Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      127 020
      Qualitative and quantitative analyses of aloe‑emodin, rhein, and emodin in qi yin granules by high‑performance thin‑layer chromatography
      N. XI (Xi Na), H. LIU (Liu Honbing), S. XU (Xu Shihao), X. YAN (Yan Xuehua)* (*College of TCM, Xinjiang Medical University, Urumqi 830011, Xinjiang, China, yan19810825@sina.com)

      J. Planar Chromatogr. 33, 579-585 (2020). HPTLC of aloe-emodin (1), rhein (2) and emodin (3) on silica gel with petroleum ether - ethyl acetate - formic acid 31:10:2. Quantitative determination by absorbance measurement at 440 nm. The hRF values for (1) to (3) were 47, 36 and 25, respectively. Linearity was between 90 and 426 ng/zone for (1), 64 and 304 ng/zone for (2) and 80 and 380 ng/zone for (3). Intermediate precision was below 2 % (n=6). Average recovery was 98.6 % for (1), 99.7 % for (2) and 100.0 % for (3).

      Classification: 9
      127 001
      Standardization and validation of a high‑performance thin‑layer chromatography method for the quantification of aflatoxin B1 and its application in surveillance of contamination level in marketed food commodities from the Mumbai region
      S. PRADHAN*, L. ANANTHANARAYAN (*Institute of Chemical Technology, Matunga, Mumbai 400019, India, laxmi.ananth.iyer@gmail.com)

      J. Planar Chromatogr. 33, 617-630 (2020). HPTLC of aflatoxin B1 in marketed samples of corn, groundnut, rice, wheat and dried chillies on silica gel with chloroform - acetone 9:1. Quantitative determination by absorbance measurement at 366 nm. The hRF value for aflatoxin B1 was 36. Linearity was between 10 and 120 ng/zone. Intermediate precision was below 2 % (n=3). The LOD and LOQ were 1 and 3 ng/zone. Average recovery was 85.2 %.

      Classification: 28b
      127 068
      Feasible TLC-spectro-densitometry technique for simultaneous determination of two hepatitis C antiviral drugs, sofosbuvir and simeprevir: Application to combined pharmaceutical dosage forms and human plasma
      B.S. MOHAMMED*, S.M. DERAYEA, A.E. HAMAD (*Dep. of Pharm. Anal. Chem., Faculty of Pharmacy, Menoufia Univ., Menoufia, Egypt, Bassam.shaaban@phrm.menofia.edu.eg)

      J. of Chromatogr. Sci. 59 (6), 576-583 (2021). HPTLC of simeprevir (SMV) and sofosbuvir (SOF) on silica gel with ethyl acetate – hexane - methanol 5:4:1. The hRF of SMV was 67 and of SOF 43. Quantitative determination by densitometry at 273 nm. The linearity range was between 60-1000 ng/band for SMV and 70-1200 ng/band for SOF, with good correlation coefficients (0.9993-0.9997) for both.  LOD was 15 and 22 ng/band and LOQ 44 and 66 ng/ band for SMV and SOF, respectively.

      Classification: 32
      127 069
      Green HPLC–DAD and HPTLC methods for quantitative determination of binary mixture of pregabalin and amitriptyline used for neuropathic pain management
      I.A. NAGUIB, N.A. ALI*, F.A. ELROBY, M.R. ELGHOBASHY (*Anal. Toxicol. Lab., Forensic Med. Authority, Ministry of Justice, Cairo 11647, Egypt, n.aboyazeed@yahoo.com)

      J. of Chromatogr. Sci. 59 (6), 536-547 (2021). HPTLC of pregabalin (PGB) and amitriptyline (AMT) as an active binary mixture in pure forms or in human biological fluids (plasma/urine)  on silica gel with ethanol - ethyl acetate - acetone - ammonia solution 160:40:20:1. Detection by spraying with 3 % ethanolic ninhydrin solution. Quantitative determination by densitometry at 220 nm for AMT and 550 nm for PGB peaks after derivatization. The linearity range was 0.2 - 2.5 μg/band for PGB and 0.1-2.0 μg/band for AMT.

