Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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Chinese J. of Henan Univ. (Med Sci.) 32 (2), 117-121 (2013). Shiming Granule is a herbal TCM preparation for invigorating blood circulation, improving liver and pulmonary functions and the eyesight. For quality control, TLC on silica gel 1) for Rhizoma et Radix Notopterygii, with n-hexane – ethyl acetate 7:3, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating until the zones are visible in daylight and under UV 366 nm; 2) for Bupleurum chinense, with ethyl acetate – methanol – water 8:2:1, detection by spraying with 2 % p-dimethylaminobenzaldehyde in 40 % sulfuric acid and heating at 60 °C, viewing under UV 366 nm; 3) for Rhizoma Atractylodis, with petroleum ether (60-90 °C) - ethyl acetate 20:1, detection by spraying with 5 % p-dimethylaminobenzaldehyde in 10 % sulfuric acid and heating until the zones are visible in daylight; 4) for Exocarpium Citri Rubrum, with ethyl acetate – methanol - water 100:17:10, detection by spraying with 3 % aluminiumchloride in ethanol, viewing under UV 366 nm; 5) for Radix Saposhnikoviae, with chloroform – methanol 4:1, detection under UV 254 nm; 6) for Salvia miltiorrhiza, with benzene – ethyl acetate 19:1, detection under UV 366 nm; 7) for Radix Paeoniae Rubra, with chloroform – methanol – formic acid 200:25:50:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating until the zones are visible in daylight; 8) for Herba Equiseti Hiemalis, with cyclohexane – ethyl acetate – formic acid 20:10:1, detection by spraying with 5 % aluminium chloride in ethanol and viewing under UV 366 nm; 9) for Cuscuta chinensis Lam., with ethyl acetate – butanone – formic acid – water 11:1:1:1, detection by spraying with 5 % aluminium chloride in ethanol and heating at 105 °C until the zones are visible, and viewing under UV 254 nm; 10) for Rehmannia glutinosa Libosch, with chloroform – methanol – ammonia 40:10:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C until the zones are visible in daylight; 11) for Rhizoma Atractylodis Macrocephalae, with cyclohexane – ethyl acetate 7:3, detection by spraying with 5 % p-dimethylaminobenzaldehyde in sulfuric acid – ethanol 1:10 and heating at 105 °C until the zones arevisible in daylight; 12) for Radix Glycyrrhizae, with ethyl acetate – formic acid – water 15:3:2, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing under UV 366 nm; 13) for Radix Achyranthis Bidentatae, with chloroform – methanol 30:1, detection by spraying with 5 % phosphomolybdic acid in n-propanol and heating at 110 °C until the zones are visible in daylight.
and Dendranthema indicum, on silica gel containing 1 % NaOH, with ethyl acetate – methanol – water 100:17:10, detection by spraying with 1 % aluminum trichloride in ethanol firstly, then with 5 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible in daylight.
J. of China Pharm. 27 (7), 722-724 (2013). Xihuang Wan pill is a herbal TCM prescribed for treatment and adjuvant therapy of various cancers. Huoxue Zhitong San powder is a herbal TCM prescribed for traumatic injury and ecchymoma. In the drug market fraud rosin was found to be added to the key ingredient olibanum. For quality control, HPTLC of the sample extracts and the standards acetyl-11-keto-beta-boswellic acid (AKBA), 11-keto-beta-boswellic acid (KBA), beta-boswellic acid (beta-BA), acetyl-beta-boswellic acid (beta-ABA), and abietic acid (LOD=1.0 µg), on silica gel with toluene – ethyl acetate – heptane – formic acid 80:20:10:3 with chamber saturation for 20 min, detection 1) under UV 254 nm and UV 366 nm; 2) by spraying with a fresh solution of anisaldehyde – sulfuric acid – acetic acid 1:10:1000 and heating at 105 °C until the zones were visible in daylight. Verification of abietic acid from added rosin by HPLC. The method was used for the analysis of 63 batches of Xihuang Wan pills sampled from 13 pharmaceutical factories and 10 batches of Huoxue Zhitong San powder from 4 factories.
