Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
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Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

      70 212
      Determination of diacetoneketogulonic acid in water samples by high-performance thin-layer chromatography
      A. EISENBEISS, S. REUKE, M. TÜRCK*, (*Cent. Anal. Lab., E. Merck, P.O. Box 4419, D-W-6100 Darmstadt, FRG)

      J. Chromatogr. 589, 390-393 (1992). TLC on silica with a) chloroform - methanol 8:2, and b) chloroform - methanol - acetic acid 80:20:2. Detection by immersing in 4-methoxybenzaldehyde solution and heating at 130 °C for 2 min. Quantification by fluorodensitometry at 366 nm.

      Classification: 37c
      96 061
      Determination of sulfonamides and trimethoprim in spiked water samples by solid-phase extraction and thin-layer chromatography
      Sandra Babic*, D. Asperger, D. Mutavdzic, A. J. M. Horvat, M. Kastelan-Macan (*Laboratory of Analytical Chemistry, Faculty of Chemical Engineering and Technology, University of Zagreb, Marulicev trg 20, 10000 Zagreb, Croatia)

      J. Planar Chromatogr. 18, 423-426 (2005). HPTLC of antibiotics (sulfadimidine, sulfadiazine, sulfaguanidine, trimethoprim) on silica gel without chamber saturation in a twin-trough chamber with chloroform - methanol 89:11. Quantification by videodensitometry at 254 nm. Limit of detection was 0.05 µg per spot for sulfadimidine, sulfadiazine, and sulfaguanidine, and 0.1 µg per spot for trimethoprim.

      Classification: 28a, 37c
      78 038
      Application of TLC and GC-MS to the identification of amino-PAHs in sewage sludges
      B. JANOZKA, K. TYRPIEN, D. BODZEK*. (Silesian Med. Acad., Fac. of Med., Dept. of Chem., H. Jordana Street 19, 41-808 Zabrze, Poland)

      J. Planar Chromatogr. 9, 450-455 (1996). Analytical TLC of aminoarenes (aminonaphthalene, -phenylnaphthalene, -pyrene, -fluoroanthene, -anthracene, -phenanthrene, -quinoline, isoquinoline, -chrysene) on RP-18 with acetonitrile - water 9:1; semipreparative TLC on aluminium oxide with dichloromethane - hexane - ether 1:1:1. Visualization under UV 254 and 366 nm.

      Classification: 37d
      117 031
      New screening concept for pesticide residue analysis in fruit and vegetables – HTpSPE-HRMS
      Claudia OELLIG*, W. SCHWACK (*Institute of Food Chemistry, University of Hohenheim, 70599 Stuttgart, Germany, claudia.oellig@uni-hohenheim.de)

      CBS 114, 13-15 (2015). To test the new HTpSPE–TOFMS screening, TLC of a pesticide mixture (acetamiprid, azoxystrobin, chlorpyrifos, fenarimol, mepanipyrim, penconazole, pirimicarb) in several plant matrices (cucumber, tomato, grape, apple extracts) on amino layer pre-treated by dipping in 2 % formic acid solution in acetonitrile and drying for 10 min. Development with 10 mL acetonitrile, migration distance 75 mm, drying 5 min; second development in the backwards direction with 10 mL acetone, migration distance 45 mm, drying 3 min. Detection under UV 254 nm, UV 366 nm and white light. For HTpSPE and μL-flow injection analysis–TOFMS the target analyte zone was eluted with the TLC–MS Interface into autosampler vials with acetonitrile – 10 mM ammonium formate 1:1, flow rate 0.2 mL/min, Elution time was 60 s. An HPLC system was coupled via a PEEK capillary and a nano-electrospray ionization interface to a TOFMS without an analytical column. The mean recovery for a pesticide mixture spiked into fruit and vegetable extracts was between 86 % and 116 % with %RSDs of 1.5–10 % (n = 5).

