Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

Page
      117 076
      Analysis of plant glycosylceramides by automated multiple development
      M. REISBERG*, R. NEUBERT, Birgit DRAEGER (*Institute of Pharmacy, Martin-Luther-
      University Halle-Wittenberg, 06099 Halle, Germany, mathias.reisberg@pharmazie.uni-halle.de)

      CBS 113, 13-15 (2014). HPTLC of glycosylceramide Glc-d18:2 h16:0 from wheat germ and standards squalene, cholesteryl oleate, glyceryl trioleate, linoleic acid, ß-sitosterol, and ß-sitosterol glucoside on silica gel in the AMD 2 with a 18-step gradient modified from Opitz et al. (Chromatographia 73 (2011) 559), methanol replaced ethanol, and the mobile phase composition was changed slightly (pre-conditioning with 4 M acetic acid before each step, drying time 1.5 min, development duration 3 h and solvent consumption 200 mL). Detection by dipping in copper sulfate phosphoric acid reagent for 20 s and heating at 130 °C for 15 min revealed grey-brown bands. Densitometry evaluation by absorbance measurement at 546 nm. For Glc-d18:2 h16:0, regression analysis showed a polynomial relationship with coefficients of determination (R2) from 0.995 to 0.999 (n=3, 50 - 1000 ng/band). LOD (S/N 3) and LOQ (S/N 10) of Glc-d18:2_x000D_ h16:0 were 10 ng/band and 50 ng/band, respectively (n = 6).

      Classification: 11
      117 103
      Experimental study of the stability of some oxicams in contact with various redox agents
      M. STAREK*, M. DABROWSKA, M. BRACHA, W. OPOKA (*Department of Inorganic
      and Analytical Chemistry, Faculty of Pharmacy, Collegium Medicum Jagiellonian
      University, 9, Medyczna Str., 30-688 Kraków, Poland, mstarek@cm-uj.krakow.pl)

      J. Planar Chromatogr. 29, 273-280 (2016). HPTLC of piroxicam, tenoxicam, meloxicam and isoxicam on silica gel with ethyl acetate – toluene – butylamine 2:2:1. Detection under UV 290 nm. The method was applied to study the effect of oxidizing or reducing agents on the stability of these drugs.

      Classification: 28a, 32a
      117 132
      A validated direct thin-layer chromatographic separation and enantioselective determination of racemic centrally acting drugs using ion-pair and ligand-exchange chiral selectors
      N. SALAMA, H. ZAAZAA, L. EL HALIM*, M. SALEM, L. EL FATTAH (*Pharmaceutical Chemistry Department, National Organization for Drug Control and Research (NODCAR), 6 Abu Hazem Street, Pyramids Ave, P.O. Box 29, Giza, Egypt, lobna_nodcar@yahoo.com)

      J. Planar Chromatogr. 29, 176-183 (2016). HPTLC of atracurium besylate (1) and atropine sulfate (2) on silica gel with acetonitrile – methanol – dichloromethane – glacial acetic acid – water containing 70 mg L-(+)-tartaric acid 70:10:5:7:1, pH 5 for (1), and methanol – water containing 40 mg L-histidine and 20 mg copper(II) acetate 22:3, pH 7 for (2). Quantitative determination by absorbance measurement at 280 nm for (1) and 215 nm for (2). The hRF values for (1) and (2) were 51 and 65, respectively. Linearity was in the range of 2-14 μg/zone for (1) and 5-35 μg/zone for (2). Intermediate precisions were below 1 %. The LOD and LOQ were 0.5 and 1.6 µg/zone for (1) and 1.2 and 3.6 µg/zone for (2). Average recovery was found to be 103.4 % for (1) and 96.6 % for (2).

      Classification: 38
      118 063
      Mesembrine alkaloids
      J. KRSTENANSKY (KGI School of Pharmacy, 535 Watson Dr., Claremont, CA 91711, USA, John_Krstenansky@kgi.edu)

      J. Ethnopharmacol. 195, 10-19 (2017). HPTLC of mesembrine alkaloids (mesembrine, mesembrenone, mesembrinol, mesembrenol, epimesembranol, epimesembrenol) in the South African medicinal plant Sceletium tortuosum on silica gel with dichloromethane – methanol – 10 % ammonia 900:100:1. Quantitative determination by absorbance measurement at 280 nm. The LOD and LOQ were in the range of 18-31 ng/zone and 44-95 ng/zone, respectively.

