Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      83 011
      Teaching the basics of pharmaceutical analysis by thin-layer chromatography and high-performance thin-layer chromatography to undergraduate students - laboratory practicals
      J.-P. SALO, H. SALOMIES, (Univ. of Helsinki, Div. of Pharm. Chem., Dept. of Pharm., P.O. Box 56 (Viikinkaari 5 E), FIN-00014, Helsinki, Finland)

      J. AOAC Int. 82, 38-47 (1999). Description of a 2-day program with 9 exercises in TLC in order to teach the basics of the technique including the preparation of written reports. The exercise consisted i.a. of the study of the influence of several factors on chromatographic behavior (e.g. sorbent type, layer thickness, particle size and distribution, chamber saturation, 2-dimensional TLC, HPTLC); visualization techniques, and discussion of the results. Substances chromatographed, e.g. benzodiazepines, sulfonamides.

      Keywords:
      Classification: 2a
      96 009
      Methods for detecting and reducing systematic errors in quantitative planar chromatography
      R.E. KAISER (Institute for Chromatography, P. O. Box 1141, 67085 Bad Dürkheim, Germany)

      - Part 1. Fundamentals of systematic quantitative errors. J. Planar Chromatogr. 18, 51-56 (2005). First part of a series covering systematic errors arising in separation systems, evaluation and calibration errors, nonlinear separation and quantitation techniques, the sf4-procedure for finding total systematic errors, systematic errors caused by regulations, and conclusions and proposals for quantitative planar liquid chromatography (PLC). 1) Nonsystematic errors: 1.1 Finding systematic errors hidden in nonsystematic errors, 1.2 Are random errors unstable? 1.3 Errors caused by (false) statements. 2) The main sources of systematic errors in quantitative PLC: 2.1 Chromatography, 2.2 Physics (baseline - baseplane; practical example). 2.3 Mathematics (detectability limit of the systematic error and the standard certainty STC). 3) Sampling chromatography.

      Classification: 2a
      55 008
      Correlation in continuous development thin-layer chromatography
      R. TECKLENBURG, D. NUROK

      Chromatographia 18, 249-252 (1984). TLC of 25 steroids on silica with ethyl acetate1,1,2-trichlorotrifluoroethane, in various proportions. Detection by spraying with 10 % aqueous sulfuric acid. Discussion of the relationship of binary solvent systems used in continuous development TLC.

      Keywords:
      Classification: 2b
      68 024
      Solid-state dissociation of metal chelates and reagents in a silica gel stationary phase in TLC
      V.V. SALOV, A.R. TIMERBAEV, O.M. PETRUKHIN*, (*Mendeleev Institute of Chemical Technology, Miusskaya pl. 9 125820 Moskow, USSR)

      J. Planar Chromatogr. 3, 73-76 (1990). Construction of an equilibrium simulation model to describe the chromatographic properties of chelates and reagents, dissociation of silanol groups and reagents, step dissociation of complexes, exchange of chelate metal for the hydrogen atom of silanol groups, and solvent adsorption on adsorption centers. This model facilitates an adequate description of the dependence of chelate and reagent Rf values on their concentration in the sorbent layer.

      Keywords:
      Classification: 2b
      76 008
      Verification of thin layer chromatography theory
      J. BLADEK*, A. ROSTOWSKI, (*Inst. of Chem., Military University of Technology, Kaliskiego 2, 01-489 Warsaw, Poland)

      Part 1: The characteristics of the initial, non-equilibrium stage of the chromatographic separation. J. Planar Chromatogr. 8, 430-438 (1995). Investigation of the factors which influence the progress of a chromatographic separation. Profiting from the properties of a liquid-crystalline detector, distributions of spot concentration at the origin, and the disturbance of these distributions during the initial, nonequilibrium stages of chromatogram development, have been displayed as three-dimensional images. The influence on the shapes of these images of the concentration of the solution investigated, the polarity of the solvent used to dissolve the sample, the volume applied, and the type of sorbent have been determined.

      Keywords:
      Classification: 2b
      100 004
      Partial least-squares study of the effects of organic modifier and physicochemical properties on the retention of some thiazoles
      Tatjana DJAKOVIC-SEKULIC*, N. PERISIC-JANJIC, C. SARBU, Z. LOZANOV-CRVENKOVIC (*Department of Chemistry, Faculty of Sciences, University of Novi Sad, Trg D. Obradovica 3, 21000 Novi Sad, Serbia; tanja@ih.ns.ac.yu)

      J. Planar Chromatogr. 20, 251-257 (2007). TLC with aqueous ammonia-organic modifier (acetonitrile, dioxane, acetone) mobile phases has been used to study the effect on retention of the chromatographic system and the physicochemical properties of twelve 2,4-dioxotetrahydro-1,3-thiazoles. Principal-component analysis and partial least-squares regression were used to determine the molecular properties with the greatest effect on retention for each modifier. Good correlation was obtained between experimental and calculated retention data. HPTLC on RP-18 without chamber saturation. Detection under UV 254 nm.

      Classification: 2c
      111 002
      A comparative study of the lipophilicity of 1,2,4-triazoles by reversed-phase and micellar TLC and OPLC
      M. JANICKA*, K. STEPNIK, A. PACHUTA (*Maria Curie-Skodowska University, Department of Physical Chemistry, Faculty of Chemistry, Maria Curie-Skodowska Sq. 3, 20-031 Lublin, Poland, malgorzata.janicka@poczta.umcs.lublin.pl)

      J. Planar Chromatogr. 26, 153-159 (2013). TLC lipophilicities of 21 newly synthesized 1,2,4-triazoles on RP-8 and RP-18 with buffered solutions of acetone, 1,4-dioxane, tetrahydrofuran and acetonitrile as well as on cyano phase with solutions of 0.03, 0.04, 0.06, 0.08 and 0.1 M sodium dodecyl sulfate modified with the constant (20 %) addition of organic modifier (acetone, 1,4-dioxane, tetrahydrofuran and acetonitrile). Partitioning lipophilicity indices showed mobile phase composed of sodium dodecyl sulfate and tetrahydrofuran as the system providing the best linear correlations between chromatographic and partitioning lipophilicities of tested 1,2,4-triazoles.

      Classification: 2c
      115 002
      A comparative quantitative structure-retention relationships study for lipophilicity determination of compounds with a phenanthrene skeleton on cyano-, reversed phase-, and
      normal phase-thin layer chromatography stationary phases
      K. CIURA*, J. NOWAKOWSKA, P. PIKUL, W. STRUCK, M. MARKUSZEWSKI (*Medical University of Gda?sk, Faculty of Pharmacy, Department of Physical Chemistry, Al. Gen. J. Hallera 107, 80-416, Gda?sk, Poland, krzesimir.ciura@gmail.com)

      J. AOAC Int. 98, 345-353 (2015). HPTLC of 14 derivatives containing the phenanthrene skeleton on RP, CN and NP phases. Quantitative structure-retention relationship analysis determined that the best conditions to predict log P was RP with acetone–water ranging from 30 to 80 % in 10 % increments of the organic modifier.

      Classification: 2c