Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      110 075
      An improved method for the extraction and quantitation of diosgenin in Tribulus terrestris L
      V. GHOSH, S. BHOPE*, V. KUBER, A. SAGULATE (*Department of Analytical Development (R&D), Tulip Lab Pvt. Ltd. F-20=21, MIDC Ranjangaon, Pune 412220, India, bshrinivas16@gmail.com)

      J. Liq. Chromatogr. Relat. Technol. 35, 1141-1145 (2012). HPTLC of diosgenin in various parts of Tribulus terrestris L. on silica gel with toluene - ethyl acetate - methanol 7:3:1. Detection by dipping in anisaldehyde reagent consisting of anisaldehyde - acetic acid - sulfuric acid - methanol 1:20:10:170, followed by heating at 110 °C for 2 min. Quantitative determination by absorbance measurement at 430 nm. The hRf value of diosgenin was 48 and selectivity regarding matrix was given. Linearity was between 50 and 240 ng/zone. The method provides acceptable intra-day and inter-day precision for diosgenin. The limits of detection and quantification were 2 and 7 ng/spot, respectively. Recovery (by standard addition) was 100.6 %. The method provided comparable results with HPLC.

      Classification: 32e
      110 092
      (Identification of Phyllanthus niruri Linn
      C. LI (Li Cai Dong)*, Y. LIANG (Liang Yun), W. ZHANG (Zhang Wei), B. WU (Wu Bin) (*Inst. of Hepatology, Lanzhou Municip. People's Hosp. No. 2, Gansu, Lamzhou 730046,China)

      and quantitative determination of gallic acid in Zhuqi Fugan granules) (Chinese). Chinese J. of Inform. on TCM 19 (4), 47-48 (2012). Zhuqi Fugan granules, a herbal TCM preparation, are effective for clearing heat and removing toxicity, nourishing the liver, and strengthening the body resistance and are clinically prescribed to cure viral hepatitis type B. For quality control, TLC of the extracts of the preparations on silica gel with cyclohexane – chloroform – ethyl acetate 4:1:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 ° until the zones are visible.

      Classification: 32e
      110 113
      (Study of the method for differentiation of the dyes adulterated in Safflower) (Chinese)
      CH. MIN (Min Chunyang), L. FU (Fu Lingyan), Q. WANG (Wang Qi), J. LU (Lu Jing)* (*National Inst. for Food & Drug Contr., Beijing 100050, China)

      J. of China Pharm. 25 (8), 772-775 (2011). Safflower, the dried flower of Carthamus tinctorius L. is a herbal TCM drug for invigorating the circulation of blood, stimulating the menstrual flow, dissipating blood stasis, relieving pain, and is prescribed clinically to cure amenorrhea, falling injuries and skin and external diseases. Due to the lack of the source some counterfeits have been found on the market in recent years. The methods were studied for differentiating the dyes used by the market for adulteration of safflower. For dyes, TLC of the extracts of the crude drugs on silica gel firstly with chloroform – methanol – glacial acetic acid 7:1:2, detection under daylight for identification of orange, then with ethyl acetate – n-butanol – ethanol – ammonia – water 1:3:3:1:1, detection under daylight for identification of acid red 73, lemon yellow and carminum respectively. Results obtained by HPLC were compatible with those obtained by TLC.

      Classification: 32e
      110 140
      High-performance thin-layer chromatographic quantification of kaempferol and apigenin in the whole-plant powder of Sida spinosa Linn
      L. SAWANT*, Y. KACHWALA, P. SANGAVE, N. PANDITA (*School of Pharmacy and Technology Management, SVKM’s NMIMS, Vile Parle (W), Mumbai-400056, India, laxmanpsawant@gmail.com)

      J. Planar Chromatogr. 25, 301-305 (2012). HPTLC of kaempferol (1) and apigenin (2) in the whole-plant powder of Sida spinosa Linn. on silica gel with dichloromethane - methanol - formic acid 16:2:1. Quantitative determination by absorbance measurement at 340 nm. Linearity was in the range of 150-450 µg/mL for (1) and 50-150 µg/mL for (2). The intermediate/inter-day/intra-day precision was below 2 %. Recovery was 99.5 % for (1) and 99.3 % for (2).

