Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      128 055
      Development and validation of HPTLC method for simultaneous estimation of bioactive components in combined extracts of three hepatoprotective plants
      S. MEHTA, A. KUMAR, R. SINGH* (*Department of Pharmaceutical Chemistry, Shivalik College of Pharmacy, Nangal, 140126, Punjab, India, rksingh244@gmail.com)

      J. Liq. Chromatogr. Relat. Technol. https://doi.org/10.1080/10826076.2021.1939046 (2021). HPTLC of picroside-I (1), andrographolide (2) and silybin (3) in Picrorhiza kurroa (roots), Andrographis paniculata (aerial parts) and Silybum marianum (seeds), respectively, on silica gel with n-butanol - glacial acetic acid - water 6:1:3. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (3) were 49, 68 and 89, respectively. Linearity was between 60 and 600 ng/zone for (1) to (3). The intermediate precision was below 2 %. The LOD and LOQ were 15 and 45 ng/zone for (1), 22 and 67 ng/zone for (2) and 26 and 78 ng/zone for (3), respectively. Recovery was between 99.7 and 103.7 % for (1), 99.7 and 101.1 % for (2) and 99.0 and 101.7 % for (3).

      Classification: 8a, 8b
      127 014
      Rapid identification and comparison of compounds with antioxidant activity in Coreopsis tinctoria herbal tea by High-Performance Thin-Layer Chromatography coupled with DPPH bioautography and densitometry
      S. LAM, S. LAM, J. ZHAO (Zhao Jing)*, S. LI (Li Shao Ping) (*State Key Laboratory of Quality Research in Chinese Medicine, Inst. of Chinese Medical Sciences, Univ. of Macau, Macao, jingzhao@umac.mo)

      J. Food. Sci. 81, 2218-2223 (2016). HPTLC of Coreopsis tinctoria samples on silica gel with toluene - ethyl acetate - formic acid - water 9:20:6:3. DPPH bioautography assay by spraying with 0.04 % 2,2-diphenyl-1-picrylhydrazyl in methanol under dark conditions. Detection under UV light at 535 nm. The hRF values for the antioxidant compounds were 30 for flavanomarein, 37 for marein and chlorogenic acid, 45 for 5,7,3',5'-tetrahydroxyflavanone-7-O-glucoside, 62 for 3,5-dicaffeoylquinic acid and 76 for isookanin and okanin. 

      Classification: 8a
      127 026
      Comparison of phytochemical composition of Ginkgo biloba extracts using a combination of non-targeted and targeted analytical approaches
      B. COLLINS*, S. KERNS, K. AILLON, G. MUELLER, C. RIDER, C. RIDER, E. DEROSE, R. LONDON, J. HARNLY, S. WAIDYANATHA (*Division of the National Toxicology Program, National Institute of Environmental Health Sciences, Research Triangle Park, NC 27709, USA, bradley.collins@nih.gov)

      Anal. Bioanal. Chem. 412, 6789-3809 (2020). HPTLC of Ginkgo biloba extracts on silica gel with ethyl acetate - acetic acid - formic acid - water 100:11:11:26 (1) or toluene - ethyl acetate - formic acid 7:3:1 (2). Detection under UV light at 366 nm or by spraying with  natural product reagent (NPR) and polyethylene glycol (PEG). The method allowed to distinguish between characteristic and uncharacteristic unfinished product samples based on the presence or absence of bands corresponding to caffeic acid, rutin, hyperoside, chlorogenic acid, and genistein standards.

      Classification: 7, 8a
      127 044
      Organ‑based chemo‑profiling of Echinops echinatus Roxb. using high‑performance thin‑layer chromatography (HPTLC) technique
      N. BHATT*, R. GUPTA, Y. BANSAL (*Department of Botany, Punjabi University, Patiala, Punjab, India, bhattnusrat91@gmail.com)

      J. Planar Chromatogr. 34, 173-181 (2021). HPTLC of caffeic acid (1), chlorogenic acid (2), quercetin (3), oleanolic acid (4), lupeol (5), betulinic acid (6), β-Sitosterol (7), campesterol (8) and ergosterol (9) in samples of Echinops echinatus on silica gel with toluene - ethyl acetate - formic acid - methanol 30:30:8:3 for (1) and (2), toluene - ethyl acetate - formic acid 5:4:1 for (3), toluene - methanol 9:1 for (4), petroleum ether - ethyl acetate - toluene 7:2:1 for (5) and (6), toluene - ethyl acetate 9:1 for (7) and toluene - methanol - formic acid for (8) and (9). Quantitative determination by absorbance measurement at 254 nm for (1) to (3), 540 nm for (4) to (6) and 530 nm for (7) to (9). The hRF values for (1) to (9) were 69, 80, 60, 30, 68, 55, 26, 67 and 75, respectively. Linearity was between 2 and 12 µg/mL for (1) to (9). Intermediate precision was below 2 % (n=6). The LOD and LOQ were 38 and 119 ng/zone for (1), 18 and 57 ng/zone for (2), 364 and 1100 ng/zone for (3), 11 and 32 ng/zone for (4), 40 and 123 ng/zone for (5), 15 and 46 ng/zone for (6), 8 and 23 ng/zone for (7), 52 and 159 ng/zone for (8) and 527 and 1598 ng/zone for (9), respectively. Recovery was between 95.7 and 99.6 % for (1) to (9). 

