Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

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      112 129
      (Exploration on the procedures for the quality control of Shiming Granules by thin-layer chromatography) (Chinese)
      Y. ZHANG (Zhang Yun)*, H. HU (Hu Haiting), Q. LI (Li Qin) (*Pharm. Coll., Henan Univ., Henan, Kaifeng, 475004, China)

      Chinese J. of Henan Univ. (Med Sci.) 32 (2), 117-121 (2013). Shiming Granule is a herbal TCM preparation for invigorating blood circulation, improving liver and pulmonary functions and the eyesight. For quality control, TLC on silica gel 1) for Rhizoma et Radix Notopterygii, with n-hexane – ethyl acetate 7:3, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating until the zones are visible in daylight and under UV 366 nm; 2) for Bupleurum chinense, with ethyl acetate – methanol – water 8:2:1, detection by spraying with 2 % p-dimethylaminobenzaldehyde in 40 % sulfuric acid and heating at 60 °C, viewing under UV 366 nm; 3) for Rhizoma Atractylodis, with petroleum ether (60-90 °C) - ethyl acetate 20:1, detection by spraying with 5 % p-dimethylaminobenzaldehyde in 10 % sulfuric acid and heating until the zones are visible in daylight; 4) for Exocarpium Citri Rubrum, with ethyl acetate – methanol - water 100:17:10, detection by spraying with 3 % aluminiumchloride in ethanol, viewing under UV 366 nm; 5) for Radix Saposhnikoviae, with chloroform – methanol 4:1, detection under UV 254 nm; 6) for Salvia miltiorrhiza, with benzene – ethyl acetate 19:1, detection under UV 366 nm; 7) for Radix Paeoniae Rubra, with chloroform – methanol – formic acid 200:25:50:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating until the zones are visible in daylight; 8) for Herba Equiseti Hiemalis, with cyclohexane – ethyl acetate – formic acid 20:10:1, detection by spraying with 5 % aluminium chloride in ethanol and viewing under UV 366 nm; 9) for Cuscuta chinensis Lam., with ethyl acetate – butanone – formic acid – water 11:1:1:1, detection by spraying with 5 % aluminium chloride in ethanol and heating at 105 °C until the zones are visible, and viewing under UV 254 nm; 10) for Rehmannia glutinosa Libosch, with chloroform – methanol – ammonia 40:10:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C until the zones are visible in daylight; 11) for Rhizoma Atractylodis Macrocephalae, with cyclohexane – ethyl acetate 7:3, detection by spraying with 5 % p-dimethylaminobenzaldehyde in sulfuric acid – ethanol 1:10 and heating at 105 °C until the zones arevisible in daylight; 12) for Radix Glycyrrhizae, with ethyl acetate – formic acid – water 15:3:2, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing under UV 366 nm; 13) for Radix Achyranthis Bidentatae, with chloroform – methanol 30:1, detection by spraying with 5 % phosphomolybdic acid in n-propanol and heating at 110 °C until the zones are visible in daylight.

      Classification: 32e
      113 075
      3, detection under UV 366 nm; 2) for Oleum menthae dementholatum, on silica gel with petroleum ether (60-90 °C) – benzene – ethyl acetate 9
      H. LIAO (Liao Honglan) , J. MA (Ma Jianxiong)* (*R & D Center, Guangxi Jinhaitang Pharm. Ltd. Co., Guangxi, Nanning 530313, China) (Study of the method for the quality control of Yinju Ganmao Pian tablets by thin-layer chromatography) (Chinese). Chinese J. of Northern Pharmacy 10 (6), 2-3 (2013). Yinju Ganmao Pian tablet is a herbal TCM for the treatment of cold caused fever, aversion to cold, headache, cough, sore throat, and tonsillitis. For quality control, TLC 1) for Evodia lepta (Spreng.) Merr., on silica gel with toluene – ethyl acetate 10

      and Dendranthema indicum, on silica gel containing 1 % NaOH, with ethyl acetate – methanol – water 100:17:10, detection by spraying with 1 % aluminum trichloride in ethanol firstly, then with 5 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible in daylight.

