Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      112 086
      A validated high-performance thin-layer chromatography method for the identification and simultaneous quantification of six markers from Platanus orientalis and their cytotoxic profiles against skin cancer cell lines
      I. KHAN, P. SANGWAN*, A. DAR, R. RAFIQ, M. FARRUKH, J. DHAR, S. TASDUQ, S. KOUL (*Bioorganic Chemistry Division, CSIR - Indian Institute of Integrative Medicine, Jammu, Jammu and Kashmir, India, skoul@iiim.res.in)

      J. Sep. Sci. 36, 2602-2610 (2013). HPTLC of betulinic acid (1), betulinic acid-3-acetate (2), 3-acetylbetulinaldehyde (3), oleanolic acid-3-acetate (4), 3-beta-hydroxy-28,19-beta-olenolide (5), and beta-sitosterol (6) in the bark of Platanus orientalis on silica gel with n-hexane - toluene - acetone 12:7:2. Detection by dipping into a ceric ammonium sulfate reagent, followed by heating at 105-110 ºC for 5-10 min. Quantitative determination by absorbance measurement at 420 nm for (1), at 550 nm for (2, 3) and at 500 nm for (4–6). The hRf values for compounds (1) to (6) were 16, 42, 85, 37, 25 and 29, respectively. Linearity was in the range of 100-600 ng/zone for (1) to (6). LOD and LOQ were 60 and 100 ng/zone for (1), 80 and 100 ng/zone for (2), 70 and 90 ng/zone for (3), 40 and 80 ng/zone for (4), 100 and 100 ng/zone for (5) and 60 and 90 ng/zone for (6), respectively. Recoveries were in the range of 95-99 % for all the analytes. Intermediate intra- and inter-day precision was below 2 % (n=3).

      Classification: 32e
      112 105
      (Study on the method for the analysis of Polygonum multiflorum Thunb
      L. SONG (Song Li)*, H. LIU (Liu Haijing), R. QIAO (Qiao Rongxia) (*Shanxi Provin. Inst. for Food & Drug Contr., Shanxi, Xi’an 710061, China)

      in Shanhaidanpian tablets) (Chinese). J. of China Pharm. 26 (9), 997-999 (2012). Shanhaidanpian tablets are a herbal TCM preparation for the treatment of poor blood flow, blood stasis and chest pain syndrome. For quality control, TLC on silica gel with toluene – ethyl acetate – formic acid 20:2:1, detection by exposure to vapors until the zones are visible in daylight. Quantitative determination of 2,3,5,4’-tetrahydroxystilbene-2-O-beta-D-glucoside by HPLC.

      Classification: 32e
      112 125
      (Study of the method for the quality control of Fufang Xiaoji Zhike Milian Gao ointment) (Chinese)
      M. ZHANG (Zhang Ming), Y. NI (Ni Ying), W. JIN (Jin Weihua), K. FAN (Fan Kaihua)* (* Dep. of Pharm., General Hosp. of Chengdu Milit. Area Command Sichuan, Chengdu 610083, China)

      Chinese J. of Med. Guide 10 (20), 99-102 (2013). Fufang Xiaoji Zhike Milian Gao ointment is herbal TCM preparation for clearing the body heat caused by inflammation, resolving phlegm and relieving asthma. For quality control, TLC on silica gel 1) for Pericarpium Citri Reticulatae and the standard hesperidin, first over 3 cm with ethyl acetate – methanol – water 99:17:13 and thenover 8 cm with toluene – ethyl acetate – formic acid – water 95:45:5:3, detection by spraying with 2 % aluminium chloride in ethanol and viewing under UV 366 nm; 2) for Schisandra Chinensis and the standard schizandrin A, with the upper phase of petroleum ether (30-60 °C) – ethyl formate – formic acid 15:5:1, detection under UV 254 nm; 3) for Crataegus pinnatifida and the standard ursolic acid, with toluene – ethyl acetate – formic acid – water 39:8:2:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 80 °C, detection under UV 366 nm. Quantification of tenuifolin by HPLC.

      Classification: 32e
      113 072
      Simultaneous estimation of kaempferol, rutin, and quercetin in various plant products and different dosage
      forms of Bhuiamla and Amla
      S. JIRGE, P. TATKE*, S. GABHE (*Shah College of Pharmacy, S.N.D.T. Women’s University, Mumbai 400 049, India, patatke@gmail.com)

      J. Planar Chromatogr. 27, 267-273 (2014). HPTLC of kaempferol (1), rutin (2), and quercetin (3) in marketed formulations containing_x000D_ Phyllanthus niruri (Bhuiamla) and Emblica officinalis (Amla) on silica gel with chloroform - methanol - formic acid 82:15:10. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (3) were 69, 53 and 12. Linearity was in the range of 21-840 ng/zone for (1), 56-1008 ng/zone for (2) and 60-1800 ng/zone for (3), respectively. The intermediate/interday/intra-day precisions were below 1 % (n=3). The LOD and LOQ were 21 and 63 ng/zone for (1), 56 and 168 ng/zone for (2) and 300 and 600 ng/zone for (3), respectively. Recoveries for (1) to (3) were obtained in the range of 81.8-119.0 %.

