Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

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      114 016
      Development and validation of a high-performance thin-layer chromatographic–densitometric method for the quantification of swertiamarin in traditional bitters and formulations
      J. AHAMAD, Naila HASSAN, Saima AMIN, S. R. MIR* (*Phyotpharmaceutical Research Laboratory, Faculty of Pharmacy, Hamdard University, PO Hamdard Nagar, New Delhi, India, showkatrmir@gmail.com)

      J. Planar Chromatogr. 28, 61-66 (2015). HPTLC of swertiamarin in extracts of Enicostemma littorale and Swertia chirata on silica gel with ethyl acetate – methanol – water 16:3:1. Quantitative determination by absorbance measurement at 246 nm. The hRF value of swertiamarin was 58. Linearity was between 200 and 1200 ng/zone. The intermediate intra-day and inter-day precisions were below 2 % (n=6). The LOD and LOQ were 38 and 115 ng/zone, respectively. Recoveries were in the range of 98-100 %.

      Classification: 8b, 32e
      118 037
      Chemical fingerprinting and quantification of biomarker wedelolactone in different sources of “Bhringaraja” by high-performance thin-layer chromatography and method validation
      K. HULLATI*, A. RODRIGUES, V. MANNUR, V. MASTIHOLIMATH, V.K. RASAL (*KLE
      University, Nehru Nagar, Belagavi, Karnataka 590 010, India, drhullatti@klepharm.edu)

      J. Planar Chromatogr. 29, 330-335 (2016). HPTLC of wedelactone in Eclipta alba, Wedelia calendulacea and Wedelia trilobata on silica gel with toluene – chloroform – ethanol – formic acid 10:8:2:1. Quantitative determination by absorbance measurement at 351 nm. The hRF value for wedelactone was 29. Linearity was between 80 and 280 ng/zone. The intermediate precision was below 2.5 % (n=3). The LOD and LOQ was 0.36 and 1.09 ng/zone, respectively. Recoveries were between 99.4 and 100.3 %.

      Classification: 8b
      121 030
      Four new xanthones from Cratoxylum cochinchinense and their in vitro antiproliferative effects
      C. ITO, T. MATSUI*, A. NIIMI, H.T.-W. TAN, M. ITOIGAWA (*Faculty of Pharmacy, Meijo University, Tempaku-ku, Nagoya, Japan; tmatsui@aichi-med-u.ac.jp)

      Planta Med. 83(09), 812-818 (2017). Some of the column subfractions obtained (with different mixtures of hexane – acetone – isopropanol) from an ethyl acetate extract of Cratoxylum cochinchinense twigs and boughs were submitted to a preparative TLC on silica gel for the isolation of the following xanthones and anthracenones: (1) β-mangostin, cochinchinone and cratoxanthone D with chloroform – acetone 10:1, (2) allanxanthone by three-stage elution with benzene – acetone 10:1, n-hexane – ethyl acetate 3:1, and n-hexane – acetone 3:1, (3) cratoxanthone A by similar three-stage elution (third step: chloroform – acetone 10:1), (4) visminone F by two-step elution with benzene – acetone 10:1, and isopropanol – acetone 5:1, (5) cratoxanthone B and garcinone E by a two-step elution with isopropanol – acetone 4:1, and n-hexane – acetone 3:1, (6) α-mangostin and mangostenol by a two-step elution with chloroform – acetone 20:1, and n-hexane – isopropanol – acetone 5:5:1, (7) cratoxanthone C by a two-step elution with benzene – ethyl acetate 5:1, and chloroform – acetone 20:1.

      Keywords: herbal
      Classification: 7, 8b, 15a
      58 049
      (Detection of crown ethers by two-dimensional thin-layer chromatography
      E. BLASIUS, W. KLEIN. Fresenius Z. Anal. Chem. 322, 348-349 (1985)

      Then chromatography in second direction with chloroform - acetone 8:2. Detection by UV and iodine vapor.

      Classification: 8b, 9
      62 058
      Chemistry and Pharmacology of Gentiana Lactea
      D. SCHAUFELBERGER, K. HOSTETTMANN, (Inst. de Pharmacognosie et Phytochimie, UNIL, 2, rue Vuillermet, CH-1005 Lausanne, Switzerland)

      Planta Med. 1988, 219-221. TLC of flavonoids and xanthones on silica with chloroform - methanol - water 70:30:3, cyclohexane - ethyl acetate 1:2 and on polyamide with methanol - acetic acid 50% 9:1. Preparative separation by centrifugal TLC (2 mm silica plates) with toluene - ethyl acetate mixtures.

      Classification: 3d, 8a, 8b
      67 058
      Novel antifungal tetracyclic compounds from Bauhinia rufescens LAM
      M.P. MAILLARD, M.C. RECIO-IGLESIAS, M. SAADON, M. STOECKLI-EVANS, K. HOSTETTMANN*, (*Ecole de Pharmacie, Univ. de Lausanne BEP, CH-1015 Lausanne, Switzerland)

      Helv. Chim. Acta 74, 791-799 (1991). TLC of phenolic tetracyclic compounds on silica with chloroform - methanol 95:5 and HPTLC on RP-18 with methanol - water 8:2 or on diol with ethyl acetate - petrol ether 1:1. Detection by UV 254/366 nm or with Godin reagent. Also bioautography with spores of the plant pathogenic fungus cladosporium cucumerinum. HPTLC on RP-8 and on diol allowed the separation of closely related compounds and transposition to prep. HPLC.

      Classification: 8b
      71 053
      Identification of red sandalwood
      E. HAHN-DEINSTROP, (Heumann Pharma GmbH, Entwicklungsanalytik II, P.O. Box 2260, Heideloffstr. 18-28, D-8500 Nürnberg, Germany)

      J. Planar Chromatogr. 6, 81-83 (1993). TLC of santalin A and B in neutral, acidic, and basic methanol on amino-modified silica with butanol - formic acid - water 19:2:5. Detection under UV 254 and 365 nm. Photodocumentation under UV 254, 366 and daylight illumination.

      Classification: 8b
      76 053
      Antibacterial phloroglucinols and flavonoids from Hypericum brasiliense
      L. ROCHA, A. MARSTON, O. POTTERAT, M.A.C. KAPLAN, H. STOECKLI,EVANS, K. HOSTETTMANN*, (*Inst. de Pharmacogn. et Phytochim., Univ. de Lausanne, BEP, CH-1015 Lausanne, Switzerland)

      Phytochemistry 40, 1447-1452 (1995). TLC of various polyphenols on silica with chloroform and chloroform - methanol 7:3. HPTLC on RP-18 with acetonitrile. Most phloroglucinols gave red spots after spraying with Godin’s reagent. determination of the antibacterial activity against Bacillus subtilis by TLC bioautography on silica.

      Keywords:
      Classification: 8a, 8b