      Classification: 32e
      113 096
      (Identification of olibanum and illegally adulterated colophony in Xihuang Wan pills and Huoxue Zhitong San powders by thin-layer chromatography) (Chinese)
      L. SUN (Sun Lei)*, Y. LIU (Liu Yan), Y. PENG (Peng Yu), H. JIN (Jin Hongyu) (*National Inst. for Food & Drug Contr., Beijing 100050, China)

      J. of China Pharm. 27 (7), 722-724 (2013). Xihuang Wan pill is a herbal TCM prescribed for treatment and adjuvant therapy of various cancers. Huoxue Zhitong San powder is a herbal TCM prescribed for traumatic injury and ecchymoma. In the drug market fraud rosin was found to be added to the key ingredient olibanum. For quality control, HPTLC of the sample extracts and the standards acetyl-11-keto-beta-boswellic acid (AKBA), 11-keto-beta-boswellic acid (KBA), beta-boswellic acid (beta-BA), acetyl-beta-boswellic acid (beta-ABA), and abietic acid (LOD=1.0 µg), on silica gel with toluene – ethyl acetate – heptane – formic acid 80:20:10:3 with chamber saturation for 20 min, detection 1) under UV 254 nm and UV 366 nm; 2) by spraying with a fresh solution of anisaldehyde – sulfuric acid – acetic acid 1:10:1000 and heating at 105 °C until the zones were visible in daylight. Verification of abietic acid from added rosin by HPLC. The method was used for the analysis of 63 batches of Xihuang Wan pills sampled from 13 pharmaceutical factories and 10 batches of Huoxue Zhitong San powder from 4 factories.

      Classification: 32e
      113 114
      (Study of the method for the quality control of Gushangling Jiaonang capsules by high-performance thin-layer chromatography) (Chinese)
      M. ZHENG (Zheng Meishan)*, X. CUI (Cui Xuan), L. XU (Xu Lianhua) (*Yanbian State Inst. for Food & Drug, Jilin, Yanji 133000, China)

      J. of China Pharm. 22 (3), 13-15 (2013). Gushangling Jiaonang capsule is a herbal TCM for post traumatic functional recovery, prescribed to treat muscle atrophy, bone hyperplasia, neck and lumbar diseases, nerve injuries etc. For quality control, HPTLC on silica gel 1) for Paeonia lactiflora Pall., with chloroform – ethyl acetate – methanol – formic acid 200:25:50:1, detection by spraying with 3 % vanillin in sulfuric acid – water 1:200 and heating mildly until the zones are visible in daylight; 2) for Angelica sinensis, with n-hexane – ethyl acetate – 9:1, detection under UV 366 nm; 3) Astragalus membranaceus (Fisch.) Bunge., with chloroform – methanol – water 13:7:2, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible in daylight.

      Classification: 32e
      114 065
      (Studies on an improved method for the quality control of Shuanghuang Tongfeng Jiaonang capsules) (Chinese)
      Y. CHEN (Chen Yutang), Y. HUANG (Huang Yirong), J. CHENG (Cheng Jinle)*, Y. LIANG (Liang Yanling), J. CHEN (Chen Jinmei) (*Zhongshan Zeus Pharm. Group Co., Ltd., Guangdong, Zhongshan 528437, China)

      Mod. Chinese Med. 3, 232-236 (2014). Shuanghuang Tongfeng Jiaonang capsules are a TCM preparation for the treatment of hyperuricemia. For quality control, TLC on silica gel (1) for Paeonia veitchii and the standard paeoniflorin, with chloroform – ethyl acetate – methanol – formic acid 200:25:50:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C until the zones are visible under white light; (2) for Astragalus membranaceus (Fisch.) Bunge. and the standard astragaloside A, with the lower phase of chloroform – methanol – water 13:6:2 after placing at a temperature lower than 10 °C for a night, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible under white light; (3) for Cortex Fraxini and the standards esculin hydrate and esculetin, with chloroform – methanol – formic acid 20:5:1, detection at UV 366 nm. Quantification of astragaloside A by HPLC.

