Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      129 032
      High‑performance thin‑layer chromatography (HPTLC) method development and validation for the quantification of catechin in the hydroalcoholic extract of Parkia roxburghii seed
      S. CHAUDHARY*, S. LALVENHIMI, S. BUSWAS, J. CHANDA, A. KAR, P. BHARDWAJ, N. SHARMA, P. MUKHERJEE (*Institute of Bioresources and Sustainable Development (IBSD), Department of Biotechnology, Government of India, Takyelpat, Imphal, Manipur 795001, India, pardeep2128@gmail.com)

      J. Planar Chromatogr. 35, 161-167 (2022). HPTLC of catechin in the seeds of Parkia roxburghiion silica gel with ethyl acetate - acetic acid - formic acid - water 40:4:3:4. Quantitative determination by absorbance measurement at 302 nm. The hRF value for catechin was 61. Interday and intra-day precisions were below 1 % (n=3). The LOD and LOQ were 12 and 37 ng/zone, respectively. Recovery was found in the range of 99.1-99.5 %.

      Classification: 8a
      129 033
      Identification of potential source of quality raw material of Costus speciosus from Western coast of Malabar
      A. SRIVASTAVA, P. RAWAT, M. KUMAR, V. NIRALA, S. SINGH, K. PRABHU, V. SUNDARESAN, S. SRIVASTAVA* (*Pharmacognosy Division, CSIR-National Botanical Research Institute, Lucknow, U.P. 226001, India, sharad_ks2003@yahoo.com)

      J. Planar Chromatogr. 35, 139-151 (2022). HPTLC of diosgenin in Costus speciosus on silica gel with n-hexane - ethyl acetate 7:2. Detection by spraying with anisaldehyde  -sulfuric acid (0.5 mL anisaldehyde in 1 mL of 97 % sulfuric acid), followed by drying at 105 °C. Quantitative determination by absorbance measurement at 440 nm. The hRF value for diosgenin was 23. Linearity was between 0.1 and 0.7 µg/zone. The LOD and LOQ were 0.84 and 2.55 µg/zone. 

      Classification: 14
      129 036
      High‑performance thin‑layer chromatography‑based quantification of therapeutic phytochemicals in the methanolic extract of Ayurvedic formulation Drakshavaleha
      D. SONA, G. BAGHEL, L. CHANDRAVANSHI, U. SAHU, N. CHAUHAN, A. KUMAR*, P. GUPTA (*Shri Narayan Prasad Awasthi (NPA) Government Ayurved College, Raipur, CG, India, drawanishkr@gmail.com)

      J. Planar Chromatogr. 35, 117-125 (2022). HPTLC of gallic acid (1), piperine (2),
      resveratrol (3), and quercetin (4) in Ayurvedic formulation Drakshavaleha on silica gel with ethyl acetate - toluene - glacial acetic acid - formic acid 10:10:2:1. Quantitative determination by absorbance measurement at 254 and 366 nm. The hRF values for (1) to (4) were 45, 72, 68 and 58, respectively. 

      Classification: 8a
      129 037
      Simultaneous determination of epimers (+)‑catechin and (‒)‑epicatechin in Onosma bracteatum Wall. using high‑performance thin‑layer chromatography‒mass spectrometry method
      A. RAJPARA, N. GANDHI, V. BHATT, M. SHAH* (*Department of Pharmacognosy, L. M. College of Pharmacy, Navrangpura, Ahmedabad 380009, Gujarat, India, mbshah2007@rediffmail.com)

      J. Planar Chromatogr. 35, 89-95 (2022). HPTLC of epimers (+)‑catechin (1) and (-)‑epicatechin (2) in Onosma bracteatum on silica gel with diisopropyl ether - ethyl acetate - formic acid 90:2:7. Detection by spraying with p-toluenesulfonic acid reagent, followed by heating at 110 °C. Quantitative determination by absorbance measurement at 280 nm. The hRF values for (1) and (2) were 47 and 37, respectively. Linearity was between 1000 and 5000 ng/zone for (1) and (2). Interday and intra-day precisions were below 2 % (n=3). The LOD and LOQ were 284 and 863 ng/zone for (1) and 183 and 611 ng/zone for (2). Average recovery was 98.9 % for (1) and 99.0 % for (2).

