Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

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      58 043
      Adonis alippica Boiss, Phytochemische Untersuchungen, Isolierung und Strukturaufklärung von Cardenoliden
      P.JUNIOR, D. KRUEGER, C. WINKLER

      (Adonis aleppica Boiss. Phytochemical investigation, isolation and structure elucidation of cardenolides). Dtsch. Apoth. Ztg. 125, 1945-1949 (1985). Separation of cardenolidaglycones (digitoxigenine, 3-epi-periplogenine, strophanthidine, strophantidol, adonioxigenine, adonitoxoligenine, strophandogenine) on silica with chloroform - methanol - water 80:19:1, after treatment with HCl on the plate. Detection with vanillin-sulfuric acid.

      Classification: 8b
      62 054
      Nachweis und Bestimmung des Süssstoffs Acesulfam-K in Lebensmittelzubereitungen
      G. LEHMANN, B. BINKLE, S. ZU WEMMER, (Fachber. Anal. Biol. Chem., Univers., D-6600 Saarbrücken, FRG)

      (Detection and determination of the sweetener Acesulfam-K in food preparations). Lebensmittelchem. Gerichtl. Chem. 41, 113-114 (1987). TLC on polyamide-cellulose with xylene - propanol - acetic acid - conc. formic acid 45:6:7:2. Detection with 0.2% methanolic dichlorofluorescein.

      Classification: 8b
      67 052
      Biotransformation of Podophyllum lignans in cell suspension cultures of Forsythia intermedia
      A.J. BROOMHEAD, P.M. DEWICK*, (*Dept. of Pharmaceutical Sciences, University of Nottingham, Nottingham, NG7 2RD, UK)

      Phytochemistry 30, 1511-1517 (1991). TLC of podophyllotoxin and related derivatives on silica with chloroform - methanol 10:1. Detection by UV or with acetic acid - conc. HNO3. Excellent preparative separation of two closely related podophyllotoxin derivatives. by preparative TLC on silica with ether. Elution of the TLC zones with acetone.

      Classification: 8b
      70 064
      Retention behavior of closely related coumarins in thin-layer chromatographic preassays for high-performance liquid chromatography according to the „PRISMA“ model
      P. HÄRMÄLÄ, (Pharmacognosy Div., Dept. of Pharm., Univ. of Helsinki, SF-001 70 Helsinki, Finland)

      J. Chromatogr. 593, 329-337 (1992). Study of the retention behavior of 14 closely related coumarins in normal-phase TLC and HPLC with the aim of testing the suitability of TLC as a pre assay of HPLC when the optimization of the mobile phase has been carried out according to the PRISMA system. Measurement of the retention in TLC and HPLC at 37 and 13 selective points, respectively. Two and three dimensional evaluations of capacity factor k' against selectivity points showed similar retention behavior for the coumarins in TLC and HPLC. Discussion of the dependency of k' on the change in solvent strength.

      Keywords:
      Classification: 2e, 8b
      75 135
      Anthocyanins of Cephaelis Cynomorium, Enterpe, Lavatera and Pinanga
      J.B. HARBORNE*, N. SAITO, C.H. DETONI, (Dept. of Bot., Univ., of Reading, Whiteknights, Reading, RG6 2AS, UK)

      Biochemical Systematics and Ecology 22, 835-836 (1994). TLC of malonylated malvidin glycosides, cyamidin-3-glucoside and cyanidin-3-rutinoside on microcrystalline cellulose with butanol - 2N hydrochloric acid 1:1 or acetone - hydrochloric acid - water 15:3:82.

      Classification: 8b, 30b
      83 040
      Identification of coumarins from the fruit of citrus hystrix DC as inhibitors of nitric oxide generation in mouse macrophage RW 264
      A. MURAKAMI, G. GAO, OE KYUNG KIM, M. OMURA, M. YANO, C. ITO, H. FURUKAWA, S. JIWAJINDA, K. KOSHIMIZU, H. OHIGASHI* (Div. of Appl. Life Sci., Graduate School of Agr., Kyoto Univ., Kyoto 606 - 8502, Japan)

      J. Agric. Food Chem. 47, 333-339 (1999). Preparative TLC of coumarins (i.a. bergamottin, oxypencedanin, 5-[(6',7'-dihydroxy-3',7'-dimethyl-2-octenyl)oxy]psoralen) on silica gel with ethyl acetate - n-hexane 1:10.

      Keywords:
      Classification: 8b
      88 045
      Isolation of (+)-catechin from oak bark by fractionation of its extract on Extrachrom (R)
      B. SIMONOVSKA*, I. VOVK, S. ANDRENSEK, T. YRJÖNEN, P. VUORELA, H. VUORELA, (*Nat. Inst. of Chem., Lab. for Food Chem., Hajdrihova 19, Sl-1000 Ljubljana, Slovenia)

      Proc. Intern. Symp. on Planar Separations, Planar Chromatography 2001, pp. 335-341. Isolation of (+)-catechin by rotating chromatography on silica gel with toluene - ethyl acetate - formic acid 35:15:1. TLC on silica gel with ethyl acetate - water - formic acid 17:3:2 resp. n-hexane - ethyl acetate - formic acid 20:19:1. Detection under UV 366 nm (flavonoids, phenolic acids), spraying with vanillin/phosphoric acid reagent (catechins, proanthocyanidins) and spraying with 1,1-diphenyl-1-picrylhydrazyl (antioxidants). Videodocumentation at 366 nm.

      Keywords:
      Classification: 8b, 32e
      93 016
      An LC/DAD-UV/MS method for the rapid detection of aristolochic acid in plant preparations
      J.-R. Ioset, G. E. Raoelison, K. Hostettmann* (*Institute de Pharmacognosie et Phytochimie, B. E. P., CH-1015 Lausanne, Switzerland)

      Planta med. 68, 856-858 (2002).TLC of aristolochic acid on silica gel with chloroform - methanol - acetic acid 13:4:1 before submitting to a second migration on RP-18 with methanol - water 7:13. Detection by spraying with diphenylamine reagent (0.5 % diphenylamine in 60 % sulfuric acid) followed by heating for 10 min at 100 °C. Detection limit 1 µg in visible light and 0.2 µg under UV light at 366 nm.

      Classification: 8b, 11a