      Classification: 8a, 13c, 14
      127 050
      A validated high‑performance thin‑layer chromatography method for quantification of echioidin from Andrographis echioides plant
      B. GHULE*, P. KAKAD, A. SHIRKE, N. KOTAGALE, L. RATHI (*Department of Pharmacognosy, Government College of Pharmacy, Kathora Naka, Amravati, Maharashtra 444604, India, ghulebv@rediffmail.com)

      J. Planar Chromatogr. 34, 131-138 (2021). HPTLC of echioidin in Andrographis echioides on silica gel with chloroform - methanol 17:3. Quantitative determination by absorbance measurement at 266 nm. The hRF value for echioidin was 61. Linearity was between 200 and 1000 ng/zone. Intermediate precision was below 2 % (n=3). The LOD and LOQ were 11 and 34 ng/zone. Average recovery was 99.0 %.

      Classification: 8a
      127 054
      Simultaneous quantification of four active metabolites in Psidium guajava L. by a validated high‑performance thin‑layer chromatography method
      S. TIWARI*, P. SHUKLA, J. DWIVEDI, S. KHATOON (*Department of Chemistry, Mansarovar Global University, Bhopal, India, surabhitiwari55@gmail.com)

      J. Planar Chromatogr. 34, 61-69 (2021). HPTLC of quercetin (1), gallic acid (2), eugenol (3) and β-sitosterol (4) in Psidium guajava on silica gel with toluene - ethyl acetate - formic acid 7:3:1 for (1) and (2) and toluene - ethyl acetate - formic acid 18:2:1 for (3) and (4). Detection by spraying with vanillin reagent. Quantitative determination of (1) - (4) by absorbance measurement at 254 nm, 370 nm, 570 nm and 600 nm. The hRF values for (1) to (4) were 52, 28, 87 and 59, respectively. Linearity was between 1 and 5 µg/zone for (1) and 2 and 10 µg/zone for (2) to (4). Intermediate precision was below 5 % (n=3). The LOD and LOQ were 535 and 1621 ng/zone for (1), 1059 and 3210 ng/zone for (2), 1034 and 3134 ng/zone for (3) and 1059 and 3210 ng/zone for (3), respectively. Average recovery was 100.0 % for (1) to (4).

      Classification: 8a
      127 056
      Qualitative and quantitative analyses of labiatenic acid, apigenin and buddleoside in Hyssopus officinalis by high‑performance thin‑layer chromatography
      X. HAN (Han Xue), L. LI (Li Li)*, J. DIAO (Diao Juanjuan) (*School of Pharmacy, Xinjiang Medical University, Urumqi 830011, Xinjiang, China, llxjmu@163.com)

      J. Planar Chromatogr. 34, 34-45 (2021). HPTLC of labiatenic acid (synonym: rosmarinic acid) (1), apigenin (2) and buddleoside (3) in Hyssopus officinalis on silica gel with dichloromethane - ethyl acetate - formic acid 6:5:1. Detection by spraying with 2 % aluminum trichloride ethanol solution, followed by heating until the zones were clear. Quantitative determination by absorbance measurement at 330 nm. The hRF values for (1) to (3) were 20, 36 and 59, respectively. Linearity was between 90 and 454 ng/zone for (1), 33 and 197 ng/zone for (2) and 20 and 120 ng/zone for (3). Intermediate precision was below 4 % (n=6). Average recovery was 101.3 % for (1), 99.8 % for (2) and 100.5 % for (3).

      Classification: 8a
      127 059
      A high‑performance thin‑layer chromatography method for the simultaneous determination of quercetin and gallic acid in Eclipta alba and Guiera senegalensis
      M. KHALID*, M. ALQARNI, A. FOUDAH, P. ALAM (*Department of Pharmacognosy, College of Pharmacy, Prince Sattam Bin Abdulaziz University, Po Box No. 173, Al-Kharj 11942, Kingdom of Saudi Arabia, drkhalid8811@gmail.com)

      J. Planar Chromatogr. 34, 39-44 (2021). HPTLC of gallic acid (2) and quercetin (1) in Eclipta alba and Guiera senegalensis on silica gel with toluene - ethyl acetate - glacial acetic acid 6:3:1. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) and (2) were 58 and 76. Linearity was between 200 and 2000 ng/zone for both (1) and (2). Intermediate precision was below 2 % (n=3). The LOD and LOQ were 3 and 10 ng/zone for (1) and 13 and 39 ng/zone for (2). Recovery was between 98.9 and 113.2 % for (1) and 100.8 and 113.7 % for (2).

      Classification: 8a