      Classification: 32e
      114 088
      In vitro radical-scavenging activity, toxicity against A
      Luciana RAVAGLIA, Kerolayne GONCALVES, Nathália MITSUKO OMAYA, Roberta GOMESCOELHO, A. A. SPIELMANN, Neli K. HONDA* (*Institute of Chemistry, Universidade Federal de Mato Grosso do Sul, 79070-900 Campo Grande, Brazil, nelihonda8@gmail.com)

      salina, and NMR profiles of extracts of lichens collected from Brazil and Antarctica. Quim. Nova. 37, 1015-1021 (2014). TLC of (1) atranorin, (2) salazinic, (3) barbatic, (4) alpha-alectoronic, (5) alpha-collatolic, (6) cryptochlorophaeic, (7) caperatic, (8) lobaric and (9) protolichesterinic acids in six lichen species named Parmotrema cetratum (Ach.) Hale (I), Parmotrema wainioi (A. L.Smith) Hale (II), Canoparmelia cryptochlorophaea (Hale) (III), Parmotrema mesotropum (Müll. Arg.) Hale (IV), Cladia aggregata (Sw.) Nyl. (V) and Stereocaulon alpinum Laurer (VI), on silica gel with toluene - ethyl acetate - acetic acid 6:4:1 for (I, IV and V) and toluene - acetic acid 17:3 for (II, III and VI). Detection by spraying with p-anisaldehyde - sulfuric acid, followed by heating at 110 ºC. The hRF values of (1) and (2) in (I) were 73 and 33, respectively, whereas the value of (3) and (4) in (II) were 15 and 36; the value of (1) in (III) was 71. DPPH radical scavenging activity was also investigated.

      Classification: 32e
      115 032
      Phytochemical investigation and spectral studies of isolated flavonoid from ethanolic extract of whole plant Blumea lacera D
      Pratibha MISHRA*, Raghuveer IRCHHIAYA, Sunil Kumar MISHRA (*Department of Pharmacy, Dr. Bhim Rao Ambedkar University, Agra, India)

      Journal of Pharmacognosy and Phytochemistry 4 (2), 1-4 (2015). HPTLC of petroleum ether and ethanol extracts of aerial parts of Blumea lacera D.C. (Asteraceae), collected in the Gorakhpur district, with chloroform - benzene - formic acid 15:5:3. Evaluation in daylight revealed 11 zones, at least 9 of them at hRf between 3 and 47. The ethanol extract was purified by washing with water, chloroform and ethyl acetate successively, and then by fractionation on a silica gel (60-120 mesh) column; the benzene subfraction yielded, after exposure to iodine vapor, one yellow zone (hRf 41), identified (by IR, NMR and MS) as 3,5-dihydroxy-3’-methyl-6,7,4’-trimethoxyflavanone.

      Classification: 8a, 32e
      117 001
      A comprehensive analysis on Symplocos racemosa Roxb – Traditional uses, botany, phytochemistry and pharmacological activities
      N. ACHARYA*, S. ACHARYA, U. SHAH, R. SHAH, L. HINGORANI (*Department of Pharmacognosy, Institute of Pharmacy, Nirma University, Ahmedabad 382481, India, niyati20103@gmail.com)

      J. Ethnopharmacol. 181, 236-251 (2016). Analysis of the botanical description, geographical location, traditional and medicinal uses, phytochemistry and pharmacological investigation, toxicological aspects, patent information and clinical studies of Symplocos racemosa. The review described methods for the determination of loturine in the bark extracts of Symplocos racemosa on silica gel with chloroform – acetonitrile – triethylamine 7:5:2, quantitative determination by absorbance measurement at 280 nm.

      Classification: 1, 32e
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