      Classification: 32a
      127 070
      Development and validation of two novel chromatographic methods: HPTLC and HPLC for determination of bromhexine hydrochloride in presence of its two impurities
      N.S. ABDELWAHAB, SELVIA M. ADLY*, N.W. ALI,MAHA M. ABDELRAHMAN (*Pharm. Anal. Chem. Dep., Faculty of Pharmacy, Beni-Suef Univ., Alshaheed Shehata Ahmed Hegazy St., Beni-Suef 62514, Egypt, selvia.maged.adly@gmail.com)

      J. of Chromatogr. Sci. 59(5), 425–431 (2021). HPTLC of bromhexine hydrochloride (BHX), impurity B (IMB) and impurity C (IMC) on silica gel with hexane - acetone - ammonia solution 450:25:4. Quantitative determination by densitometry at 240 nm. The linearity was in the range of 0.40-10.00, 0.20-2.00 and 0.20-2.00 μg/band for BHX, IMB and IMC, respectively. Comparison with an HPLC method showed no significant differences regarding accuracy and precision.

      Classification: 32a
      127 071
      Simultaneous determination of paracetamol, propyphenazone and caffeine in presence of paracetamol impurities using dual-mode gradient HPLC and TLC densitometry methods
      H. IBRAHIM*, A.M. HAMDY, H.A. MEREY, A.S. SAAD (*Anal. Chem. Dep., , Fac. of Pharmacy, Egyptian Russian Univ., Cairo-Suez Road, Badr City 11829, Egypt, hany.ibrahim@eru.edu.eg)

      J. of Chromatogr. Sci. 59 (2), 140-147 (2021). TLC of paracetamol (PC), propyphenazone (PZ) and caffeine (CF) in the presence of the two PC impurities 4-aminophenol and 4-nitrophenol, on silica gel with chloroform - toluene - ethyl acetate - methanol - acetic acid 60:60:10:20:1. Quantitative determination by densitometry at 220 nm.

      Classification: 32a
      127 072
      Application of optimized and validated agar overlay TLC–bioautography assay for detecting the antimicrobial metabolites of pharmaceutical interest
      B.R. NUTHAN, D. RAKSHITH, K.M. MARULASIDDASWAMY, H.C.Y. RAO, K.P. RAMESHA, N.C. MOHANA, S. SIDDAPPA, D. DARSHAN, K.K.S. KUMARA, S. SATISH* (*Dep. of Studies in Microbiol., Univ. of Mysore, Manasagangotri, Mysuru 570 006, India, satish.micro@gmail.com)

      J. of Chromatogr. Sci. 58 (8), 737-746 (2020). Presentation of a method for determination of the antimicrobial capability of the metabolite coriloxin, derived from mycoendophytic Xylaria sp. NBRTSB-20, and purified by column chromatography with its purity assessed by HPLC, UPLC-ESI-QTOF-MS, FT-IR and NMR. Determination of the antimicrobial capability by TLC–bioautography with the agar overlay technique. Evaluation under visible light. The LOD of coriloxin antimicrobial activity was 10 μg for Escherichia coli and 20 μg for Staphylococcus aureus and Fusarium oxysporum. Inter- and intra-day precision was below 6.6 %. The recovery was between 91.2 to 108.7 % with RSD values of 0.9-2.3 %.

      Classification: 4e
      127 073
      A validated stability-indicating HPTLC assay for determination of 10-hydroxy-2-decenoic acid content in royal jelly products using robust regression methods
      M.A. KORANY, M.S. MONEEB*, A.M. ASAAD, N.A. EL-SEBAKHY, A.A. EL-BANNA (*Dep. of Pharm. Anal. Chem., Fac. of Pharmacy, Univ. of Alexandria, El-Khartoum square - Azarita, Alexandria 21521, Egypt, marwamoneeb@yahoo.com)

      J. of Chromatogr. Sci. 58 (6), 520 – 534 (2020). HPTLC of 10-hydroxy-2-decenoic acid (10-HDA) in royal jelly products marketed in Egypt, on silica gel with chloroform - acetic acid 10:1. Quantitative determination by densitometry at 210 nm. First and second derivative treatment of the data and comparison between three statistical regression methods: parametric, nonparametric and weighted regression (WR). Derivative treatment of the data improved the sensitivity of the chromatographic signals. The WR method was advantageous over the use of the other two models and resulted in an enhancement of the accuracy and precision of the 10-HDA analysis. Recovery was 99.9 % with WR and 99.6 and 98.6 % with the other statistical methods. Further, the royal jelly standard was subjected to forced degradation studies including the effect of hydrolysis, oxidation, photolysis and dry heat.

       

      Classification: 11a
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