Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      132 026
      New chromatographic techniques for sensitive mebendazole quantification in the presence of degraded product, commercial tablets application, and greenness assessment
      A. AHMED*, H. BETAKOUSHY, F. ABDALLAH (*Nahda University, Faculty of Pharmacy, Pharmaceutical Chemistry Department, Beni-Suef 62514, Egypt, hany.batakoushy@phrm.menofia.edu.eg)

      J. AOAC Int. 106, 846-853 (2023). HPTLC of mebendazole (1) in the presence of its degraded product (2) on silica gel with ethanol - ethyl acetate - formic acid 60:160:1. Quantitative determination by absorbance measurement at 254 nm. The hRF values for mebendazole and its degraded product were 80 and 30, respectively. Linearity was in the range of 0.2-3 μg/zone. Intermediate precisions were below 2 % (n=3). LOD and LOQ were 0.58 and 1.85 μg/zone for (1) and 0.31 and 0.96 μg/zone for (2), respectively. Recovery was 100.2 % for (1) and 99.7 % for (2). 

      Classification: 32a
      132 027
      Principles of white analytical chemistry and design of experiments to development of stability-indicating chromatographic method for the simultaneous estimation of thiocolchicoside and lornoxicam
      P. PRAJAPATI*, V. PULUSU, S. SHAH (*Maliba Pharmacy College, Department of Quality Assurance, Maliba Campus, Bardoli-Mahuva Road, Tarsadi, Mahuva, Surat, Gujarat 394 350, India, pintu21083@gmail.com)

      J. AOAC Int. 106, 1654-1665 (2023). HPTLC of thiocolchicoside (1) and lornoxicam (2) on silica gel with n-heptane - acetone - ethanol 3:1:1. Quantitative determination by absorbance measurement at 370 nm. The hRF values for (1) and (2) were 25 and 60, respectively. Linearity was in the range of 20-100 ng/zone for (1) and (2). Intermediate precisions were below 2 % (n=3). LOD and LOQ were 0.3 and 1.0 μg/zone, respectively. Recovery was between 98 and 102 %. The developed method’s greenness was evaluated using the AGREE (Analytical Procedure Greenness) tool.

      Classification: 32a
      132 028
      Stability-indicating densitometric analysis of evogliptin tartrate in bulk and tablet dosage form
      S. SRIVASTAVA*, S. DHANESHWAR, N. KAWATHEKAR (*Department of Pharmaceutical Chemistry, Amity Institute of Pharmacy, Lucknow, Amity University Uttar Pradesh, Noida, Uttar Pradesh, India, suneeladhaneshwar@rediffmail.com)

      J. AOAC Int. 106, 1471-1477 (2023). HPTLC of evogliptin on silica gel with acetonitrile - water - formic acid 15:4:1. Quantitative determination by absorbance measurement at 270 nm. The hRF value for evogliptin was 62. Linearity was in the range of 1-5 μg/zone. Intermediate precisions were below 2 % (n=3). LOD and LOQ were 0.3 and 1.0 μg/zone, respectively. Average recovery was 101.1 %.   

      Classification: 32a
      132 029
      Red, green, and blue model-based assessment and principles of white analytical chemistry to robust stability-indicating chromatographic estimation of thiocolchicoside and diclofenac sodium
      P. PRAJAPATI*, V. PULUSU, S. SHAH (*Maliba Pharmacy College, Department of Quality Assurance, Maliba Campus, Bardoli-Mahuva Rd, Tarsadi, Mahuva, Surat, India, pintu21083@gmail.com)

      J. AOAC Int. 106, 1374-1388 (2023). HPTLC of diclofenac sodium (1) and thiocolchicoside (2) on silica gel with n-heptane - methyl acetate - ethanol 7:1:2. Quantitative determination by absorbance measurement at 278 nm. The hRF values for (1) and (2) were 79 and 12, respectively. Linearity was between was in the range of 100-500 ng/zone for (1) and 20-100 ng/zone for (2). Intermediate precisions were below 2 % (n=3). 

