Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. The saved items can be printed to PDF using the print function of your web browser.

      126 011
      Quality risk assessment and DoE-based analytical quality by design approach to stability-indicating assay method for acidic degradation kinetic study of apremilast
      P. PRAJAPATI*, H. PATEL, S. SHAH (*Maliba Pharmacy College, Maliba Campus, Uka Tarsadia University, Bardoli, Gujarat 394350, India, pintu.prajapati@utu.ac.in)

      J. Planar Chromatogr. 33, 231-244 (2020). HPTLC of apremilast on silica gel with toluene - methanol - ethyl acetate 7:2:1. Quantitative determination by absorbance measurement at 241 nm. The hRF value for apremilast was 63. Linearity was between 200 and 1000 ng/zone. Inter-day and intra-day precision were below 1 % (n=3). The LOD and LOQ were 4 and 13 ng, respectively. Recovery rate was between 99.7 and 100.0 %. Apremilast was subjected to acidic, alkaline, oxidative, dry heat, neutral, and photolytic degradation conditions. The method was implemented using a quality risk management and quality by design approach for regulatory requirements.

      Classification: 23e
      106 114
      HPLC, TLC, and first-derivative spectrophotometry stability-indicating methods for the determination of tropisetron in the presence of its acid degradates
      L.S. ABDEL-FATTAH, Z. EL-SHERIF, K.M. KILANI, Dalia A. EL-HADDAD* (*National Organization for Drug Control & Research, 6&7 AboHazem St, Pyramids, P. O. Box 29, Giza, Egypt; daliaelhaddad@hotmail.com)

      J. AOAC Int. 93, 1180-1191 (2010). TLC of tropisetron and its acid-induced degradation products on silica gel with methanol - glacial acetic acid 22:3 with chamber saturation for 45 min. Detection under UV light at 254 nm. Quantitative determination by scanning at 285 nm. The hRf values were 44, 84, and 92 for tropisetron and degradates I and II, respectively. Linearity was between 1 and 10 µg/zone. Mean accuracy was 100.2 %. The precision was 0.64 %.The limit of detection and quantification for tropisetron was 0.26 and 0.80 µg/zone, respectively. The intraday and interday precisions were evaluated by assaying freshly prepared samples of tropisetron in triplicate concentrations, i. e. 3, 5, and and 9 µg/zone, resulting in 99.8 %, 100.3 %, and 100.4 %, respectively, for interday precision and 99.7 %, 100.2 %, and 99.7 %, respectively, for intraday precision (with a precision of 0.9 %, 0.6 %, 0.8 % and 0.6 %, 0.4 %, 0.6 %, respectively).

      Classification: 23
      54 089
      Magyar Kemini Folyoirat 90, 124-129 (1984)
      G. KORANYI, E. SZEBENYI-GYOERI, A. VELIN-PRIKIDANOVICS, J. BERLIK

      (Hungarian). (Electrochemical studies on benzimidazole derivatives. I. Anodic oxidation of 2-amino-benzimidazole.) TLC of 2-amino-benzimidazole on silica with chloroform - CCl4 - methanol 8:5:1.

      Keywords:
      Classification: 23
      73 015
      Reversed phase liquid chromatography of some benzimidazole derivatives
      S.M. PETROVIC*, M. ACANSKI, N.U. PERISIC-JANJIC, D.J. VLAOVIC, (*Dept. Anal. Chem., Fac Technol., Univ. Novi Sad, Cara Lazaral, P. O. Box 340, 21000 Novi Sad, Yugoslavia)

      Chromatographia 37, 98-104 (1993). RP TLC of title compounds on RP-18 silica with aqueous NH3 (pH 11.19-11.69) - methanol 25:75. Determination of Rf values and calculation of k values. Study of the retention behavior of the compounds as a function of the pH values. Investigation of the effect of composition of the aqueous phase, the molecular structure of the aqueous phase, and the type of organic modifier on the relationship between the retention constant (log k) and the pH of the aqueous phase.

      Keywords:
      Classification: 2c, 23
      102 071
      Application of topological index and the Rf parameter to the estimation of lipophilic properties of selected porphyrins
      Marzena PODGÓRNA (Institute of Chemistry, Silesian University, 9 Szkolna Street, 40-006 Katowice, Poland)

      J. Liq. Chromatogr. Relat. Technol. 31, 1458-1464 (2008). TLC of porphyrins and four alkoxy porphyrin derivatives on RP-18 with dichloromethane - methanol 3:2 saturated for 30 min. Detection by visual evaluation under white light.

      Classification: 23a
      65 027
      Laser fluorometric detection of porphyrin methyl esters for high-performance thin-layer chromatography
      C.W. HUIE*, W.R. WILLIAMS, (Dep. Chem., State Univ. New York, Binghampton, New York 13910 USA)

      Anal. Chem. 61, 2288-2292 (1989). Description of a new detection method for the determination of porphyrins present in biological materials. Separation of carboxylic acid porphyrins by HPTLC after esterification. Detection by using one of the visible lines of an argon-ion laser for fluorometric excitation. Demonstration of good selectivity and detectability for the determination of porphyrin profiles in human urine. Detection limits in the 18 - 35 pg ranges.

      Keywords:
      Classification: 3f, 23a
      94 041
      TLC and RPTLC separation of porphine, selected porphyrins, and their metalloderivatives
      M. STEFANIAK, P. KUS, J. SLIWIOK* (*Department of Chemistry, Silesian University, 9, Szkolna Street, 40-006 Katowice, Poland)

      J. Planar Chromatogr. 17, 72-74 (2004). TLC of porphine, meso-mono-tert-butylporphyrin, meso-tetra-tert-butylporphyrin and their respective Zn(II), Ni(II), and Cu(II) derivatives on silica gel with n-hexane - chloroform 7:3, and on RP-18 with methanol or methanol - water 9:1 after presaturation of the plates for 30 min. The porphyrins were detected visually.

      Classification: 23a
      61 143
      Indoles in edible members of the cruciferae
      M.E. WALL*, H. TAYLOR, P. PERERA, M.C. WANI, (*Res. Triangle Inst., Res. Triangle Park, North Carolina 27709, USA)

      Journal of Natural Products 51, 129-135 (1988). TLC of indole-3-carboxaldehyde and indole-3-acetonitrile on silica with dichloromethane and with dichloromethane - methanol 95:5 and 90:10. Color reaction after spraying with Ehrlich’s reagent.

      Classification: 23c