J. of China Pharm. 22 (3), 13-15 (2013). Gushangling Jiaonang capsule is a herbal TCM for post traumatic functional recovery, prescribed to treat muscle atrophy, bone hyperplasia, neck and lumbar diseases, nerve injuries etc. For quality control, HPTLC on silica gel 1) for Paeonia lactiflora Pall., with chloroform – ethyl acetate – methanol – formic acid 200:25:50:1, detection by spraying with 3 % vanillin in sulfuric acid – water 1:200 and heating mildly until the zones are visible in daylight; 2) for Angelica sinensis, with n-hexane – ethyl acetate – 9:1, detection under UV 366 nm; 3) Astragalus membranaceus (Fisch.) Bunge., with chloroform – methanol – water 13:7:2, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible in daylight.
Mod. Chinese Med. 3, 232-236 (2014). Shuanghuang Tongfeng Jiaonang capsules are a TCM preparation for the treatment of hyperuricemia. For quality control, TLC on silica gel (1) for Paeonia veitchii and the standard paeoniflorin, with chloroform – ethyl acetate – methanol – formic acid 200:25:50:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C until the zones are visible under white light; (2) for Astragalus membranaceus (Fisch.) Bunge. and the standard astragaloside A, with the lower phase of chloroform – methanol – water 13:6:2 after placing at a temperature lower than 10 °C for a night, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible under white light; (3) for Cortex Fraxini and the standards esculin hydrate and esculetin, with chloroform – methanol – formic acid 20:5:1, detection at UV 366 nm. Quantification of astragaloside A by HPLC.
salina, and NMR profiles of extracts of lichens collected from Brazil and Antarctica. Quim. Nova. 37, 1015-1021 (2014). TLC of (1) atranorin, (2) salazinic, (3) barbatic, (4) alpha-alectoronic, (5) alpha-collatolic, (6) cryptochlorophaeic, (7) caperatic, (8) lobaric and (9) protolichesterinic acids in six lichen species named Parmotrema cetratum (Ach.) Hale (I), Parmotrema wainioi (A. L.Smith) Hale (II), Canoparmelia cryptochlorophaea (Hale) (III), Parmotrema mesotropum (Müll. Arg.) Hale (IV), Cladia aggregata (Sw.) Nyl. (V) and Stereocaulon alpinum Laurer (VI), on silica gel with toluene - ethyl acetate - acetic acid 6:4:1 for (I, IV and V) and toluene - acetic acid 17:3 for (II, III and VI). Detection by spraying with p-anisaldehyde - sulfuric acid, followed by heating at 110 ºC. The hRF values of (1) and (2) in (I) were 73 and 33, respectively, whereas the value of (3) and (4) in (II) were 15 and 36; the value of (1) in (III) was 71. DPPH radical scavenging activity was also investigated.
Journal of Pharmacognosy and Phytochemistry 4 (2), 1-4 (2015). HPTLC of petroleum ether and ethanol extracts of aerial parts of Blumea lacera D.C. (Asteraceae), collected in the Gorakhpur district, with chloroform - benzene - formic acid 15:5:3. Evaluation in daylight revealed 11 zones, at least 9 of them at hRf between 3 and 47. The ethanol extract was purified by washing with water, chloroform and ethyl acetate successively, and then by fractionation on a silica gel (60-120 mesh) column; the benzene subfraction yielded, after exposure to iodine vapor, one yellow zone (hRf 41), identified (by IR, NMR and MS) as 3,5-dihydroxy-3’-methyl-6,7,4’-trimethoxyflavanone.
J. Ethnopharmacol. 181, 236-251 (2016). Analysis of the botanical description, geographical location, traditional and medicinal uses, phytochemistry and pharmacological investigation, toxicological aspects, patent information and clinical studies of Symplocos racemosa. The review described methods for the determination of loturine in the bark extracts of Symplocos racemosa on silica gel with chloroform – acetonitrile – triethylamine 7:5:2, quantitative determination by absorbance measurement at 280 nm.