      Classification: 32e
      113 089
      Quantitative estimation of artesunate and amodiaquine HCl by high-performance thin-layer chromatography method in bulk and pharmaceutical formulations
      P. RAUT, A. SHARMA, G. AGARWAL, S. CHARDE* (*Department of Pharmacy, Faculty Division-III, Birla Institute of Technology and Science, Pilani 333 031, Rajasthan, India, shrikanthcharde@bits-pilani.ac.in)

      J. Liq. Chromatogr. Relat. Technol. 37, 1568-1582 (2014). HPTLC of artesunate (1) and amodiaquine (2) on silica gel with acetonitrile – water – ammonia 40:7:2. Quantitative determination by absorbance measurement at 366 nm. The hRf values for (1) and (2) were 44 and 50, respectively. Linearity was in the range of 100-600 ng/zone for (1) and 50-300 ng/zone for (2). The intermediate/interday/intra-day precisions were below 2 % (n=9). The LOD and LOQ were 25 and 60 ng/zone for (1) and 12 and 30 ng/zone for (2), respectively. Recovery was 98.1-99.9 % for (1) and 99.3-100.9 % for (2).

      Classification: 32e
      113 111
      High-performance thin-layer chromatographic quantification of three active compounds from the decoction of abnormal Savda Munziq prescription
      X. ZHANG (Zhang Xuejia), J. LI (Li Jie), H. UPUR, S. TIAN (Tian Shuge)* (*Xinjiang Key Laboratory of Molecular Biology and Endemic Diseases, Collegeof TCM, Xinjiang Medical University, Urumqi 830011, China, tianshuge@hotmail.com)

      J. Planar Chromatogr. 27, 186-191 (2014). HPTLC of rutin (1), rosmarinic acid (2), and glycyrrhizin (3) in the medicinal preparation Savda Munziq on silica gel with ethyl acetate - formic acid - acetic acid - water 30:2:2:3. Quantitative determination by absorbance measurement at 250 nm. The hRF values for (1) to (3) were 16, 86 and 9, respectively. Linearity was in the range of 128-2048 ng/zone for (1), 322-5144 ng/zone for (2) and 70-1120 ng/zone for (3), respectively. The intermediate/inter-day/intra-day precisions were below 3 % (n=3). The LOD and LOQ were 37 and 124 ng/zone for (1), 38 and 127 ng/zone for (2) and 33 and 111 ng/zone for (3), respectively. Recovery for (1) to (3) was in the range of 95.4-104.0 %.

      Classification: 32e
      114 061
      (Study of the method for the quality control of Danggui Buxue Wan pills) (Chinese)
      X. BI (Bi Xiaoli)*, Q. CHENG (Cheng Qingyun), S. LI (Li Sumei) (*Guangdong Prov. Inst. of TCM, Guangdong, Guangzhou 510095, China)

      Shanxi J. Trad. Chinese Med. 9, 43-46 (2013). Danggui Buxue Wan pill is TCM compound for the treatment of psoriasis (blood dryness type), chronic eczema, neurodermatitis, skin pruritus and other skin diseases. For the quality control, TLC on silica gel (1) for Angelica sinensis with cyclohexane – dichloromethane – ethyl acetate – formic acid 4:1:1:0.1, detection at UV 366 nm; (2) for Fallopia multiflora (Thunb.) Harald. with the upper phase of toluene – ethyl acetate – formic acid 20:2:1, detection at UV 366 nm; (3) for Paeonia lactiflora Pall. with chloroform – ethyl acetate – methanol - formic acid 45:5:10:0.2, detection by spraying with 5% vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C until the spots were visible. All were identified by fingerprint comparison with the standard (paeoniflorin or ferulic acid) and/or the standard ingredient drug.

      Classification: 4d, 32e
      114 082
      (Studies of the method for the quality control of Sangao Tiaohe Wan pills) (Chinese)
      W. LIU (Liu Wenlong), Y. HUANG (Huang Yuyan)* (*Dongyuan Health school, Guangdong, Dongguan 523186, China)

      Chinese J. Mod. Drug Appl. 7 (13), 4-6 (2013). Sangao Tiaohe Wan pill is TCM compound for the treatment of high blood pressure, high blood lipids, diabetes mellitus, vasculitis, etc. For quality control, TLC on silica gel (1) for Salvia miltiorrhiza Bunge and tanshinone ll A with benzene – ethyl acetate 19:1, detection under white light; (2) for Panax pseudoginseng, notoginsenoside R1, ginsenoside Rb1 and ginsenoside Rg1 with chloroform - ethyl acetate – methanol – water 15:40:22:10, detection by spraying with 10 % sufuric acid in ethanol and heating at 105 °C until the spots were visible. Quantitation of tanshinone ll A by HPLC.

      Classification: 4d, 32e
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