      Classification: 32a
      132 031
      A green reversed phase HPLC and HPTLC methods and their validation for simultaneous estimation of remogliflozin, vildgliptin and metformin in fixed dose combination formulation
      K. SETHY, G. KRISHNA, R. KATTA (*Department of Pharmaceutical Chemistry, School of Pharmacy, Centurion University of Technology and Management, Bhubaneswar, Odisha, India, gopalmedchem@gmail.com)

      J. Liq. Chromatogr. Relat. Technol. doi:10.1080/10826076.2023.2284721 (2023). HPTLC of remogliflozin (1), vildgliptin (2) and metformin (3) on silica gel with phosphate buffer - acetonitrile - glacial acetic acid 15:35:1. Quantitative determination by absorbance measurement at 205 nm. The hRF values for (1) to (3) were 78, 60 and 36, respectively. Linearity was in the range of 50-100 ng/zone for (1) to (3). Intermediate precisions were below 2 % (n=6). LOD and LOQ were 5 and 16 ng/zone for (1), 3 and 8 ng/zone for (2) and 47 and 142 ng/zone for (3). Recovery was between 98 and 102 %.

      Classification: 32a
      132 034
      Emerging approaches for the detection of trimethylamine N-oxide: A gut derived metabolite
      A. KOTTARATHIL, D. S. RAJKUMAR, R. PADMANABAN* (*Immunodynamics and Interface Laboratory, Centre of Advanced Study in Crystallography and Biophysics, University of Madras, Chennai, India, drprajashree@gmail.com)

      J. Liq. Chromatogr. Relat. Technol. doi:10.1080/10826076.2023.2284737 (2023). HPTLC of quercetin (1), myricetin (2), tannic acid (3), gallic acid (4), ellagic acid (5), ascorbic acid (6) and humic acid (7) on silica gel with toluene - ethyl acetate - formic acid - methanol 15:15:4:2 in the first dimension and toluene - ethyl acetate - formic acid 6:3:1 in the second dimension for (1) to (4) and ethyl acetate - acetone - water - formic acid 5:3:1:1 for (5) and (6). Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (5) were 15, 73, 80, 21 and 62, respectively. Linearity was in the range of 100-600 ng/zone for (1) to (5) and (7) and 200-1200 ng/zone for (6). Intermediate precisions were below 2 % (n=3). LOD and LOQ were 26 and 79 ng/zone for (1), 22 and 80 ng/zone for (2), 21 and 64 ng/zone for (3), 31 and 94 ng/zone for (4), 10 and 102 ng/zone for (5), 65 and 197 ng/zone for (6) and 22 and 66 ng/zone for (7), respectively. Average recovery was between 99.1 and 103.1 % for (1) to (7).

      Classification: 7
      132 035
      Application of TLC-smartphone method for the analysis of carbamazepine in plasma
      M. ALI SOUSSI*, Y. MALLEK, W. AYED, S. LIOUANE, W. DOUKI (*Toxicology Laboratory, Fattouma Bourguiba University Hospital, Monastir, Tunisia, mohamedalisoussi@yahoo.fr)

      J. Liq. Chromatogr. Relat. Technol. 46, 335-342 (2023). HPTLC of carbamazepine in plasma on silica gel with cyclohexane - chloroform - acetic acid 2:2:1. Detection under UV light at 254 nm, followed by photographing with a smartphone. Images were processed using the JustTLC software. The hRF value for carbamazepine was 78. Linearity was in the range of 5-10 μg/mL. Intermediate precisions were below 2 % (n=3). LOD and LOQ were 0.94 and 2.8 μg/mLAverage recovery was 98 %.

      Classification: 32a
      132 038
      Validation of a high‑performance thin‑layer chromatography method for the quantitative determination of trehalulose
      M. MELLO, C. JACOBS, M. ISLAM, L. LIM, Cornelia LOCHER* (*Division of Pharmacy, School of Allied Health, University of Western Australia, Crawley, WA 6009, Australia, connie.locher@uwa.edu.au)

      J. Planar Chromatogr. 36, 201-210 (2023). HPTLC of trehalulose on silica gel with 1-butanol - 2-propanol - 5 mg/mL aqueous boric acid solution 3:5:1. Detection by spraying with aniline - diphenylamine - phosphoric acid reagent, followed by heating to 115 °C for 10 min. Plates were analyzed under white light using three sets of images: remission white, transmission white and remission–transmission white. The hRF value for trehalose was 5 (1) to (3) were 38, 24 and 50, respectively. Linearity was in the range of 100-800 ng/zone. Intermediate precisions were below 2 % (n=3). LOD and LOQ were 20 and 61 ng/zone, respectively. Mean recovery was 102.3 %.

      Classification: 10a
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