      Classification: 38
      129 038
      High‑performance thin‑layer chromatography‑based method development for the analysis of 4‑methoxy‑2‑nitroaniline as potential genotoxic impurity
      P. MINIYAR*, P. CHAVAN, S. PATIL, A. THOMAS, S. CHITLANGE (*STES’s Sinhgad Institute of Pharmaceutical Sciences, Savitribai Phule Pune University, Lonavala 410401, India, miniyarpankaj@gmail.com)

      J. Planar Chromatogr. 35, 73-81 (2022). HPTLC of omeprazole (1) and its impurity 4‑methoxy‑2‑nitroaniline (1) on silica gel with methanol - n-hexane - ethyl acetate 1:10:11. Quantitative determination by absorbance measurement at 291 and 223 nm for (1) and (2), respectively. The hRF values for (1) and (2) were 25 and 89, respectively. Linearity was between 100 and 500 ng/zone for (1) and 10 and 50 ng/zone for (2). Interday and intra-day precisions were below 1 % (n=3). The LOD and LOQ were 3.2 and 9.8 ng/zone for (1) and 0.41 and 1.25 ng/zone for (2), respectively. Recovery was in the range of 98-102 % for (2).

      Classification: 32a
      129 040
      Effect of shodhana (purification process) on guggulsterone E and Z in Commiphora mukul
      U. GAJJAR*, K. PUNDRIKAKSHUDHU (*Department of Pharmacognosy, Shree S.K. Patel College of Pharmaceutical Education and Research, Ganpat University, Kherva, Mehsana, Gujarat 384012, India, drumanggajjar@gmail.com)

      J. Planar Chromatogr. 35, 13-21 (2022). HPTLC of guggulsterone E (1) and Z (2) in Commiphora mukul on silica gel with toluene - acetone 9:1. Quantitative determination by absorbance measurement at 250 nm. The hRF values for (1) and (2) were 18 and 23, respectively. Linearity was between 60 and 360 ng/zone for (1) and (2). 

      Classification: 13c
      129 041
      Inherent stability testing of empagliflozin in the presence of metformin HCl by HPTLC and characterization of degradation products of empagliflozin by LC–ESI–QTOF–MS/MS
      V. VICHARE*, V. CHOUDHARI, V. TAMBE, S. DHOLE (*PES Modern College of Pharmacy (for Ladies), Moshi, Pune, Maharashtra, India, vicharevijaya11@gmail.com)

      J. Planar Chromatogr. 35, 61-71 (2022). HPTLC of empagliflozin (1) in the presence of metformin HCl (2) on silica gel with toluene - methanol - ammonia - glacial acetic acid 72:26:1:1. Quantitative determination by absorbance measurement at 230 nm. The hRF values for (1) and (2) were 15 and 48, respectively. Linearity was between 11 and 112 ng/zone for (1) and 85 and 850 ng/zone for (2). Interday and intra-day precisions were below 2 % (n=3). The LOD and LOQ were 0.6 and 1,7 ng/zone for (1) and 5 and 15 ng/zone for (2), respectively. Recovery was found to be in the range of 99.4-101.0 % for (1) and 100.3-101.4 % for (2). Degradation products were characterized by liquid chromatography coupled with electrospray ionizationquadrupole-time of flighttandem mass spectrometry (LCESIQTOFMS/MS).

      Classification: 8b, 17c
      129 042
      A validated high‑performance thin‑layer chromatography method for the simultaneous quantification of 6‑gingerol, guggulsterone E and guggulsterone Z in coded formulation AYUSH SG‑5 prepared for rheumatoid arthritis
      V. KUMAR*, V. KUSHWAHA, Y. GANDHI, S. MISHRA, V. CHARDE, C. JAGTAP, G. BABU, A. SINGH, R. SINGH, N. SRIKANTH (*Chemistry Section, Department of Chemistry, Central Ayurveda Research Institute, Jhansi, Uttar Pradesh 284003, India, vijaychem99@gmail.com)

      J. Planar Chromatogr. 35, 23-33 (2022). HPTLC of 6‑gingerol (1), guggulsterone (2) E and guggulsterone Z (3) on silica gel with toluene - acetone 9:1. Quantitative determination by absorbance measurement at 280 nm. The hRF values for (1) and (2) were 15, 19 and 25, respectively. Linearity was between 100 and 1200 ng/zone for (1) to (3). Interday and intra-day precisions were below 3 % (n=5). The LOD and LOQ were 100 and 400 ng/zone for (1) to (3), respectively. Recovery was between 95.4 and 101.05 %. 

      Classification: 7
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