Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      117 121
      Optimization of TLC method for separation and determination of ziprasidone and its impurities
      D. OBRADOVIC, S. FILIPIC, K. NIKOLIC, M. CARAPIC, D. AGBABA* (*Department of Pharmaceutical Chemistry, Faculty of Pharmacy, University of Belgrade, Vojvode Stepe
      450, Belgrade 11000, Serbia, danica@pharmacy.bg.ac.rs)

      J. Liq. Chromatogr. Relat. Technol. 39, 271-276 (2016). HPTLC of ziprasidone and its impurities on silica gel with toluene – methanol – glacial acetic acid 15:1:1. Quantitative determination by absorbance measurement at 250 and 320 nm. The hRF value was 42 for ziprasidone and 19, 28, 31, 58 and 70 for its impurities. LOQ of impurities was 25 ng/zone. Recovery was between 94.9 and 106.7 %. See also J. Planar Chromatogr. 29, 239-246 (2016).

      Classification: 32a
      119 102
      Simultaneous densitometric analysis of amlodipine, hydrochlorothiazide, lisinopril, and valsartan by HPTLC in pharmaceutical formulations and human plasma
      J. PANDYA, M. SANYAL, P. SHRIVASTAV* (*Department of Chemistry, School of Sciences, Gujarat University, Navrangpura, Ahmedabad, Gujarat, India, pranav_shrivastav@yahoo.com)

      J. Liq. Chromatogr. Relat. Technol. 40, 467-478 (2017). HPTLC of lisinopril (1), amlodipine (2), valsartan (3) and hydrochlorothiazide (4) in pharmaceutical formulations and in human plasma on silica gel with methanol – dichloromethane – glacial acetic acid 90:10:1. Quantitative determination by absorbance measurement at 215 nm. The hRF values for (1) to (4) were 29, 56, 67 and 75, respectively. Linearity was between 400 and 2000 ng/zone for (1), 200 and 1500 ng/zone for (2), 1000 and 7000 ng/zone for (3) and 300 and 1500 ng/zone for (4). LOD and LOQ were 83 and 252 ng/zone for (1), 54 and 164 ng/zone for (2), 156 and 474 ng/zone for (3) and 77 and 234 ng/zone for (4), respectively. The intermediate precision was <3 % (n=6). Recovery rate ranged from 99.3 to 100.9 % for (1-4).

      Classification: 32a
      122 065
      Development and validation of simplified high-performance thin-layer chromatography densitometric methods for the determination of sulfalene, sulfadoxine, and pyrimethamine
      Y. MWALWISI, L. HOELLEIN, D. SHEWIYO, U. HOLZGRABE, E. KALLE* (*School of Pharmacy, Muhimbili University of Health and Allied Sciences, Upanga West, P.O. Box 65545/11103 Dar es Salaam, Tanzania, elia.kaale@muhas.ac.tz)

      J. Planar Chromatogr. 31, 290-296 (2018). HPTLC of sulfadoxine (1), sulfalene (2), and_x000D_ pyrimethamine (3) on silica gel with toluene - ethyl acetate - methanol 100:56:43. Quantitative determination by absorbance measurement at 254 nm. Linearity was between 1 and 3 μg/zone for (1) and (2), and 0.05 and 0.15 μg/zone for (3). LOD was 0.107 ng/zone for (1), 0.04 ng/zone for (2) and 1.62 ng/zone for (3), and LOQ was 0.32 ng/zone for (1), 0.13 ng/zone for (2) and 4.92 ng/zone for (3). The intermediate precision was <4 %. Average recovery was 98.0 % for (1), 97.2 % for (2) and 101.8 % for (3).

      Classification: 28a, 32a
      55 126
      Identification of a propantheline analog in propantheline bromide tablets
      B. FORD, A. WALL, M. JOHNSTON, A. LEA

      J.A.O.A.C. 67, 934-939 (1984). TLC of xanthone, propantheline, xanthonoic acid, 9-hydroxy propantheline, methyl xanthanoate, methyl 9-hydroxy-xanthanoate on silica with 1,2-dichloroethane - methanol - formic acid 80:20:2 and 1,2-dichloroethane - methanol 98:2. Detection by UV 366 nm.

      Keywords: quality control
      Classification: 32a
      56 161
      Application of principal components analysis to TLC data for 596 basic and neutral drugs in four eluent systems
      G. MUSUMARRA, G. SCARLATA, G. ROMANO, S. CLEMENTI, S. WOLD

      J. Chromatogr. Sci. 22, 538-547 (1984). Principal component analysis (PCA) with Rf values for 596 basic and neutral drugs in 4 eluent mixtures on silica. Two-component model explaining 77 % of the total variance. Each drug is characterized on a plane by two principal component scores. For the identification of unknowns the method provides a drastically reduced short list of possible candidates. The 4 eluent systems are: a) methanol - NH3 100:1.5, b) cyclohexane - toluene - diethylamine 75:15:10, c) chloroform - methanol 9:1, d) acetone.

      Classification: 2c, 32a
      57 160
      Chinese J
      Y. FU

      of Antibiotics (Kangshengsu) 10, 63 (1985). (Chinese). (Determination of erythromycins by TLC-spectrophotometric method.) TLC of erythromycins A and C with dichloromethane - ethyl acetate - benzene - ethanol 3:4:2:1. Elution of the spots with ethanol. Treatment of the eluates with sulfuric acid solution at 50 °C for 10 minutes. Quantification of eluate by spectrophotometry at 485 mm.

      Classification: 32a
      58 151
      Simple separation of adenosine-5'-phosphosulfate, adenosine-5'-phosphoramidate and cyclic adenosine-5'-monophosphate nucleotides involved in adenosine-5'- phosphosulfate degradation
      F. KRAUSS, A. SCHIDT

      J. Chromatogr. 348, 296-298 (1985). TLC of the title compounds on silica with 2-propanol -25 % NH3 - ethanol 6:3:1. Detection by UV 254 nm. Nucleotides with 2 negative charges did not migrate.

      Classification: 21, 32a
      61 215
      Synthesis of 1-(3-amino-2-propanolo)-5,5-diphenyl-hydantoin derivatives as potential antiarrhythmic agents
      K. KIEC-KONONOWICZ*, A. ZEJC, G. CHLON, E. STYPULA, J. KRUPINSKA, (*Departm. of Pharmaceutical Chemistry, Medical Academy, 30-065 Kraków, Poland)

      Acta Pharm. Jugoslavica 37, 123-130 (1987). TLC on silica with benzene - acetone 40:3 or n-butanol - formic acid - water 7:2:2 or ethyl acetate - chloroform 1:1. Detection under UV 254 nm.

      Classification: 32a