Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
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      130 004
      Identification of acetylcholinesterase inhibitors in water by combining two-dimensional thin-layer chromatography and high-resolution mass spectrometry
      Lena STÜTZ*, W. SCHULZ, R. WINZENBACHER (*Laboratory for Operation Control and Research, Zweckverband Landeswasserversorgung, Langenau, Germany; stuetz.l@lw-online.de)

      J Chromatogr A, 1624, 461239 (2020). Samples were chemical standards of acetylcholinesterase (AChE) inhibitors (azamethiphos, caffeine, donepezil, galanthamine, methiocarb-sulfoxide, paraoxon-ethyl) and of neurotoxic compounds, as well as drinking or contaminated water samples enriched through solid phase extraction. HPTLC on spherical silica gel (pre-washed twice by 20 min immersion in isopropanol, heated 20 min at 120 °C before and after pre-washing with acetonitrile). First separation (preparative TLC) with automated multiple development (16 steps). Effect-directed analysis for AChE inhibitors by immersion (speed 5 cm/s, time 1 s) into enzyme solution, incubation 5 min at 37 °C and immersion into substrate solution (indoxyl acetate 2 % in methanol); visualization under UV 366 nm. Active zones from untreated layers were eluted through the oval head of a TLC-MS interface to a second plate for a second separation with a panel of other mobile phases. Bands of interest were eluted from the second layer with water through the oval elution head of the TLC-MS interface pump, into a RP18 liquid chromatography guard column, followed by a quadrupole time-of-flight mass spectrometer. Full scan mass spectra (m/z 100–1200) were recorded in negative and positive modes using electrospray ionization (and collision-induced dissociation for MS2). Among the water contaminants, lumichrome (riboflavin photolysis product), paraxanthine and linear alkylbenzene sulfonates were identified as AChE inhibitors.

      Classification: 3d, 4d, 4e, 22, 29b, 35d, 37c
      64 296
      Quantitative thin-layer chromatography of Nicotiana tabacum leaf surface components
      D.R. LAWSON*, D.A. DANEHOWER, (*Dep. Crop Sci., North Carolina State Univ., Raleigh, NC 27695-7629, USA)

      J. Chromatogr. 463, 429-440 (1989). TLC on silica with isopropanol - chloroform - dichloromethane - hexane 8:8:6:79. Detection by charring with 30% sulfuric acid. Quantification of underivatized chromatogram by densitometry at 200 nm.

      Classification: 35d
      87 161
      (Determination of the oxidation products of disulfonated and trisulfonated PDBP by thin-layer chromatography
      H. DONG (Dong Huiru)*, J. ZHANG (Zhang Jingchang), H. JIU (Jiu Hua), J. ZHANG (Zhang Jiangjing), (*Dept. App. Chem., Beijing Univ. Chem. Technol., Beijing 100029, P.R. China)

      Chin. J. Anal. Lab. (Fenxi Shiyanshi) 20 (3), 48-50 (2001). TLC on silica gel with isopropanol - ethanol - NH3 1:1:1. Detection under UV 254 nm. Quantification by UV spectrophotometry at 252 nm. Investigation of the optimization of the separation and validation of the method.

      Keywords:
      Classification: 4e, 24, 35d
      65 144
      Adsorption chromatography on cellulose V
      M. LEDERER*, M. SCHUDEL, (*Inst. Police Sci. Criminol., Univ. Lausanne, Place du Château 3, CH-1005 Lausanne, Switzerland)

      A simple chromatographic system for the identification of inks. J. Chromatogr. 475, 451-456 (1989). Proposal of a simple TLC system for the identification of inks based on cellulose layer, solution of ammonium sulfate or 1% sodium chloride as developing solvent; UV detection and photo dokumentation.

      Classification: 30a, 35d
      88 185
      (Separation of sulfonated products by thin-layer chromatography
      H. DONG (Dong Huiru)*, J. ZHANG (Zhang Jingchang), J. ZHANG (Zhang Jianjun), H. JIN (Jin Hua), (*Dept. Appl. Chem., Beijing Univ. Chem. Eng., Beijing 100029, P.R. China)

      Chinese Anal. Chem. (Fenxi Huaxue) 29 (9), 1109-1110 (2001). TLC on silica gel with 1) isopropanol - ethanol - NH3 2:2:1, 2) propanol - ethanol - NH3 2:2:1, 3) isopropanol - ethanol -water 1:1:1, and 4) propanol ethanol - water 1:1:1. Detection under UV 254 nm. Identification by finger print technique.

      Keywords:
      Classification: 35d
      65 185
      Separation of natural product sweetening agents using overpressured layer Chromatography
      F. FULLAS, J. KIM, C.M. COMPADRE, A.D. KINGHORN*, (*Prog. Collab. Res. Pharm. Sci. and Dep. Med. Chem. & Pharmacog., Coll. Pharm., Univ. Illinois at Chicago, Chicago, IL 60612, USA)

      J. Chromatogr. 464, 213-219 (1989). Analytical OPLC of polypodoside A, B and C on silica with ethyl acetate - ethanol - water 130:27:20, chloroform - methanol - water 6:3:1 and the lower layer of hexane - chloroform - methanol - water 0.8:6:3:1. Detection by spraying with 60% sulfuric acid and heating at 110°C for 10 min.; densitometry. Also preparative OPLC.

      Keywords:
      Classification: 3d, 35d
      94 110
      Some possibility of Thin-layer chromatographic analysis of Baltic amber and other natural resins
      A. MATUSZEWSKA*, A. JOHN (*Dep. Geochem., Mineralogy, and Petrography, Fac. Earth Sci., Silesian Univ., 60 Bedzinska Str., 41-200 Sosnowiec, Poland)

      Acta Chromatographica 14, 82-91 (2004). Comparative investigation of the group composition of ethanol extracts obtained from natural resins of different origin and geological age by TLC on silica gel with dichloromethane - methanol 10:1 for carboxylic acids and a-hydroxy and a-keto acids, and with hexane - benzene - methanol 2:6:1 for other compounds. Detection with phosphoric and sulfuric acid and under UV 254 nm for additional identification of unsaturated compounds. Discussion of the potential of using the characteristics of the chromatograms as an auxiliary tool for classification of natural resins and, especially important, fossil resins.

      Keywords:
      Classification: 35d
      67 236
      TLC-scanning for direct quantitation of natural waxes
      R. MARTINEZ, P. MOYNA, (Farmacognosia y Productos Naturales, Facultad de Quimica, Av. Gral. Glores 2124, Montevideo, Urugay)

      J. Liquid Chromatogr. 13, 1959-1965 (1990). TLC of natural waxes on silica with a solvent mixture. Detection by charring with sulfuric acid - water 1:1, and heating at 200 °C Investigation of the influence of heating time and amount of charring agent.

      Classification: 35d