      Classification: 3a, 29, 37
      77 038
      Thin-layer-chromatography in water analysis
      K. MÜLLER, M. EGELKRAUT-HOLTUS, M. SIEBER, (Macherey-Nagel GmbH & Co. KG, Abt. LC, Produktgruppe DC, Neumann-Neander-Str. 6-8, D-52355 D¸ren)

      Dünnschicht-Chromatographie InCom Sonderband 1996, 157-165. HPTLC of benzo[g,h,i]perylene, indeno[1,2,3]pyrene, benzo[a]pyrene, benzo[b]fluoroanthene, benzo[k]fluoroanthene and fluoroanthene on caffeine-impregnated silica prewashed with dichloromethane, precooled for 30 min at -20 °C, with dichloromethane at -20 °C. After removal of the eluent the plates are dipped for 2 s into a solution of paraffin (low viscosity)/n-hexane 1:2 and dried again (for stabilization and intensification of the inherent fluorescence of the PAH). Quantification by densitometry.

      Classification: 5b, 37
      93 080
      Cleaning validation by TLC determination of norfloxacin as residue on pharmaceutical equipment surfaces
      I. VOVK*, B. SIMONOVSKA (*National Institute of Chemistry, Hajdrihova 19, SI-1000 Ljubljana, Slovenia, irena.vovk@ki.si, breda.simonovska@ki.si)

      CBS 89, 2-3 (2002). HPTLC of norfloxacin on silica gel (prewashed with methanol - chloroform 1:1) with methanol - chloroform - ammonia 51:34:15 in horizontal developing chamber with sandwich configuration. Quantitative determination by fluorescence measurement at 313/>400 nm.

      Classification: 28a, 37
      79 241
      HPLC and TLC identification of nitrogen polynuclear aromatic compounds in airborne particulate matter
      B. JANOZKA*, D. BODZEK, A. SZOTEK, L. WARZECHA, (*Silesian Med. Acad., Fac. of Med., Dept. of Chem., 41-808 Zabrze, H. Jordana Str. 19, Poland)

      J. Planar Chromatogr. 10, 55-58 (1997). TLC of nitronaphthalene, nitrofluorene, nitroanthracene, nitropyrene, quinoline, azafluorene, and benzo(h)-quinoline on RP-18 silica with acetonitrile - water 9:1 for nitroarenes and with methanol - water 9:1 for azaarenes. Detection under UV 254 and 366 nm, then by spraying with 15% tin(II) chloride in 36% hydrochloric acid + p-dimethyl-aminobenzaldehyde for nitroarenes and Dragendorff's reagent for azaarenes. Detection limits for 2-nitrofluorene 0.10 µg, for 9-nitroanthracene 0.075 µg, for 1-nitropyrene 0.025 µg, for 1-nitronaphthalene 0.10 µg.

      Keywords:
      Classification: 5b, 37b
      114 106
      A simple TLC–densitometric method for the quantification of acrylic acid in aqueous solutions
      Mei SANO, T. CHIN, T. TAKAHASHI, Hitomi OHARA, Y. ASO* (*Department of Biobased Materials Science, Kyoto Institute of Technology, 1 Hashigami-cho, Matsugasaki, Sakyoku, Kyoto 606-8585, Japan, aso@kit.ac.jp)

      J. Planar Chromatogr. 28, 12-16 (2015). HPTLC of acrylic acid (as trans-cinnamic acid after labeling through a coupling reaction with iodobenzene at 60 ºC for 30 min) in water samples on silica gel with chloroform - methanol - acetic acid mixture 90:10:1. Quantitative determination by absorbance measurement at 254 nm. The hRF value for labeled acrylic acid was 47. Linearity was between 0.1 and 1 mM. The intermediate precisions were below 1.2 % (n=3). The LOD for the labeled acrylic acid was 0.1 nmol. Recoveries were in the range of 97-103 %.

      Classification: 37c