBS 107, 5-7 (2011). HPTLC of coenzyme Q10 in toluene extracts of soft gel capsules on silica gel (pre-washed by development from both sides with methanol) with toluene in the horizontal developing chamber from both sides. Detection under UV 254 nm. The hRf value of coenzyme Q10 is 20. Quantitative absorption measurement at 282 nm, evaluation via peak height. Linearity was in the range of 20-50 ng/band. Polynomial calibration ranged 20-150 ng/band. The parallel analysis of 60 samples (10 samples each from 6 batches) and 12 standards required only 86 min. The test for content uniformity was performed with 10 samples according to the European Pharmacopoeia and the USP 34 and the requirements were met.

      Classification: 20
      111 069
      Stability-indicating HPTLC method for simultaneous estimation of famotidine, paracetamol, and ibuprofen in combined tablet dosage forms
      N. DUBEY*, D. KUMAR, S. JADHAWANI (*College of Pharmacy, IPS Academy, Indore 452015 Madhya Pradesh, India, nitindubeympharm@yahoo.com)

      J. Planar Chromatogr. 25, 162-167 (2012). HPTLC of famotidine (1), paracetamol (2), and ibuprofen (3) in combined dosage forms on silica gel with chloroform - methanol - ethyl acetate - acetic acid 215:161:591:32. Quantitative determination by absorbance measurement at 256 nm. The hRf values of compounds (1) to (3) were 21, 80 and 89, respectively. Linearity was in the range of 160-960 ng/zone for (1), 400-2400 ng/zone for (2) and 600-3600 ng/zone for (3).

      Classification: 32a
      111 117
      Quantification of protodioscin and prototribestin in fruits of Tribulus terrestris L
      A. RAWAT, A. SRIVASTAVA, S. SHANKAR, S. SRIVASTAVA* (*National Botanical Research Institute, Rana Pratap Marg, Post Box No. 436, Lucknow-226 001, UP, India, sharad_ks2003@yahoo.com)

      collected from different phyto-geographical zones of India. J. Liq. Chromatogr. Relat. Technol. 36, 1810-1821 (2013). HPTLC of protodioscin (1) and prototribestin (2) in fruits of Tribulus terrestris on silica gel with n-butanol - glacial acetic acid - water 40:3:10. Quantitative determination by absorbance measurement at 366 nm. The hRf values of (1) and (2) were 41 and 39, respectively. Linearity was in the range of 100-1000 ng/zone for both (1) and (2). LOD and LOQ were 40 and 100 ng/zone for (1) and 35 and 100 ng/zone for (2). Intermediate precision was below 1.0 %. Recovery ranged 98.0-103.0 % for (1) and 99.1-101.9 % for (2).

      Classification: 32e
      112 015
      Combination of high-performance thin-layer chromatography with a specific bioassay – a tool for effect-directed analysis
      D. SPIRA*, G. REIFFERSCHEID, S. BUCHINGER (*Federal Institute of Hydrology, Am Mainzer Tor 1, 56068 Koblenz, Germany, spira@bafg.de)

      J. Planar Chromatogr. 26, 395-401 (2013). HPTLC of 17alpha-ethinylestradiol (1), 17beta-estradiol (2) and estrone (3) on silica gel with chloroform - acetone - petroleum 11:4:5. The method was combined with the Yeast Estrogen Screen for the detection of estrogenic effects in sediment extracts of a river. Quantitative determination by absorbance measurement at 320 nm. The hRf values of compounds (1) to (3) were 74, 61 and 84, respectively.LOD and LOQ were calculated for the estrogenic model compound (1): LOD was 0.46 pg without prior development of the TLC plate and 0.48 pg after development, LOQ was 0.8 pg without development and 1.6 pg after development.

      Classification: 4e, 13b
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