Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      64 205
      Influence of gases on the HPTLC determination of some fluorescent fluorobenzoxadiazole-thiol derivatives
      B. LINLING, W.R.G. BAEYSENS, H. MARYSAEL, K. STRAGIER, (State Univ. of Ghent, Fac. of Pharm. Sci., Lab. of Pharm., Chem. and Drug Anal., Pharm. Inst., Havelbethestr. 72, B-9000 Ghent, Belgium)

      J. High Resol. Chrom. 12, 345-347 (1989). TLC separation of thiol compounds (captopril, coenzyme A, cysteamine HCl, cysteine HCl, glutathione) after derivatization with ammonium 7-flurobenzo-2-oxa-1,3-diazole-4-sulfonate (SBD-F) on HPTLC silica with isopropylether - methanol - water - acetic acid 9:8:2:1 as eluent in a twin trough chamber. Visualization under UV 366 nm, quantification by densitometry. Enhancement at signals by nitrogen- or helium-flushing.

      Keywords: densitometry
      Classification: 3e, 24
      68 114
      2-Trichloromethylbenzimidazole, a selective chromogenic reagent for the detection of o-phenylenediamine on thin-layer plates
      L. KONOPSKI, (Inst. Ind. Org. Chem., 03-236 Warsaw, Poland)

      J. Chromatogr. 541, 480-482 (1991). Description of a new, selective method for the detection of o-phenylenediamine and some of its derivatives on TLC plates by treating the chromatograms with Me trichloromethylacetimidate and exposing to pyridine vapor. Detection limits, between 80 and 2000 ng.

      Keywords:
      Classification: 3e, 17
      77 020
      Thin-layer chromatography with chemiluminescent detection of enhancers of the luminol -H2O2-peroxidase system
      A.N. DIAZ, F.G. SANCHEZ*, J.A. GONZALEZ GARCIA, (*Dept. De Quim. Anal., Fac. de Ciencias, Univ. de Malaga, 29071 - Malaga, Spain)

      J. Chromatogr. A 724, 411-415 (1996). TLC of p-iodophenol and p-coumaric acid on cellulose with 0.1 M tris-HCl buffer (pH 8.5). Detection by spraying with a solution of 2mM luminol, 6 mM H2O2 and 0.744 U/mL peroxidase in a 0.094 M tris-HCl buffer (pH 8.5). Determination by densitometry with a single optical fibre that collected the emission signal to a spectrometer. Detection limit 38 ng and 14 ng respectively.

      Classification: 3e, 4e
      85 141
      A new visualization reagent for cation separation by TLC
      A. PATRUT, C. MARUTOIU*, O.-F. MARUTOIU, M. I. MOISE, (*Inst. of Chem. 'Raluca Ripan', 30 F‚nt‚nele Street, Ro-3400 Cluj-Napoca, Romania)

      J. Planar Chromatogr. 13, 151-153 (2000). TLC separation of Cr, Mn, Fe, Co, Ni, Cu, Zn, Ag, Cd, Pb on cellulose with methanol - benzene - ethyl methyl ketone - 1-butanol - 25% NH3 6:4:4:3:3, methanol - benzene - ethyl acetate - ethyl methyl ketone - 25% NH3 5:4:5:3:3, and methanol - benzene - ethyl methyl ketone - 1-butanol - 2 M HCl 6:4:4:3:3. Detection after drying by spraying with a new visualization reagent, a 0.01% solution of 9-formylacridine in dichloromethane. The plates were then heated at 120°C for 10 min and examined under UV 366 nm.

      Keywords:
      Classification: 3e, 33a
      97 010
      Planar chromatography of heterocyclic thiols with detection by use of the iodine-azide reaction
      R. ZAKREWSKI*, W. CIESELSKI (*Department of Instrumental Analysis, University of Lodz, Pomorska 163, 90-236 Lodz, Poland)

      J. Planar Chromatogr. 19, 4-9 (2006). TLC and HPTLC of 2-thioguanidine and 6-mercaptopurine on silica gel with methanol in a horizontal DS-chamber. Spots were visualized with a freshly prepared solution of sodium azide and starch, adjusted to a pH within the range 5.5-6.0, and then exposed to iodine vapor. The thiols became visible as white spots on a violet-gray background. The iodine-azide reagent enabled detection of quantities in the range 1-80 pmol per spot.

      Classification: 3e
      100 012
      Coralyne cation, a fluorescent probe for general detection in planar chromatography
      Elena MATEOS, V.L. CEBOLLA*, L. MEMBRADO, J. VELA, Eva GALVEZ, Muriel MATT, F.P. COSSIO (*Instituto de Carboquímica, CSIC, P.O. Box 549, 50080 Zaragoza, Spain; vcebolla@carbon.icb.csic.es)

      J. Chromatogr. A 1046 (2), 251-257 (2007). Fluorescence scanning densitometry of various analytes on HPTLC silica gel plates impregnated with a solution of coralyne cation, based on the increase or decrease, that the corresponding analyte induces on native coralyne emission at a given excitation wavelength. Compared to a procedure previously described for berberine cation, and Reichardt's dye probes, the sensitivity of coralyne in HPTLC detection of non-fluorescent, structurally different analytes (e.g. long-chain alkanes, alcohols, alkylbromides, neutral lipids) is superior.

      Classification: 3e
      112 012
      Modified ninhydrin reagents to detect colors of amino acid zones on thin-layer chromatographic plates
      A. SINHABABU*, S. BASU (*Natural Product Laboratory, Department of Chemistry, The University of Burdwan, Burdwan – 713 104, West Bengal, India, sinhababu04@yahoo.co.in)

      J. Planar Chromatogr. 26, 517-520 (2013). TLC of amino acids on silica gel with 1-propanol - water 7:3. Detection by spraying with (1) 1 % 2-hydroxybenzenecarbaldehyde solution in propanone; or (2) 1 % 4-bromobenzenecarbaldehyde solution in propanone (2), followed by heating at 110 ºC for 10 min. After cooling, all plates (treated with (1) or (2)) were sprayed with ninhydrin (indane-1,2,3-trione monohydrate) reagent and air dried. Amino acid zones in various shades from yellow to brownish-red were detected (detailed table provided in paper). Plates were heated again at 110°C for 10 min and color changes were recorded. The LOD were determined visually by comparison of standard solutions (1 mg/L) and further dilution until no zone was seen. LOD for (1) and (2) were in the range of 0.1-1.0 µg/zone and 0.01-1.0 µg/zone, respectively.

      Classification: 3e, 18a
      58 072
      Techniques for quantitative high-performance thin-layer chromatographic analysis for nonfluorescent compounds as exemplified by bile acid determination
      R. KLAUS

      J. Chromatogr. 333, 276-287 (1985). HPTLC of lacking native fluorescence but which can be converted to fluorescent derivatives: cholic acid, deoxycholic acid, hydroxycholic acid, glycocholic acid, lithocholic acid and taurocholic acid on silica with isooctane - ethyl acetate - formic acid - diisopropyl ether 5:4:1:1. Derivatization with 5 % perchloric acid in methanol.

      Classification: 3e, 13d