      Classification: 22
      119 016
      RP-18 chromatographic-based study of the blood–brain barrier permeability of selected sunscreens and preservatives
      J. PYZOWSKI*, E. BRZEZINSKA, A. SOBANSKA (*Department of Analytical
      Chemistry, Faculty of Pharmacy, Medical University of Lodz, ul. Muszy?skiego
      1, 90-151 ?ód?, Poland, jaroslaw.pyzowski@umed.lodz.pl)

      J. Planar Chromatogr. 30, 275-284 (2017). HPTLC of selected cosmetic raw materials (UV filters and preservatives) on RP-18 with acetonitrile ‒ pH 7.4 phosphate buffered saline 7:3. Qualitative determination at UV 254 nm. Molecular descriptors were calculated to examine the behavior towards the blood-brain barriers.

      Classification: 2c
      119 054
      Concurrent analysis of the biologically active markers
      ?-amyrin and ?-sitosterol by applying a validated high-performance thin-layer chromatography method in the aerial parts of Tinospora cordifolia and Calotropis gigantia
      M. ALAJMI, A. HUSSAIN, P. ALAM* (*Department of Pharmacognosy, College
      of Pharmacy, King Saud University, P.O. Box 2457, Riyadh 11451, Saudi Arabia, alamperwez007@gmail.com)

      J. Planar Chromatogr. 30, 175-180 (2017). HPTLC of β-amyrin (1) and β-sitosterol (2) in the aerial parts of Tinospora cordifolia and Calotropis gigantia on silica gel with n-hexane – ethyl acetate 3:1. Detection by spraying with p-anisaldehyde reagent. Quantitative determination by absorbance measurement at 530 nm. The hRF values for (1) and (2) were 39 and 26, respectively. Linearity was between 100 and 1400 ng/zone for (1) and (2). LOD and LOQ were 18 and 55 ng/zone for (1) and 30 and 91 ng/zone for (2). The intermediate precision was <2 % (n=6). Recovery rate ranged from 98.4 to 99.3 % for (1) and 98.3 to 99.9 % for (2).

      Classification: 13c
      119 085
      Development and validation of a high-performance thin-layer chromatography method for the determination of artesunate and amodiaquine in tablet formulations
      Y. MWALWISI, S. OMOLO, L. HOELLEIN, D. SHEWIYO, U. HOLZGRABE, E. KAALE* (*Muhimbili University of Health and Allied Sciences, School of Pharmacy, Dar es Salaam, Tanzania, elia.kaale@muhas.ac.tz)

      J. Planar Chromatogr. 30, 307-312 (2017). HPTLC of artesunate (1) and amodiaquine (2) on silica gel with toluene – acetonitrile – methanol – ammonium acetate – triethylamine 20:10:6:2:1. Detection of (1) by spraying with a mixture of methanol and sulfuric acid 19:1, followed by heating at 75 °C for 5 min. Quantitative determination by absorbance measurement at 503 nm for (1) and 345 nm for (2). The hRF values for (1) and (2) were 35 and 68, respectively. Linearity was between 93 and 280 ng/zone for (1) and 250 and 1250 ng/zone for (2). The intermediate precision (n=6) was <5 % for (1) and 2 % for (2). Recovery rate ranged from 90 to 110 % for (1) and from 98 to 102 % for (2).

      Classification: 28a, 32a
      120 008
      L-Theanine – an astounding sui generis integrant in tea
      E. SHARMA, R. JOSHI, A. GULATI* (*CSIR-Institute of Himalayan Bioresource Technology, Palampur, Himachal Pradesh, India, ashugulati@ihbt.res.in)

      Food Chem. 242, 601-610 (2018). Review of recent research on L-theanine, including the use of HPTLC for the rapid quantitative determination in Camellia sinensis and the combination with other non-chromatographic techniques.

      Classification: 1, 18a
Page