      Classification: 32e
      110 159
      (Study on the method for the identification of Saxifraga stolonifera (L
      CH. XIAN (Xian Chun), X. GONG (Gong Xiaojian)*, ZH. YANG (Yang Zhannan) (*Key Lab. for Inform. System of Mountainous Areas & Protection of Ecological Environment, Guizhou Norm. Univ., Guizhou, Guiyang, 550001, China)

      by thin-layer chromatography) (Chinese). J. of Guizhou Normal Univ. (Natural Sci.) 30 (3), 7-8 (2012). Saxifraga stolonifera (L.) Meerb is a TCM herb for heat-clearing and detoxification and is often used as the key component in the preparations for curing otitis media, traumatic bleeding and hyperplasia of the prostate. TLC of the extracts of the whole medicinal herb and gallic acid as standard on polyamide phase with chloroform – methanol – formic acid 25:5:1, detection by spraying with a solution of ferric chloride – 2N hydrochloric acid – water 2:1:100 and heating until the zones are visible, viewing in daylight.

      Classification: 32e
      110 176
      (Study of the method for the quality control of Tengzi tea) (Chinese)
      Q. ZHAO (Zhao Qizhong)*, Q. ZHAO (Zhao Qian), Q. LI (Li Qinfang), Y. LI (Li Yanju) (*Puer Municip. Inst. for Food & Drug, Yuannan, Puer 665000, China)

      Chinese J. Ethnopharm. (12), 41-42 (2011). Tengzi tea, Ampelopsiscan oniensis (Hook. et Am.) Planch, is an age-old herbal TCM drug for invigorating the circulation of blood, diminishing inflammation, relieving pains and stoping bleeding, and is prescribed clinically to cure colds and rheumatism, and as adjunctive therapy for hypertension and coronary disease. TLC of the extracts of the crude drugs on polyamide phase with chloroform – ethyl acetate – formic acid 10:10:1, detection under UV 366 nm. In addition microscopic differentiation, and determination of the water content by oven drying. Determination of the extract content by cold-maceration and hot-maceration with water, ethanol or diluted ethanol.

      Classification: 32e
      111 072
      (Study of the method for the quality control of Genianan capsules by thin-layer chromatography) (Chinese)
      J. GONG (Gong Ju) (Gaoan Municip Huangshagang health center, Jiangxi, Gaoan 330803, China)

      Chinese J. of Jiangxi Ind. (3), 68-70 (2012). Genianan capsules are a herbal TCM for treating some diseases during women’s menopause such as tinnitus, palpitation, insomnia, blood pressure instability, etc. For quality control, TLC on silica gel 1) Radix Polygoni Multiflori and Caulis Polygoni Multiflori and standard emodin, with toluene – ethyl acetate – formic acid 15:2:1, detection under UV 366 nm; 2) for Fructus Schisandrae Chinensis and the standards deoxyschizandrin and schizandrin B, with petroleum ether (30-60 °C) – ethyl acetate – formic acid 15:5:1, detection under UV 254 nm; 3) for Radix Ophiopogonis, with chloroform – acetone 22:5, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing in daylight; 4) Rhizoma Curculigins and the standard curculigoside, with ethyl acetate – methanol – formic acid 100:10:1, detection by spraying with 0.1 mol potassium ferricyanide – 0.1 mol ferric chloride 1:1 and viewing in daylight.

      Classification: 32e
      111 092
      (Study of the quality control of Chongderi pills) (Chinese) Chinese J
      P. KOU (Kou Peiyan) (Baotou Municip. Test Center for Foods & Pharm., The Inner Mongolia Autonomous Region, Baotou 014030, China)

      of Northern Pharmacy 9 (4), 4-5 (2012) Chongderi pills are a herbal traditional Mongolian medicine for treating diarrhea, invigorating the circulation of blood, stimulating the menstrual flow, and dissipating blood stasis, etc. For quality control, TLC on silica gel 1) for Radix aucklandiae, with benzene – methanol 27:1, detection by spraying with 1% vanillin in sulfuric acid – ethanol, detection under daylight; 2) for Rhizoma acori tatarinowii, with petroleum ether (60-90 º) – ethyl acetate 9:1, detection by exposure to iodine vapors, viewing under daylight; 3) for safflower carthamus, with ethyl acetate – formic acid – water – methanol 35:10:15:2, detection under daylight. Identification by comparison with the standards.

      Classification: 32e
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