Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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J. Planar Chromatogr. 5, 282-283 (1992). TLC of 4-methylbenzyl alcohol, 2-phenylethanol, 1-phenyl-1-ethanol, myristyl alcohol, isoborneol, menthol, cetyl and stearyl alcohol on silica with hexane - acetone 8:2. Detection with thymol blue and bromothymol blue (each dissolved in aqueous sodium hydroxide solution, 2 %, 100 mL), evaluation 10 min. after spraying, then heating at 110 °C for 10 min. and re-examination. Detection limit: between 1.5 and 12 µg.
Journal of Pharmacy Research 4(5), 1401-1404 (2011). HPTLC of fluconazole and its structurally related impurities, on silica gel (prewashed with methanol) with n-butanol - water - acetic acid 8:2:1 with chamber saturation for 20 min. The hRf value of fluconazole was 67 and of the two separated impurities 49 (impurity B) and 79 (impurity E). Quantitative determination by densitometry in absorbance mode at 254 nm. The method was linear in the range of 1-6 µg/band for fluconazole and 0.5-2.5 µg/band for both impurities.
Apoth. Ztg. 125, 1163-1166 (1985). Zum Nachweis des Ethanols als 3,5-Dinitrobenzoesäureethylester. (Determination of ethanol as 3,5-dinitrobenzoic acid ethyl ester). Determination of ethanol, methanol, propanol, isopropanol, butanol as 3,5-dinitrobenzoic acid esters on RP-18 silica with methanol - dioxane - water 3:1:1. Detection by UV.
J. Planar Chromatogr. 8, 420-426 (1995). Introduction of a thermodynamic definition of a mixed (adsorption - partition) mechanism of solute retention in liquid chromatography on chemically bonded alkyl stationary phases, together with a practical example of how to quantify the complementary contributions, which certainly differ from one solute to another. - TLC of 5 higher fatty alcohols (lauryl, myristyl, cetyl, stearyl, and arachidyl alcohol) on silica with mixtures of 2-propanol - hexane, heptane, or octane, and t-butanol - hexane in different proportions. Detection by spraying with a 0.1% solution of Rhodamine B in water.
J. Planar Chromatogr. 24, 160-165 (2011). HPTLC of venlafaxine hydrochloride in bulk and formulations on silica gel with butanol - acetic acid - water 3:1:1. Quantitative determination by densitometry in absorbance mode at 284 nm. The hRf value was 58. Linearity was between 100 and 600 ng/zone. The limit of detection and quantification was 39 and 131 ng/zone, respectively. The repeatability and the intermediate precision (%RSD, n = 6), were between 0.3-0.7 % and 0.6-0.9 %, respectively. The recovery was between 99.1 and 101.7 %.
J. Chromatogr. 341, 426-431 (1985). TLC of the fluorescent derivatives formed from primary or secondary alcohols and 3-chloroformyl-7- methoxycoumarin on silica with benzene - ethyl acetate 8:2. Rf values and detection limits for several alcohols were given. 1) HPLC method was also described, 2) 17-oxosteroids were determined in urine from normal humans after enzymic hydrolysis, extraction, and derivatization with 3-chloroformyl-7-methoxycoumarin.
Selected application: lower alcohols, tryptophan enantiomers, gold and platinum. J. Chromatogr. A 746, 261-268 (1996). TLC of lower alcohols on cellulose with butanol - NH3 30 % 1:1. Detection by spraying with 5% NiSO4. TLC of tryptophan enantiomers on cellulose with 1M NaCl and 40 mM a-cyclodextrin solution at 7°C. Detection by exposure to iodine vapor. TLC of gold and platinum on cellulose with 2.5 M HCl. Detection by spraying with 1M Na2S. Quantification by videodensitometry. Comparison with previous TLC method.
J. Planar Chromatogr. 24, 529-533 (2011). HPTLC of fluconazole (2-(2-difluorophenyl)-1,3-bis(1H-1,2,4-triazol-1-yl)-2-propanol) on silica gel with ethyl acetate - methanol - ammonia - diaminoethane 170:20:10:1. Quantitative determination by densitometry at 216 nm. The hRf value was 40. The %RSD for repeatability and intermediate precision were 1.6 and 3.1 %, respectively. The mean recovery was 99.1 %.